REDOX SIGNALING IN THE CHLOROPLAST: STRUCTURE OF OXIDIZED PEA FRUCTOSE-1,6-BISPHOSPHATE PHOSPHATASE

Method: X-RAY DIFFRACTION D_max: 108.4 Å Quality: GOOD

SAXS Profile

P(r) Distribution

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1. Structure Basics

entry_id	1dcu
deposition_date	1999-11-05
title	REDOX SIGNALING IN THE CHLOROPLAST: STRUCTURE OF OXIDIZED PEA FRUCTOSE-1,6-BISPHOSPHATE PHOSPHATASE
keywords	CHLOROPLAST, PHOTOSYNTHESIS, REDOX REGULATION, THIOREDOXIN, ALLOSTERY, HYDROLASE; HYDROLASE
method	X-RAY DIFFRACTION

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Download Data

SAXS curve (.dat) P(r) distribution (.pr.out) Structure (CIF)

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2. SAXS Parameters (CRYSOL)

rg_guinier	34.60 Å
rg_electron	33.60 Å
i0	296360000.00
molecular_weight	140640.0 kDa
excluded_volume	176500 Å³
envelope_volume	211760 Å³
shell_volume	51296 Å³
envelope_diameter	110.7 Å
shell_rg	41.49 Å
envelope_rg	33.51 Å
shape_rg	33.63 Å
total_rg	34.06 Å
total_atoms	9907
n_residues	1306
n_harmonics	20
q_range	— – 0.5000 Å⁻¹
n_points	101
shell_type	directional
solvent_density	0.3340 e/Å³
contrast_shell	0.0300 e/Å³
crysol_version	4.1.3

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3. P(r) Analysis (GNOM)

dmax	108.4 Å
rg_real	34.53 Å
rg_real_error	0.65 Å
i0_real	2.9640e+08
i0_real_error	4.6700e+06
rg_reciprocal	34.57 Å
i0_reciprocal	296400000.0000
total_estimate	0.8877
solution_quality	GOOD a GOOD solution
n_peaks	1
r_peak_primary	40.1 Å
skewness	0.251
kurtosis	-0.509
angular_range	— – 0.2300 Å⁻¹
current_alpha	0.0000
highest_alpha	230900000.0000
n_real_points	47
gnom_version	4.1.3
quality_criteria	AN1: 0.000; Oscil: 0.944; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.999; Smooth: 0.707

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4. Crystallography & Experiment

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5. Entities & Polymer Info (2)

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6. Citations (1)

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length_a	71.604 Å
length_b	126.316 Å
length_c	78.023 Å
angle_alpha	90.00 °
angle_beta	97.73 °
angle_gamma	90.00 °
z_pdb	8

space_group	P 1 21 1
int_tables_number	4
crystal_system	—

resolution	2.200 Å
resolution_low	23.800 Å
r_factor	—
r_work	0.1890
r_free	0.2470

description	FRUCTOSE-1,6-BISPHOSPHATASE
formula_weight	39242.0 kDa
ec_number	3.1.3.11
mutation	A197I, E232K
src_method	nat
entity_count	4

type	polypeptide(L)
strand_id	A,B,C,D
atom_count	10102

REDOX SIGNALING IN THE CHLOROPLAST: STRUCTURE OF OXIDIZED PEA FRUCTOSE-1,6-BISPHOSPHATE PHOSPHATASE

SAXS Profile

P(r) Distribution

1. Structure Basics

Download Data

2. SAXS Parameters (CRYSOL)

3. P(r) Analysis (GNOM)

4. Crystallography & Experiment

Unit Cell

Symmetry

Refinement

Diffraction

5. Entities & Polymer Info (2)

Entity 1 polymer

Polymer

Entity 2 water

6. Citations (1)

7. Files & Curves (10)

Files (7)

Curves (3)

description	water
formula_weight	18.0 kDa
src_method	nat
entity_count	195

fit	/app/data/saxs_computation/dc/1dcu/1dcu.fit
pddf	/app/data/pr_computation/dc/1dcu/1dcu.pr.out
profile	/app/data/saxs_computation/dc/1dcu/1dcu.dat