← Back to search
1dfy

NMR STRUCTURE OF CONTRYPHAN-SM CYCLIC PEPTIDE (MAJOR FORM-CIS)

Method: SOLUTION NMR Dmax: 16.9 Å Quality: GOOD

SAXS Profile

SAXS profile for 1dfy

P(r) Distribution

P(r) distribution for 1dfy

1. Structure Basics

entry_id1dfy
deposition_date1999-11-22
titleNMR STRUCTURE OF CONTRYPHAN-SM CYCLIC PEPTIDE (MAJOR FORM-CIS)
keywordsCYCLIC PEPTIDE, DISULFIDE BRIDGE, D-TRYPTOPHAN, CIS-TRANS ISOMERISM, CONTRYPHAN, TOXIN; TOXIN
methodSOLUTION NMR

Download Data

2. SAXS Parameters (CRYSOL)

rg_guinier4.34
rg_electron5.14
i06319400.00
molecular_weight19884.0 kDa
excluded_volume24302 ų
envelope_volume1468 ų
shell_volume2722 ų
envelope_diameter16.9
shell_rg9.60
envelope_rg5.78
shape_rg5.17
total_rg5.28
total_atoms2520
n_residues100
n_harmonics20
q_range— – 0.5000 −1
n_points101
shell_typedirectional
solvent_density0.3340 e/ų
contrast_shell0.0300 e/ų
crysol_version4.1.3

3. P(r) Analysis (GNOM)

dmax16.9
rg_real4.25
rg_real_error0.36
i0_real6.3190e+06
i0_real_error5.1730e+04
rg_reciprocal4.25
i0_reciprocal6319000.0000
total_estimate0.7885
solution_quality GOOD a GOOD solution
n_peaks2
r_peak_primary6.8
skewness-1.190
kurtosis-3.649
angular_range— – 0.5000 −1
current_alpha0.0000
highest_alpha180.8000
n_real_points80
gnom_version4.1.3
quality_criteria AN1: 0.000; Oscil: 0.534; Stabil: 0.981; Sysdev: 1.000; Positv: 1.000; Valcen: 0.874; Smooth: 0.827

4. Crystallography & Experiment

5. Entities & Polymer Info (1)

6. Citations (1)

7. Files & Curves (10)