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1ccm

DIRECT NOE REFINEMENT OF CRAMBIN FROM 2D NMR DATA USING A SLOW-COOLING ANNEALING PROTOCOL

Method: SOLUTION NMR Dmax: 31.0 Å Quality: REASONABLE

SAXS Profile

SAXS profile for 1ccm

P(r) Distribution

P(r) distribution for 1ccm

1. Structure Basics

entry_id1ccm
deposition_date1993-04-14
titleDIRECT NOE REFINEMENT OF CRAMBIN FROM 2D NMR DATA USING A SLOW-COOLING ANNEALING PROTOCOL
keywordsPLANT SEED PROTEIN; PLANT SEED PROTEIN
methodSOLUTION NMR

Download Data

2. SAXS Parameters (CRYSOL)

rg_guinier9.04
rg_electron9.58
i023759800.00
molecular_weight37892.0 kDa
excluded_volume46550 ų
envelope_volume7799 ų
shell_volume6864 ų
envelope_diameter32.2
shell_rg15.20
envelope_rg10.56
shape_rg9.60
total_rg9.82
total_atoms2616
n_residues368
n_harmonics20
q_range— – 0.5000 −1
n_points101
shell_typedirectional
solvent_density0.3340 e/ų
contrast_shell0.0300 e/ų
crysol_version4.1.3

3. P(r) Analysis (GNOM)

dmax31.0
rg_real9.02
rg_real_error0.33
i0_real2.3760e+07
i0_real_error2.5790e+05
rg_reciprocal9.02
i0_reciprocal23760000.0000
total_estimate0.6640
solution_quality REASONABLE a REASONABLE solution
n_peaks1
r_peak_primary30.6
skewness0.167
kurtosis-0.468
angular_range— – 0.5000 −1
current_alpha0.0000
highest_alpha14470.0000
n_real_points80
gnom_version4.1.3
quality_criteria AN1: 0.000; Oscil: 0.855; Stabil: 1.000; Sysdev: 0.368; Positv: 1.000; Valcen: 0.959; Smooth: 0.000

4. Crystallography & Experiment

5. Entities & Polymer Info (1)

6. Citations (6)

7. Files & Curves (10)