data_SASDAG4_MAIN # _sas_result.id 79 _sas_result.SASBDB_code SASDAG4 _sas_result.experimental_MW 100.000 _sas_result.experimental_MW_error . _sas_result.MW_standard 100.000 _sas_result.MW_standard_error . _sas_result.MW_Porod . _sas_result.MW_Porod_error . _sas_result.I0_from_PR . _sas_result.I0_from_PR_error . _sas_result.I0_from_Guinier 121.0000000000 _sas_result.I0_from_Guinier_error . _sas_result.Rg_from_PR 4.600 _sas_result.Rg_from_PR_error . _sas_result.Rg_from_Guinier 4.600 _sas_result.Rg_from_Guinier_error . _sas_result.D_max 15.00 _sas_result.Porod_volume . _sas_result.Porod_volume_error . _sas_result.estimated_volume 330.00 _sas_result.estimated_volume_error . _sas_result.estimated_volume_method . _sas_result.Guinier_point_min 18 _sas_result.Guinier_point_max 60 _sas_result.type_of_curve merged _sas_result.standard . _sas_result.Dmax_error . _sas_result.comments . # _sas_scan.title HumMFE-2 _sas_scan.detc_id 1 _sas_scan.id 79 _sas_scan.measurement_date 2011-03-22 _sas_scan.storage_temperature 15.0 _sas_scan.cell_temperature 15.0 _sas_scan.exposure_time 15.000 _sas_scan.number_of_frames 8 _sas_scan.unit 1/nm _sas_scan.qmin 0.0671 _sas_scan.qmax 4.7168 _sas_scan.sample_id 127 _sas_scan.result_id 79 _sas_scan.beam_id 1 # _sas_beam.id 1 _sas_beam.instrument_name "DORIS III X33" _sas_beam.instrument_city Hamburg _sas_beam.instrument_country Germany _sas_beam.shape 0.60 _sas_beam.type_of_source "X-ray synchrotron" _sas_beam.radiation_wavelength 0.150000 _sas_beam.dist_spec_to_detc 2.70000 # _sas_detc.id 1 _sas_detc.name "Pilatus 1M-W" _sas_detc.type . _sas_detc.pixsize_x 0.172 # _sas_sample.id 127 _sas_sample.name HsMfe2 _sas_sample.ext_coefficient . _sas_sample.contrast . _sas_sample.specific_vol . _sas_sample.purity_method . _sas_sample.dry_vol . _sas_sample.sample_MW . _sas_sample.specimen_concentration 1.30-5.50 _sas_sample.concentration_method . _sas_sample.entity_id 149 # _sas_buffer.id 58 _sas_buffer.name "Sodium Phosphate" _sas_buffer.concentration 20.00 _sas_buffer.unit mM _sas_buffer.pK . _sas_buffer.pH 7.500 _sas_buffer.comment . _sas_buffer.composition ;200 NaCl 5% (v/v) Glycerol 1mM Na2EDTA 1mMNaN3 ; _sas_buffer.sample_id 127 # _entity.id 149 _entity.type protein _entity.pdbx_description "Peroxisomal multifunctional enzyme type 2" _entity.formula_weight 79.700 _entity.pdbx_number_of_molecules 2 # _entity_name_com.entity_id 149 _entity_name_com.name HsMfe2 # _entity_poly.entity_id 149 _entity_poly.pdbx_seq_one_letter_code ;MGSPLRFDGRVVLVTGAGAGLGRAYALAFAERGALVVVNDLGGDFKGVGKGSLAADKVVE EIRRRGGKAVANYDSVEEGEKVVKTALDAFGRIDVVVNNAGILRDRSFARISDEDWDIIH RVHLRGSFQVTRAAWEHMKKQKYGRIIMTSSASGIYGNFGQANYSAAKLGLLGLANSLAI EGRKSNIHCNTIAPNAGSRMTQTVMPEDLVEALKPEYVAPLVLWLCHESCEENGGLFEVG AGWIGKLRWERTLGAIVRQKNHPMTPEAVKANWKKICDFENASKPQSIQESTGSIIEVLS