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1a13

G PROTEIN-BOUND CONFORMATION OF MASTOPARAN-X, NMR, 14 STRUCTURES

Method: SOLUTION NMR Dmax: 15.8 Å Quality: REASONABLE

SAXS Profile

SAXS profile for 1a13

P(r) Distribution

P(r) distribution for 1a13

1. Structure Basics

entry_id1a13
deposition_date1997-12-20
titleG PROTEIN-BOUND CONFORMATION OF MASTOPARAN-X, NMR, 14 STRUCTURES
keywordsMAST CELL DEGRANULATION; MAST CELL DEGRANULATION
methodSOLUTION NMR

Download Data

2. SAXS Parameters (CRYSOL)

rg_guinier5.65
rg_electron6.73
i05139470.00
molecular_weight21826.0 kDa
excluded_volume29007 ų
envelope_volume4006 ų
shell_volume4658 ų
envelope_diameter27.9
shell_rg12.57
envelope_rg8.47
shape_rg6.67
total_rg7.53
total_atoms3346
n_residues196
n_harmonics20
q_range— – 0.5000 −1
n_points101
shell_typedirectional
solvent_density0.3340 e/ų
contrast_shell0.0300 e/ų
crysol_version4.1.3

3. P(r) Analysis (GNOM)

dmax15.8
rg_real5.44
rg_real_error0.02
i0_real4.9690e+06
i0_real_error2.6460e+04
rg_reciprocal5.78
i0_reciprocal5139000.0000
total_estimate0.6536
solution_quality REASONABLE a REASONABLE solution
n_peaks1
r_peak_primary5.0
skewness0.311
kurtosis-0.753
angular_range— – 0.5000 −1
current_alpha8.2280
highest_alpha232.9000
n_real_points80
gnom_version4.1.3
quality_criteria AN1: 0.000; Oscil: 0.993; Stabil: 0.972; Sysdev: 0.000; Positv: 1.000; Valcen: 0.603; Smooth: 0.000

4. Crystallography & Experiment

5. Entities & Polymer Info (1)

6. Citations (1)

7. Files & Curves (10)