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1ccn

DIRECT NOE REFINEMENT OF CRAMBIN FROM 2D NMR DATA USING A SLOW-COOLING ANNEALING PROTOCOL

Method: SOLUTION NMR Dmax: 34.5 Å Quality: GOOD

SAXS Profile

SAXS profile for 1ccn

P(r) Distribution

P(r) distribution for 1ccn

1. Structure Basics

entry_id1ccn
deposition_date1993-04-14
titleDIRECT NOE REFINEMENT OF CRAMBIN FROM 2D NMR DATA USING A SLOW-COOLING ANNEALING PROTOCOL
keywordsPLANT SEED PROTEIN; PLANT SEED PROTEIN
methodSOLUTION NMR

Download Data

2. SAXS Parameters (CRYSOL)

rg_guinier10.38
rg_electron9.59
i0607091.00
molecular_weight4736.0 kDa
excluded_volume5819 ų
envelope_volume6138 ų
shell_volume5895 ų
envelope_diameter31.1
shell_rg14.29
envelope_rg9.96
shape_rg9.62
total_rg10.92
total_atoms327
n_residues46
n_harmonics20
q_range— – 0.5000 −1
n_points101
shell_typedirectional
solvent_density0.3340 e/ų
contrast_shell0.0300 e/ų
crysol_version4.1.3

3. P(r) Analysis (GNOM)

dmax34.5
rg_real10.36
rg_real_error0.23
i0_real6.0710e+05
i0_real_error5.5660e+03
rg_reciprocal10.36
i0_reciprocal607100.0000
total_estimate0.8821
solution_quality GOOD a GOOD solution
n_peaks2
r_peak_primary12.2
skewness0.279
kurtosis-0.265
angular_range— – 0.5000 −1
current_alpha0.0000
highest_alpha57720.0000
n_real_points80
gnom_version4.1.3
quality_criteria AN1: 0.000; Oscil: 0.873; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.983; Smooth: 0.862

4. Crystallography & Experiment

5. Entities & Polymer Info (1)

6. Citations (6)

7. Files & Curves (10)