KIDSEGGVSANHTSRATSTATSGFAGAIGQKLPPFSYAYTELEAIMYALGVGASIKDPKD LKFIYEGSSDFSCLPTFGVIIGQKSMMGGGLAEIPGLSINFAKVLHGEQYLELYKPLPRA GKLKCEAVVADVLDKGSGVVIIMDVYSYSEKELICHNQFSLFLVGSGGFGGKRTSDKVKV AVAIPNRPPDAVLTDTTSLNQAALYRLSGDWNPLHIDPNFASLAGFDKPILHGLCTFGFS ARRVLQQFADNDVSRFKAIKARFAKPVYPGQTLQTEMWKEGNRIHFQTKVQETGDIVISN AYVDLAPTSGTSAKTPSEGGKLQSTFVFEEIGRRLKDIGPEVVKKVNAVFEWHITKGGNI GAKWTIDLKSGSGKVYQGPAKGAADTTIILSDEDFMEVVLGKLDPQKAFFSGRLKARGNI MLSQKLQMILKDYAKL ; # _entity_src_gen.entity_id 149 _entity_src_gen.gene_src_common_name "Homo sapiens" # _struct_ref.id 1 _struct_ref.entity_id 149 _struct_ref.db_name UniProt _struct_ref.db_code P51659 _struct_ref.details http://www.uniprot.org/uniprot/P51659 # _citation.id 5 _citation.title "Quaternary structure of human, Drosophila melanogaster and Caenorhabditis elegans MFE-2 in solution from synchrotron small-angle X-ray scattering." _citation.year "2013 Feb 14" _citation.pdbx_database_id_DOI 10.1016/j.febslet.2012.12.014 _citation.pdbx_database_id_PubMed 23313254 _citation.journal_abbrev "FEBS Lett" _citation.journal_volume 587 _citation.journal_issue 4 _citation.page_first 305 _citation.page_last 310 # loop_ _citation_author.citation_id _citation_author.ordinal _citation_author.name 5 1 "Mehtälä ML" 5 2 "Haataja TJ" 5 3 "Blanchet CE" 5 4 "Hiltunen JK" 5 5 "Svergun DI" # _pdbx_contact_author.id 11 _pdbx_contact_author.name_first Clement _pdbx_contact_author.name_last Blanchet _pdbx_contact_author.role . _pdbx_contact_author.address_1 EMBL-Hamburg _pdbx_contact_author.address_2 "European Molecular Biology Laboratory (EMBL) - Hamburg outstation" _pdbx_contact_author.address_3 "Notkestraße 85, Geb. 25A, 22607 Hamburg, Deutschland, Germany" # loop_ _sas_scan_intensity.id _sas_scan_intensity.momentum_transfer _sas_scan_intensity.intensity _sas_scan_intensity.intensity_su_counting _sas_scan_intensity.scan_id 1 6.710100E-02 1.290238E+02 3.498732E+01 79 2 6.983610E-02 1.265754E+02 1.297410E+01 79 3 7.257120E-02 1.173399E+02 1.070358E+01 79 4 7.530620E-02 1.347367E+02 9.309028E+00 79 5 7.804130E-02 1.342545E+02 8.136590E+00 79 6 8.077640E-02 1.236397E+02 7.156902E+00 79 7 8.351150E-02 1.242702E+02 6.350945E+00 79 8 8.624660E-02 1.206853E+02 5.596882E+00 79 9 8.898170E-02 1.171750E+02 4.971724E+00 79 10 9.171680E-02 1.193035E+02 4.489614E+00 79 11 9.445180E-02 1.157936E+02 4.064994E+00 79 12 9.718690E-02 1.180486E+02 3.653005E+00 79 13 9.992200E-02 1.159753E+02 3.333332E+00 79 14 1.026570E-01 1.136686E+02 3.028850E+00 79 15 1.053920E-01 1.133709E+02 2.750591E+00 79 16 1.081270E-01 1.129822E+02 2.520314E+00 79 17 1.108620E-01 1.120313E+02 2.306479E+00 79 18 1.135970E-01 1.140800E+02 2.144339E+00 79 19 1.163330E-01 1.110619E+02 1.993769E+00 79 20 1.190680E-01 1.095960E+02 1.814325E+00 79 21 1.218030E-01 1.096124E+02 