REMARK 265 REMARK 265 EXPERIMENT TYPE : X-RAY SOLUTION SCATTERING REMARK 265 DATA ACQUISITION REMARK 265 RADIATION SOURCE : BENDING MAGNET REMARK 265 SYNCHROTRON (Y/N) : Y REMARK 265 BEAMLINE : REMARK 265 REMARK 265 DATA REDUCTION SOFTWARE : SCATTER (v ) REMARK 265 SOFTWARE AUTHOR : RP RAMBO REMARK 265 DATA ANALYSIS SOFTWARE : SCATTER (v ) REMARK 265 SOFTWARE AUTHOR : RP RAMBO REMARK 265 REMARK 265 EXPERIMENTAL INFO REMARK 265 INFORMATION CAN BE ADDED BY DUPLICATING THE NOTE LINE BELOW REMARK 265 REMARK 265 NOTE : REMARK 265 REMARK 265 EXPERIMENTAL DETAILS REMARK 265 BUFFER COMPOSITION REMARK 265 TEMPERATURE (KELVIN) : 298 REMARK 265 PH : X.X REMARK 265 SAMPLE BUFFER : XXX mM HEPES REMARK 265 SAMPLE BUFFER : XXX mM KCl REMARK 265 SAMPLE BUFFER : X mM TCEP REMARK 265 SAMPLE BUFFER : X mM KNitrate REMARK 265 REMARK 265 DATASET MAY CONTAIN FEWER POINTS THAN ORIGINAL DATA : Av5_15153_Sub_15151_GraTdelta92diges_HPLCSample_00007AzInt_Px_frame_16-1091 REMARK 265 REFINEMENT OR MANUAL TRIMMING OF SCATTERING CURVE MAY PRODUCE FEWER DATA. REMARK 265 PERCENT KEPT : 96.004 REMARK 265 REMARK 265 SAXS DERIVED PARAMETERS REMARK 265 REMARK 265 RECI REFERS TO RECIPROCAL SPACE VALUES DERIVED FROM GUINIER ANALYSIS REMARK 265 REAL REFERS TO REAL SPACE VALUES DERIVED FROM P(R)-DISTRIBUTION REMARK 265 REAL I(0) : 1.335E-02 REMARK 265 REAL I(0) ERROR (+/-) : 4.977E-04 REMARK 265 RECI I(0) : 1.438E-02 REMARK 265 RECI I(0) ERROR (+/-) : 1.614E-05 REMARK 265 PERCENT DIFFERENCE : 7.414 REMARK 265 REAL Rg : 1.491E+01 (Angstroms) REMARK 265 REAL Rg ERROR (+/-) : 1.363E+00 (Angstroms) REMARK 265 RECI Rg : 1.539E+01 (Angstroms) REMARK 265 RECI Rg ERROR (+/-) : 7.710E-02 REMARK 265 PERCENT DIFFERENCE : 2.108 REMARK 265 VOLUME : 17615282 (Angstroms^3) REMARK 265 Porod Volume Mass (d 1.11) : 11354428 (Angstroms^3) RECI REMARK 265 Porod Volume Mass (d 1.11) : 10542717 (Angstroms^3) REAL REMARK 265 Porod Volume Mass (d 1.37) : 11672777 (Angstroms^3) RECI REMARK 265 Porod Volume Mass (d 1.37) : 10838307 (Angstroms^3) REAL REMARK 265 POROD EXPONENT (P_E) : 0.079 REMARK 265 REAL : 19.231 (Angstroms) REMARK 265 DMAX : 69 (Angstroms) REMARK 265 RESOLUTION LIMIT QMAX : 6.641562E-01 (Angstroms^-1) REMARK 265 RESOLUTION LIMIT (d-SPACING): 9.5 (Angstroms) REMARK 265 RESOLUTION LIMIT BIN WIDTH : 4.7 (Angstroms) REMARK 265 COLUMNS : q, I_OBS(q), error, I_CALC(q) REMARK 265 q : defined in inverse Angstroms 1.45956E-02 