1djp
CRYSTAL STRUCTURE OF PSEUDOMONAS 7A GLUTAMINASE-ASPARAGINASE WITH THE INHIBITOR DON COVALENTLY BOUND IN THE ACTIVE SITE
SAXS Profile
P(r) Distribution
1. Structure Basics
| entry_id | 1djp |
| deposition_date | 1999-12-03 |
| title | CRYSTAL STRUCTURE OF PSEUDOMONAS 7A GLUTAMINASE-ASPARAGINASE WITH THE INHIBITOR DON COVALENTLY BOUND IN THE ACTIVE SITE |
| keywords | ;PGA, Glutaminase, Asparaginase, DON, 6-diazo-5-oxo-L-norvaline, Glutaminase-Asparaginase, suicide inhibitor, covalently bound inhibitor, HYDROLASE ;; HYDROLASE |
| method | X-RAY DIFFRACTION |
Download Data
2. SAXS Parameters (CRYSOL)
| rg_guinier | 25.99 Å |
| rg_electron | 25.17 Å |
| i0 | 83808400.00 |
| molecular_weight | 70999.0 kDa |
| excluded_volume | 88625 ų |
| envelope_volume | 103180 ų |
| shell_volume | 33339 ų |
| envelope_diameter | 90.8 Å |
| shell_rg | 33.32 Å |
| envelope_rg | 25.44 Å |
| shape_rg | 25.14 Å |
| total_rg | 26.08 Å |
| total_atoms | 4990 |
| n_residues | 660 |
| n_harmonics | 20 |
| q_range | — – 0.5000 Å−1 |
| n_points | 101 |
| shell_type | directional |
| solvent_density | 0.3340 e/ų |
| contrast_shell | 0.0300 e/ų |
| crysol_version | 4.1.3 |
3. P(r) Analysis (GNOM)
| dmax | 88.1 Å |
| rg_real | 25.93 Å |
| rg_real_error | 0.51 Å |
| i0_real | 8.3810e+07 |
| i0_real_error | 1.1160e+06 |
| rg_reciprocal | 25.95 Å |
| i0_reciprocal | 83810000.0000 |
| total_estimate | 0.8770 |
| solution_quality | GOOD a GOOD solution |
| n_peaks | 1 |
| r_peak_primary | 30.3 Å |
| skewness | 0.313 |
| kurtosis | -0.312 |
| angular_range | — – 0.3050 Å−1 |
| current_alpha | 0.0000 |
| highest_alpha | 27380000.0000 |
| n_real_points | 62 |
| gnom_version | 4.1.3 |
| quality_criteria | AN1: 0.000; Oscil: 0.802; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.997; Smooth: 0.995 |