1.708736E+00 79 22 1.245380E-01 1.088163E+02 1.579164E+00 79 23 1.272730E-01 1.086493E+02 1.489495E+00 79 24 1.300080E-01 1.080909E+02 1.394520E+00 79 25 1.327430E-01 1.074740E+02 1.290280E+00 79 26 1.354780E-01 1.060426E+02 1.233389E+00 79 27 1.382130E-01 1.053151E+02 1.148880E+00 79 28 1.409480E-01 1.050070E+02 1.090427E+00 79 29 1.436830E-01 1.039033E+02 1.035854E+00 79 30 1.464180E-01 1.034140E+02 9.755805E-01 79 31 1.491540E-01 1.021002E+02 9.462190E-01 79 32 1.518890E-01 1.022753E+02 8.930203E-01 79 33 1.546240E-01 1.025690E+02 8.430950E-01 79 34 1.573590E-01 1.015273E+02 8.089465E-01 79 35 1.600940E-01 1.008023E+02 7.792793E-01 79 36 1.628290E-01 9.988845E+01 7.620349E-01 79 37 1.655640E-01 9.976028E+01 7.174836E-01 79 38 1.682990E-01 9.823411E+01 6.908754E-01 79 39 1.710340E-01 9.841981E+01 6.679442E-01 79 40 1.737690E-01 9.666957E+01 6.476244E-01 79 41 1.765040E-01 9.678503E+01 6.319937E-01 79 42 1.792400E-01 9.652623E+01 6.001483E-01 79 43 1.819750E-01 9.579443E+01 5.916247E-01 79 44 1.847100E-01 9.553677E+01 5.713439E-01 79 45 1.874450E-01 9.401548E+01 5.543179E-01 79 46 1.901800E-01 9.307227E+01 5.313189E-01 79 47 1.929150E-01 9.245448E+01 5.210487E-01 79 48 1.956500E-01 9.176735E+01 5.142634E-01 79 49 1.983850E-01 9.133929E+01 4.958854E-01 79 50 2.011200E-01 9.062626E+01 4.816467E-01 79 51 2.038550E-01 8.972394E+01 4.721414E-01 79 52 2.065900E-01 8.915377E+01 4.601012E-01 79 53 2.093250E-01 8.820208E+01 4.543605E-01 79 54 2.120610E-01 8.776573E+01 4.412905E-01 79 55 2.147960E-01 8.661576E+01 4.322552E-01 79 56 2.175310E-01 8.628915E+01 4.239837E-01 79 57 2.202660E-01 8.592568E+01 4.177074E-01 79 58 2.230010E-01 8.521166E+01 4.081574E-01 79 59 2.257360E-01 8.488362E+01 4.023835E-01 79 60 2.284710E-01 8.409796E+01 3.984102E-01 79 61 2.312060E-01 8.331657E+01 3.896546E-01 79 62 2.339410E-01 8.297674E+01 3.857525E-01 79 63 2.366760E-01 8.208099E+01 3.758025E-01 79 64 2.394110E-01 8.120442E+01 3.736893E-01 79 65 2.421460E-01 8.078641E+01 3.692951E-01 79 66 2.448820E-01 8.035938E+01 3.620518E-01 79 67 2.476170E-01 7.921449E+01 3.584030E-01 79 68 2.503520E-01 7.886540E+01 3.530749E-01 79 69 2.530870E-01 7.770329E+01 3.502754E-01 79 70 2.558220E-01 7.714068E+01 3.436311E-01 79 71 2.585570E-01 7.652062E+01 3.390561E-01 79 72 2.612920E-01 7.591626E+01 3.373167E-01 79 73 2.640270E-01 7.525301E+01 3.326325E-01 79 74 2.667620E-01 7.453663E+01 3.290284E-01 79 75 2.694970E-01 7.341848E+01 3.215740E-01 79 76 2.722320E-01 7.290009E+01 3.179955E-01 79 77 2.749680E-01 7.214942E+01 3.171326E-01 79 78 2.777030E-01 7.150577E+01 3.131376E-01 79 79 2.804380E-01 7.097058E+01 3.112648E-01 79 80 2.831730E-01 7.000115E+01 3.017964E-01 79 81 2.859080E-01 6.919610E+01 3.013575E-01 79 82 2.886430E-01 6.852669E+01 2.991964E-01 79 83 2.913780E-01 