1.43606E-02 9.20191E-05 1.50366E-02 1.52038E-02 1.43313E-02 8.92719E-05 1.49426E-02 1.58119E-02 1.42924E-02 8.28853E-05 1.48538E-02 1.64201E-02 1.41915E-02 8.51332E-05 1.47696E-02 1.70282E-02 1.42070E-02 7.89232E-05 1.46894E-02 1.76364E-02 1.40426E-02 8.01362E-05 1.46127E-02 1.82445E-02 1.40719E-02 7.62277E-05 1.45392E-02 1.88527E-02 1.39906E-02 7.54321E-05 1.44684E-02 1.94608E-02 1.40603E-02 7.70663E-05 1.44000E-02 2.00690E-02 1.41575E-02 7.15176E-05 1.43338E-02 2.06771E-02 1.39337E-02 7.09686E-05 1.42695E-02 2.12852E-02 1.39933E-02 6.89889E-05 1.42070E-02 2.18934E-02 1.37958E-02 6.93868E-05 1.41459E-02 2.25015E-02 1.38759E-02 6.90182E-05 1.40861E-02 2.31097E-02 1.39054E-02 6.61211E-05 1.40276E-02 2.37178E-02 1.37260E-02 6.59266E-05 1.39701E-02 2.43260E-02 1.38820E-02 6.35449E-05 1.39135E-02 2.49341E-02 1.38080E-02 6.45134E-05 1.38578E-02 2.55422E-02 1.36889E-02 6.23949E-05 1.38027E-02 2.61504E-02 1.37217E-02 6.15261E-05 1.37483E-02 2.67585E-02 1.36516E-02 6.19929E-05 1.36945E-02 2.73667E-02 1.35383E-02 5.99458E-05 1.36411E-02 2.79748E-02 1.35059E-02 6.04811E-05 1.35882E-02 2.85829E-02 1.34897E-02 5.67399E-05 1.35356E-02 2.91911E-02 1.33563E-02 5.86629E-05 1.34833E-02 2.97992E-02 1.33369E-02 5.83159E-05 1.34312E-02 3.04074E-02 1.34190E-02 5.65950E-05 1.33794E-02 3.10155E-02 1.33818E-02 5.61820E-05 1.33277E-02 3.16236E-02 1.32941E-02 5.43647E-05 1.32761E-02 3.22318E-02 1.31454E-02 5.55549E-05 1.32247E-02 3.28399E-02 1.31746E-02 5.46894E-05 1.31733E-02 3.34480E-02 1.31088E-02 5.39280E-05 1.31219E-02 3.40562E-02 1.31912E-02 5.60102E-05 1.30706E-02 3.46643E-02 1.30091E-02 5.45743E-05 1.30192E-02 3.52724E-02 1.29751E-02 5.66552E-05 1.29678E-02 3.58805E-02 1.28484E-02 5.42776E-05 1.29163E-02 3.64887E-02 1.29186E-02 5.43360E-05 1.28648E-02 3.70968E-02 1.29685E-02 5.66589E-05 1.28132E-02 3.77049E-02 1.28611E-02 5.40737E-05 1.27615E-02 3.83131E-02 1.28786E-02 5.61384E-05 1.27096E-02 3.89212E-02 1.26815E-02 5.27396E-05 1.26577E-02 3.95293E-02 1.26786E-02 5.44661E-05 1.26055E-02 4.01374E-02 1.26861E-02 5.48828E-05 1.25533E-02 4.07455E-02 1.25654E-02 5.31084E-05 1.25009E-02 4.13537E-02 1.24024E-02 5.40799E-05 1.24483E-02 4.19618E-02 1.23909E-02 5.22813E-05 1.23955E-02 4.25699E-02 1.23282E-02 5.38259E-05 1.23426E-02 4.31780E-02 1.24183E-02 5.32427E-05 1.22895E-02 4.37862E-02 1.22720E-02 5.13367E-05 1.22362E-02 4.43943E-02 1.23185E-02 5.30337E-05 1.21827E-02 4.50024E-02 1.22912E-02 