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9rca

Solution NMR structure of the lipoyl domain of the E2 subunit in the human alpha-ketoglutarate dehydrogenase complex

Method: SOLUTION NMR Dmax: 49.3 Å Quality: REASONABLE

SAXS Profile

SAXS profile for 9rca

P(r) Distribution

P(r) distribution for 9rca

1. Structure Basics

entry_id9rca
deposition_date2025-05-27
last_revision2026-06-10
titleSolution NMR structure of the lipoyl domain of the E2 subunit in the human alpha-ketoglutarate dehydrogenase complex
keywords;Lipoyl domain; alpha-ketoglutarate dehydrogenase complex; 2-oxoglutarate dehydrogenase complex; dihydrolipoamide succinyltransferase; E2 subunit, TRANSFERASE ;; TRANSFERASE
methodSOLUTION NMR

Download Data

2. SAXS Parameters (CRYSOL)

rg_guinier13.25
rg_electron12.78
i0108937000.00
molecular_weight86416.0 kDa
excluded_volume107820 ų
envelope_volume15545 ų
shell_volume10030 ų
envelope_diameter50.0
shell_rg18.97
envelope_rg14.50
shape_rg12.76
total_rg13.05
total_atoms12070
n_residues840
n_harmonics20
q_range— – 0.5000 −1
n_points101
shell_typedirectional
solvent_density0.3340 e/ų
contrast_shell0.0300 e/ų
crysol_version4.1.3

3. P(r) Analysis (GNOM)

dmax49.3
rg_real13.30
rg_real_error0.42
i0_real1.0890e+08
i0_real_error1.3110e+06
rg_reciprocal13.30
i0_reciprocal108900000.0000
total_estimate0.7167
solution_quality REASONABLE a REASONABLE solution
n_peaks2
r_peak_primary13.7
skewness0.435
kurtosis-0.172
angular_range— – 0.5000 −1
current_alpha0.0000
highest_alpha197000.0000
n_real_points80
gnom_version4.1.3
quality_criteria AN1: 0.000; Oscil: 0.517; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.761; Smooth: 0.000

4. Crystallography & Experiment

5. Entities & Polymer Info (1)

6. Citations (1)

7. Files & Curves (10)