6.771837E+01 2.922147E-01 79 84 2.941130E-01 6.696917E+01 2.919465E-01 79 85 2.968480E-01 6.629144E+01 2.875325E-01 79 86 2.995830E-01 6.549107E+01 2.885479E-01 79 87 3.023180E-01 6.487882E+01 2.858309E-01 79 88 3.050530E-01 6.391469E+01 2.804756E-01 79 89 3.077890E-01 6.284386E+01 2.789230E-01 79 90 3.105240E-01 6.234096E+01 2.748610E-01 79 91 3.132590E-01 6.199828E+01 2.757315E-01 79 92 3.159940E-01 6.139603E+01 2.722117E-01 79 93 3.187290E-01 6.060044E+01 2.690357E-01 79 94 3.214640E-01 5.975137E+01 2.706902E-01 79 95 3.241990E-01 5.915237E+01 2.645239E-01 79 96 3.269340E-01 5.818127E+01 2.634575E-01 79 97 3.296690E-01 5.759695E+01 2.597870E-01 79 98 3.324040E-01 5.696163E+01 2.569516E-01 79 99 3.351390E-01 5.645655E+01 2.583588E-01 79 100 3.378750E-01 5.564745E+01 2.541760E-01 79 101 3.406100E-01 5.510726E+01 2.513842E-01 79 102 3.433450E-01 5.443090E+01 2.496325E-01 79 103 3.460800E-01 5.341803E+01 2.466786E-01 79 104 3.488150E-01 5.289216E+01 2.456208E-01 79 105 3.515500E-01 5.234600E+01 2.428639E-01 79 106 3.542850E-01 5.174725E+01 2.419636E-01 79 107 3.570200E-01 5.104513E+01 2.393650E-01 79 108 3.597550E-01 5.048045E+01 2.377197E-01 79 109 3.624900E-01 4.979116E+01 2.342272E-01 79 110 3.652250E-01 4.919220E+01 2.328009E-01 79 111 3.679600E-01 4.840712E+01 2.322154E-01 79 112 3.706960E-01 4.825468E+01 2.306900E-01 79 113 3.734310E-01 4.759191E+01 2.272120E-01 79 114 3.761660E-01 4.703532E+01 2.234265E-01 79 115 3.789010E-01 4.627434E+01 2.242410E-01 79 116 3.816360E-01 4.565208E+01 2.214190E-01 79 117 3.843710E-01 4.505288E+01 2.208591E-01 79 118 3.871060E-01 4.450483E+01 2.171867E-01 79 119 3.898410E-01 4.419054E+01 2.155833E-01 79 120 3.925760E-01 4.349617E+01 2.156246E-01 79 121 3.953110E-01 4.283088E+01 2.118081E-01 79 122 3.980460E-01 4.229448E+01 2.107392E-01 79 123 4.007810E-01 4.180044E+01 2.091825E-01 79 124 4.035170E-01 4.135989E+01 2.062746E-01 79 125 4.062520E-01 4.090351E+01 2.079882E-01 79 126 4.089870E-01 4.032843E+01 2.021956E-01 79 127 4.117220E-01 4.011242E+01 2.021234E-01 79 128 4.144570E-01 3.918775E+01 2.005651E-01 79 129 4.171920E-01 3.876057E+01 1.984632E-01 79 130 4.199270E-01 3.828807E+01 1.980956E-01 79 131 4.226620E-01 3.762024E+01 1.942556E-01 79 132 4.253970E-01 3.722252E+01 1.939341E-01 79 133 4.281320E-01 3.652845E+01 1.916936E-01 79 134 4.308670E-01 3.624687E+01 1.898383E-01 79 135 4.336030E-01 3.581680E+01 1.891856E-01 79 136 4.363380E-01 3.525104E+01 1.865851E-01 79 137 4.390730E-01 3.503400E+01 1.876688E-01 79 138 4.418080E-01 3.424912E+01 1.832898E-01 79 139 4.445430E-01 3.376510E+01 1.812353E-01 79 140 4.472780E-01 3.328925E+01 1.820855E-01 79 141 4.500130E-01 3.280405E+01 1.784078E-01 79 142 4.527480E-01 3.243172E+01 1.786249E-01 79 143 4.554830E-01 3.189390E+01 1.757531E-01 79 144 4.582180E-01 