5.14314E-05 1.21290E-02 4.56105E-02 1.21715E-02 5.27775E-05 1.20752E-02 4.62186E-02 1.20465E-02 5.09505E-05 1.20211E-02 4.68267E-02 1.21216E-02 5.08787E-05 1.19668E-02 4.74348E-02 1.19229E-02 5.16078E-05 1.19123E-02 4.80430E-02 1.19159E-02 5.07153E-05 1.18576E-02 4.86511E-02 1.19329E-02 5.08158E-05 1.18027E-02 4.92592E-02 1.18176E-02 4.98472E-05 1.17476E-02 4.98673E-02 1.17048E-02 5.02934E-05 1.16923E-02 5.04754E-02 1.16930E-02 5.01125E-05 1.16368E-02 5.10835E-02 1.16296E-02 4.96415E-05 1.15811E-02 5.16916E-02 1.16622E-02 4.91805E-05 1.15252E-02 5.22997E-02 1.15621E-02 4.90838E-05 1.14691E-02 5.29078E-02 1.13643E-02 4.94535E-05 1.14128E-02 5.35159E-02 1.14568E-02 4.89567E-05 1.13563E-02 5.41240E-02 1.13035E-02 4.79416E-05 1.12997E-02 5.47321E-02 1.13299E-02 4.79621E-05 1.12428E-02 5.53402E-02 1.12572E-02 4.80214E-05 1.11857E-02 5.59483E-02 1.11399E-02 4.82498E-05 1.11285E-02 5.65564E-02 1.10898E-02 4.71664E-05 1.10711E-02 5.71645E-02 1.10077E-02 4.74318E-05 1.10135E-02 5.77726E-02 1.09567E-02 4.68554E-05 1.09557E-02 5.83806E-02 1.09795E-02 4.73166E-05 1.08978E-02 5.89887E-02 1.09507E-02 4.66822E-05 1.08397E-02 5.95968E-02 1.08106E-02 4.57379E-05 1.07814E-02 6.02049E-02 1.06925E-02 4.69006E-05 1.07230E-02 6.08130E-02 1.06628E-02 4.60114E-05 1.06645E-02 6.14211E-02 1.05137E-02 4.59654E-05 1.06057E-02 6.20292E-02 1.05979E-02 4.54362E-05 1.05469E-02 6.26373E-02 1.05609E-02 4.51694E-05 1.04879E-02 6.32453E-02 1.05180E-02 4.60430E-05 1.04288E-02 6.38534E-02 1.04150E-02 4.46169E-05 1.03695E-02 6.44615E-02 1.02528E-02 4.47474E-05 1.03101E-02 6.50696E-02 1.03153E-02 4.47439E-05 1.02506E-02 6.56776E-02 1.02117E-02 4.42238E-05 1.01910E-02 6.62857E-02 1.01010E-02 4.49476E-05 1.01313E-02 6.68938E-02 1.00927E-02 4.31577E-05 1.00715E-02 6.75019E-02 1.00815E-02 4.41159E-05 1.00115E-02 6.81099E-02 9.88554E-03 4.36774E-05 9.95150E-03 6.87180E-02 9.87462E-03 4.36446E-05 9.89139E-03 6.93260E-02 9.88102E-03 4.35394E-05 9.83120E-03 6.99341E-02 9.78585E-03 4.21980E-05 9.77093E-03 7.05422E-02 9.75574E-03 4.33816E-05 9.71059E-03 7.11502E-02 9.67249E-03 4.28063E-05 9.65017E-03 7.17583E-02 9.56150E-03 4.26482E-05 9.58970E-03 7.23663E-02 9.51302E-03 4.22486E-05 9.52917E-03 7.29744E-02 9.50429E-03 4.20446E-05 9.46859E-03 7.35824E-02 9.46463E-03 4.24384E-05 9.40797E-03 7.41905E-02 9.32070E-03 4.17640E-05 9.34730E-03 7.47986E-02 9.23991E-03 4.13952E-05 9.28660E-03 7.54066E-02 9.19814E-03 4.14637E-05 