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1dg0

NMR STRUCTURE OF DES[GLY1]-CONTRYPHAN-R CYCLIC PEPTIDE (MAJOR FORM)

Method: SOLUTION NMR Dmax: 15.2 Å Quality: GOOD

SAXS Profile

SAXS profile for 1dg0

P(r) Distribution

P(r) distribution for 1dg0

1. Structure Basics

entry_id1dg0
deposition_date1999-11-22
titleNMR STRUCTURE OF DES[GLY1]-CONTRYPHAN-R CYCLIC PEPTIDE (MAJOR FORM)
keywordsCYCLIC PEPTIDE, DISULFIDE BRIDGE, D-TRYPTOPHAN, CIS-TRANS ISOMERISM, CONTRYPHAN, TOXIN; TOXIN
methodSOLUTION NMR

Download Data

2. SAXS Parameters (CRYSOL)

rg_guinier4.28
rg_electron5.22
i05332530.00
molecular_weight18742.0 kDa
excluded_volume23105 ų
envelope_volume1356 ų
shell_volume2580 ų
envelope_diameter17.3
shell_rg9.50
envelope_rg5.75
shape_rg5.23
total_rg5.40
total_atoms2340
n_residues80
n_harmonics20
q_range— – 0.5000 −1
n_points101
shell_typedirectional
solvent_density0.3340 e/ų
contrast_shell0.0300 e/ų
crysol_version4.1.3

3. P(r) Analysis (GNOM)

dmax15.2
rg_real4.21
rg_real_error0.32
i0_real5.3330e+06
i0_real_error4.7720e+04
rg_reciprocal4.21
i0_reciprocal5333000.0000
total_estimate0.7781
solution_quality GOOD a GOOD solution
n_peaks1
r_peak_primary6.7
skewness-0.923
kurtosis-3.528
angular_range— – 0.5000 −1
current_alpha0.0000
highest_alpha143.3000
n_real_points80
gnom_version4.1.3
quality_criteria AN1: 0.000; Oscil: 0.758; Stabil: 0.989; Sysdev: 1.000; Positv: 1.000; Valcen: 0.868; Smooth: 0.000

4. Crystallography & Experiment

5. Entities & Polymer Info (1)

6. Citations (1)

7. Files & Curves (10)