3.153906E+01 1.740238E-01 79 145 4.609530E-01 3.113457E+01 1.738207E-01 79 146 4.636880E-01 3.080816E+01 1.730742E-01 79 147 4.664240E-01 3.010032E+01 1.704086E-01 79 148 4.691590E-01 2.973341E+01 1.690476E-01 79 149 4.718940E-01 2.945437E+01 1.687199E-01 79 150 4.746290E-01 2.913356E+01 1.675895E-01 79 151 4.773640E-01 2.875291E+01 1.664274E-01 79 152 4.800990E-01 2.840517E+01 1.644544E-01 79 153 4.828340E-01 2.799462E+01 1.631939E-01 79 154 4.855690E-01 2.764362E+01 1.630046E-01 79 155 4.883040E-01 2.728865E+01 1.617431E-01 79 156 4.910390E-01 2.678672E+01 1.581772E-01 79 157 4.937740E-01 2.631137E+01 1.578170E-01 79 158 4.965090E-01 2.601960E+01 1.573349E-01 79 159 4.992450E-01 2.565905E+01 1.564331E-01 79 160 5.019800E-01 2.537409E+01 1.544423E-01 79 161 5.047150E-01 2.510608E+01 1.543540E-01 79 162 5.074500E-01 2.481657E+01 1.528703E-01 79 163 5.101850E-01 2.436669E+01 1.519434E-01 79 164 5.129200E-01 2.403345E+01 1.500197E-01 79 165 5.156550E-01 2.370299E+01 1.485147E-01 79 166 5.183900E-01 2.338465E+01 1.487195E-01 79 167 5.211250E-01 2.303535E+01 1.483545E-01 79 168 5.238600E-01 2.270140E+01 1.469733E-01 79 169 5.265950E-01 2.245947E+01 1.448909E-01 79 170 5.293310E-01 2.217627E+01 1.439069E-01 79 171 5.320660E-01 2.180544E+01 1.430366E-01 79 172 5.348010E-01 2.157958E+01 1.426538E-01 79 173 5.375360E-01 2.116369E+01 1.412579E-01 79 174 5.402710E-01 2.085901E+01 1.396744E-01 79 175 5.430060E-01 2.057863E+01 1.393427E-01 79 176 5.457410E-01 2.030249E+01 1.389200E-01 79 177 5.484760E-01 2.009939E+01 1.369291E-01 79 178 5.512110E-01 1.988589E+01 1.373542E-01 79 179 5.539460E-01 1.954169E+01 1.354980E-01 79 180 5.566810E-01 1.934704E+01 1.361811E-01 79 181 5.594160E-01 1.901106E+01 1.333483E-01 79 182 5.621520E-01 1.875554E+01 1.321669E-01 79 183 5.648870E-01 1.855942E+01 1.334558E-01 79 184 5.676220E-01 1.826939E+01 1.311521E-01 79 185 5.703570E-01 1.800194E+01 1.314070E-01 79 186 5.730920E-01 1.768231E+01 1.290801E-01 79 187 5.758270E-01 1.717662E+01 1.260107E-01 79 188 5.785620E-01 1.723633E+01 1.281097E-01 79 189 5.812970E-01 1.697153E+01 1.257887E-01 79 190 5.840320E-01 1.699879E+01 1.289221E-01 79 191 5.867670E-01 1.661912E+01 1.253018E-01 79 192 5.895020E-01 1.644740E+01 1.260784E-01 79 193 5.922380E-01 1.607390E+01 1.256470E-01 79 194 5.949730E-01 1.602083E+01 1.223381E-01 79 195 5.977080E-01 1.587062E+01 1.237103E-01 79 196 6.004430E-01 1.547119E+01 1.221365E-01 79 197 6.031780E-01 1.544443E+01 1.228837E-01 79 198 6.059130E-01 1.524499E+01 1.222378E-01 79 199 6.086480E-01 1.530089E+01 1.225288E-01 79 200 6.113830E-01 1.500409E+01 1.225024E-01 79 201 6.141180E-01 1.473272E+01 1.206479E-01 79 202 6.168530E-01 1.439060E+01 1.179635E-01 79 203 6.195880E-01 1.412896E+01 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