9.22587E-03 7.60147E-02 9.19623E-03 4.14824E-05 9.16511E-03 7.66227E-02 9.10037E-03 4.17859E-05 9.10434E-03 7.72307E-02 9.03900E-03 4.04745E-05 9.04355E-03 7.78388E-02 8.98758E-03 4.07524E-05 8.98276E-03 7.84468E-02 8.86390E-03 4.07343E-05 8.92196E-03 7.90549E-02 8.86037E-03 4.07820E-05 8.86117E-03 7.96629E-02 8.80321E-03 4.03925E-05 8.80039E-03 8.02709E-02 8.74217E-03 3.96553E-05 8.73961E-03 8.08790E-02 8.71211E-03 4.01879E-05 8.67886E-03 8.14870E-02 8.58441E-03 3.97520E-05 8.61813E-03 8.20950E-02 8.60257E-03 3.99953E-05 8.55743E-03 8.27031E-02 8.47740E-03 3.96032E-05 8.49677E-03 8.33111E-02 8.49385E-03 3.94406E-05 8.43614E-03 8.39191E-02 8.34737E-03 3.94559E-05 8.37556E-03 8.45271E-02 8.31367E-03 3.87625E-05 8.31503E-03 8.51351E-02 8.16915E-03 3.87448E-05 8.25456E-03 8.57432E-02 8.17799E-03 3.87915E-05 8.19414E-03 8.63512E-02 8.08006E-03 3.89833E-05 8.13379E-03 8.69592E-02 7.97764E-03 3.89474E-05 8.07351E-03 8.75672E-02 7.90473E-03 3.79242E-05 8.01331E-03 8.81752E-02 7.97381E-03 3.82147E-05 7.95318E-03 8.87832E-02 7.91001E-03 3.77990E-05 7.89314E-03 8.93912E-02 7.79246E-03 3.83322E-05 7.83319E-03 8.99992E-02 7.81191E-03 3.78071E-05 7.77334E-03 9.06072E-02 7.60151E-03 3.75040E-05 7.71358E-03 9.12152E-02 7.61203E-03 3.78325E-05 7.65392E-03 9.18232E-02 7.62410E-03 3.72442E-05 7.59438E-03 9.24312E-02 7.50509E-03 3.73099E-05 7.53495E-03 9.30392E-02 7.41701E-03 3.68702E-05 7.47563E-03 9.36472E-02 7.38044E-03 3.70233E-05 7.41644E-03 9.42552E-02 7.27781E-03 3.74229E-05 7.35737E-03 9.48632E-02 7.25448E-03 3.62202E-05 7.29843E-03 9.54712E-02 7.20043E-03 3.75149E-05 7.23963E-03 9.60792E-02 7.10968E-03 3.77864E-05 7.18096E-03 9.66871E-02 7.10875E-03 3.83921E-05 7.12244E-03 9.72951E-02 6.98918E-03 3.88254E-05 7.06406E-03 9.79031E-02 6.96162E-03 3.79185E-05 7.00584E-03 9.85111E-02 7.04579E-03 3.88700E-05 6.94777E-03 9.91190E-02 6.95585E-03 3.82228E-05 6.88986E-03 9.97270E-02 6.81394E-03 3.87555E-05 6.83211E-03 1.00335E-01 6.74796E-03 3.81808E-05 6.77453E-03 1.00943E-01 6.74123E-03 3.81287E-05 6.71713E-03 1.01551E-01 6.56204E-03 3.87445E-05 6.65989E-03 1.02159E-01 6.61267E-03 3.82497E-05 6.60283E-03 1.02767E-01 6.54898E-03 3.82823E-05 6.54596E-03 1.03375E-01 6.49700E-03 3.78573E-05 6.48926E-03 1.03983E-01 6.40433E-03 3.81502E-05 6.43276E-03 1.04591E-01 6.38208E-03 3.86434E-05 6.37644E-03 1.05199E-01 6.28404E-03 3.76893E-05 6.32033E-03 1.05807E-01 6.23323E-03 3.80467E-05 6.26441E-03 