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1b4c

SOLUTION STRUCTURE OF RAT APO-S100B USING DIPOLAR COUPLINGS

Method: SOLUTION NMR Dmax: 53.1 Å Quality: GOOD

SAXS Profile

SAXS profile for 1b4c

P(r) Distribution

P(r) distribution for 1b4c

1. Structure Basics

entry_id1b4c
deposition_date1998-12-17
titleSOLUTION STRUCTURE OF RAT APO-S100B USING DIPOLAR COUPLINGS
keywords;S100BETA, S100B, DIPOLAR COUPLINGS, EF-HAND, S100 PROTEIN, CALCIUM- BINDING PROTEIN, FOUR-HELIX BUNDLE, THREE-DIMENSIONAL STRUCTURE, SOLUTION STRUCTURE, METAL BINDING PROTEIN ;; METAL BINDING PROTEIN
methodSOLUTION NMR

Download Data

2. SAXS Parameters (CRYSOL)

rg_guinier17.75
rg_electron16.92
i02968150000.00
molecular_weight450620.0 kDa
excluded_volume556580 ų
envelope_volume47246 ų
shell_volume20919 ų
envelope_diameter59.0
shell_rg25.29
envelope_rg18.51
shape_rg16.92
total_rg17.01
total_atoms61320
n_residues3864
n_harmonics20
q_range— – 0.5000 −1
n_points101
shell_typedirectional
solvent_density0.3340 e/ų
contrast_shell0.0300 e/ų
crysol_version4.1.3

3. P(r) Analysis (GNOM)

dmax53.1
rg_real17.58
rg_real_error0.27
i0_real2.9680e+09
i0_real_error3.5960e+07
rg_reciprocal17.60
i0_reciprocal2968000000.0000
total_estimate0.8933
solution_quality GOOD a GOOD solution
n_peaks2
r_peak_primary22.6
skewness-0.024
kurtosis-0.516
angular_range— – 0.4500 −1
current_alpha0.0000
highest_alpha771200.0000
n_real_points76
gnom_version4.1.3
quality_criteria AN1: 0.000; Oscil: 0.892; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.974; Smooth: 0.960

4. Crystallography & Experiment

5. Entities & Polymer Info (1)

6. Citations (3)

7. Files & Curves (10)