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1d00

STRUCTURE OF TNF RECEPTOR ASSOCIATED FACTOR 2 IN COMPLEX WITH A 5-RESIDUE CD40 PEPTIDE

Method: X-RAY DIFFRACTION D_max: 134.1 Å Quality: GOOD

SAXS Profile

P(r) Distribution

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1. Structure Basics

entry_id	1d00
deposition_date	1999-09-07
title	STRUCTURE OF TNF RECEPTOR ASSOCIATED FACTOR 2 IN COMPLEX WITH A 5-RESIDUE CD40 PEPTIDE
keywords	B-SANDWICH, PROTEIN-PEPTIDE COMPLEX, APOPTOSIS; APOPTOSIS
method	X-RAY DIFFRACTION

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Download Data

SAXS curve (.dat) P(r) distribution (.pr.out) Structure (CIF)

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2. SAXS Parameters (CRYSOL)

rg_guinier	41.55 Å
rg_electron	41.11 Å
i0	326711000.00
molecular_weight	150610.0 kDa
excluded_volume	189650 Å³
envelope_volume	262030 Å³
shell_volume	54738 Å³
envelope_diameter	134.9 Å
shell_rg	45.13 Å
envelope_rg	40.07 Å
shape_rg	41.10 Å
total_rg	41.35 Å
total_atoms	10600
n_residues	1384
n_harmonics	20
q_range	— – 0.5000 Å⁻¹
n_points	101
shell_type	directional
solvent_density	0.3340 e/Å³
contrast_shell	0.0300 e/Å³
crysol_version	4.1.3

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3. P(r) Analysis (GNOM)

dmax	134.1 Å
rg_real	41.48 Å
rg_real_error	1.23 Å
i0_real	3.2670e+08
i0_real_error	5.5330e+06
rg_reciprocal	41.55 Å
i0_reciprocal	326700000.0000
total_estimate	0.8976
solution_quality	GOOD a GOOD solution
n_peaks	2
r_peak_primary	52.9 Å
skewness	0.219
kurtosis	-0.521
angular_range	— – 0.1900 Å⁻¹
current_alpha	0.0000
highest_alpha	29690000.0000
n_real_points	39
gnom_version	4.1.3
quality_criteria	AN1: 0.000; Oscil: 0.925; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.999; Smooth: 0.891

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4. Crystallography & Experiment

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5. Entities & Polymer Info (3)

Entity 1 polymer

description	TUMOR NECROSIS FACTOR RECEPTOR ASSOCIATED PROTEIN 2
formula_weight	19006.9 kDa
src_method	man
entity_count	8

Polymer

type	polypeptide(L)
strand_id	A,B,C,D,E,F,G,H
atom_count	10670

AMADLEQKVLEMEASTYDGVFIWKISDFARKRQEAVAGRIPAIFSPAFYTSRYGYKMCLRIYLNGDGTGRGTHLSLFFVVMKGPNDALLRWPFNQKVTLMLLDQNNREHVIDAFRPDVTSSSFQRPVNDMNIASGCPLFCPVSKMEAKNSYVRDDAIFIKAIVDLTGL

Source

organism	Homo sapiens
common_name	human
ncbi_taxonomy_id	9606
host_organism	Escherichia coli

Entity 2 polymer

description	B-CELL SURFACE ANTIGEN CD40
formula_weight	596.7 kDa
src_method	syn
entity_count	8

Polymer

type	polypeptide(L)
strand_id	I,J,K,L,M,N,O,P

XPVQETX

Entity 3 water

description	water
formula_weight	18.0 kDa
src_method	nat
entity_count	70

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6. Citations (2)

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length_a	111.400 Å
length_b	111.400 Å
length_c	111.400 Å
angle_alpha	103.70 °
angle_beta	103.70 °
angle_gamma	103.70 °
z_pdb	24

space_group	R 3
int_tables_number	146
crystal_system	—

resolution	2.000 Å
resolution_low	20.000 Å
r_factor	—
r_work	0.2190
r_free	0.2540

fit	/app/data/saxs_computation/d0/1d00/1d00.fit
pddf	/app/data/pr_computation/d0/1d00/1d00.pr.out
profile	/app/data/saxs_computation/d0/1d00/1d00.dat

STRUCTURE OF TNF RECEPTOR ASSOCIATED FACTOR 2 IN COMPLEX WITH A 5-RESIDUE CD40 PEPTIDE

SAXS Profile

P(r) Distribution

1. Structure Basics

Download Data

2. SAXS Parameters (CRYSOL)

3. P(r) Analysis (GNOM)

4. Crystallography & Experiment

Unit Cell

Symmetry

Refinement

Diffraction

5. Entities & Polymer Info (3)

Entity 1 polymer

Polymer

Source

Entity 2 polymer

Polymer

Entity 3 water

6. Citations (2)

7. Files & Curves (10)

Files (7)

Curves (3)