1.06414E-01 6.22184E-03 3.78872E-05 6.20869E-03 1.07023E-01 6.17590E-03 3.78821E-05 6.15318E-03 1.07630E-01 6.12464E-03 3.82000E-05 6.09787E-03 1.08238E-01 6.00200E-03 3.73452E-05 6.04278E-03 1.08846E-01 6.05573E-03 3.79984E-05 5.98790E-03 1.09454E-01 5.94422E-03 3.75101E-05 5.93323E-03 1.10062E-01 5.91945E-03 3.77879E-05 5.87879E-03 1.10670E-01 5.75565E-03 3.72117E-05 5.82456E-03 1.11278E-01 5.74274E-03 3.73669E-05 5.77056E-03 1.11886E-01 5.77120E-03 3.76673E-05 5.71680E-03 1.12494E-01 5.69331E-03 3.71250E-05 5.66326E-03 1.13102E-01 5.60711E-03 3.73614E-05 5.60994E-03 1.13710E-01 5.52267E-03 3.69173E-05 5.55687E-03 1.14318E-01 5.57786E-03 3.70987E-05 5.50404E-03 1.14925E-01 5.40555E-03 3.71479E-05 5.45144E-03 1.15533E-01 5.42374E-03 3.68509E-05 5.39909E-03 1.16141E-01 5.39094E-03 3.67761E-05 5.34698E-03 1.16749E-01 5.26873E-03 3.68139E-05 5.29512E-03 1.17357E-01 5.25176E-03 3.70827E-05 5.24351E-03 1.17965E-01 5.15894E-03 3.66016E-05 5.19214E-03 1.18573E-01 5.14893E-03 3.64201E-05 5.14103E-03 1.19181E-01 5.13943E-03 3.67514E-05 5.09018E-03 1.19789E-01 5.08184E-03 3.61257E-05 5.03958E-03 1.20397E-01 4.99769E-03 3.69301E-05 4.98924E-03 1.21004E-01 4.99682E-03 3.58658E-05 4.93917E-03 1.21612E-01 4.87033E-03 3.63512E-05 4.88935E-03 1.22220E-01 4.85136E-03 3.63994E-05 4.83980E-03 1.22828E-01 4.77036E-03 3.68937E-05 4.79051E-03 1.23436E-01 4.72723E-03 3.80754E-05 4.74149E-03 1.24044E-01 4.67316E-03 3.78432E-05 4.69275E-03 1.24652E-01 4.68845E-03 3.88494E-05 4.64426E-03 1.25260E-01 4.63140E-03 3.90486E-05 4.59605E-03 1.25867E-01 4.58190E-03 3.91470E-05 4.54812E-03 1.26475E-01 4.44996E-03 3.98390E-05 4.50046E-03 1.27083E-01 4.48395E-03 3.93364E-05 4.45308E-03 1.27691E-01 4.42658E-03 4.06020E-05 4.40597E-03 1.28299E-01 4.36249E-03 4.02053E-05 4.35914E-03 1.28907E-01 4.38637E-03 4.03965E-05 4.31259E-03 1.29515E-01 4.27833E-03 4.11006E-05 4.26633E-03 1.30122E-01 4.19091E-03 4.03434E-05 4.22034E-03 1.30730E-01 4.18610E-03 4.20401E-05 4.17463E-03 1.31338E-01 4.19716E-03 4.05345E-05 4.12922E-03 1.31946E-01 4.06744E-03 4.17195E-05 4.08408E-03 1.32554E-01 4.00647E-03 4.21988E-05 4.03923E-03 1.33161E-01 4.00557E-03 4.16756E-05 3.99467E-03 1.33769E-01 3.93084E-03 4.25322E-05 3.95039E-03 1.34377E-01 3.85154E-03 3.99519E-05 3.90640E-03 1.34985E-01 3.90289E-03 3.99773E-05 3.86270E-03 1.35593E-01 3.81557E-03 3.96232E-05 3.81929E-03 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