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1b2g

PH AFFECTS GLU B13 SWITCHING AND SULFATE BINDING IN CUBIC INSULIN CRYSTALS (PH 9.00 COORDINATES)

Method: X-RAY DIFFRACTION Dmax: 36.4 Å Quality: GOOD

SAXS Profile

SAXS profile for 1b2g

P(r) Distribution

P(r) distribution for 1b2g

1. Structure Basics

entry_id1b2g
deposition_date1998-11-26
titlePH AFFECTS GLU B13 SWITCHING AND SULFATE BINDING IN CUBIC INSULIN CRYSTALS (PH 9.00 COORDINATES)
keywordsHORMONE, HORMONE-GROWTH FACTOR COMPLEX; HORMONE/GROWTH FACTOR
methodX-RAY DIFFRACTION

Download Data

2. SAXS Parameters (CRYSOL)

rg_guinier11.29
rg_electron9.90
i0824784.00
molecular_weight5782.0 kDa
excluded_volume7173 ų
envelope_volume7763 ų
shell_volume6980 ų
envelope_diameter33.3
shell_rg15.02
envelope_rg10.24
shape_rg9.91
total_rg11.35
total_atoms403
n_residues51
n_harmonics20
q_range— – 0.5000 −1
n_points101
shell_typedirectional
solvent_density0.3340 e/ų
contrast_shell0.0300 e/ų
crysol_version4.1.3

3. P(r) Analysis (GNOM)

dmax36.4
rg_real11.23
rg_real_error0.30
i0_real8.2480e+05
i0_real_error8.4850e+03
rg_reciprocal11.23
i0_reciprocal824800.0000
total_estimate0.8886
solution_quality GOOD a GOOD solution
n_peaks2
r_peak_primary14.8
skewness0.134
kurtosis-0.311
angular_range— – 0.5000 −1
current_alpha0.0000
highest_alpha82370.0000
n_real_points80
gnom_version4.1.3
quality_criteria AN1: 0.000; Oscil: 0.864; Stabil: 0.999; Sysdev: 1.000; Positv: 1.000; Valcen: 1.000; Smooth: 0.961

4. Crystallography & Experiment

5. Entities & Polymer Info (3)

6. Citations (7)

7. Files & Curves (10)