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1bus

SOLUTION CONFORMATION OF PROTEINASE INHIBITOR IIA FROM BULL SEMINAL PLASMA BY 1H NUCLEAR MAGNETIC RESONANCE AND DISTANCE GEOMETRY

Method: SOLUTION NMR Dmax: 44.8 Å Quality: GOOD

SAXS Profile

SAXS profile for 1bus

P(r) Distribution

P(r) distribution for 1bus

1. Structure Basics

entry_id1bus
deposition_date1990-05-14
titleSOLUTION CONFORMATION OF PROTEINASE INHIBITOR IIA FROM BULL SEMINAL PLASMA BY 1H NUCLEAR MAGNETIC RESONANCE AND DISTANCE GEOMETRY
keywordsPROTEINASE INHIBITOR; PROTEINASE INHIBITOR
methodSOLUTION NMR

Download Data

2. SAXS Parameters (CRYSOL)

rg_guinier11.77
rg_electron11.37
i018418600.00
molecular_weight30920.0 kDa
excluded_volume37486 ų
envelope_volume16537 ų
shell_volume10997 ų
envelope_diameter46.0
shell_rg18.55
envelope_rg13.11
shape_rg11.36
total_rg12.12
total_atoms2740
n_residues280
n_harmonics20
q_range— – 0.5000 −1
n_points101
shell_typedirectional
solvent_density0.3340 e/ų
contrast_shell0.0300 e/ų
crysol_version4.1.3

3. P(r) Analysis (GNOM)

dmax44.8
rg_real11.74
rg_real_error0.36
i0_real1.8420e+07
i0_real_error1.9460e+05
rg_reciprocal11.74
i0_reciprocal18420000.0000
total_estimate0.8219
solution_quality GOOD a GOOD solution
n_peaks2
r_peak_primary14.8
skewness0.237
kurtosis-0.282
angular_range— – 0.5000 −1
current_alpha0.0000
highest_alpha173500.0000
n_real_points80
gnom_version4.1.3
quality_criteria AN1: 0.000; Oscil: 0.613; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.845; Smooth: 0.996

4. Crystallography & Experiment

5. Entities & Polymer Info (1)

6. Citations (4)

7. Files & Curves (10)