data_SASDEJ5_MAIN # _sas_result.id 1137 _sas_result.SASBDB_code SASDEJ5 _sas_result.experimental_MW 161.000 _sas_result.experimental_MW_error . _sas_result.MW_standard . _sas_result.MW_standard_error . _sas_result.MW_Porod 156.000 _sas_result.MW_Porod_error . _sas_result.I0_from_PR . _sas_result.I0_from_PR_error . _sas_result.I0_from_Guinier 152.0000000000 _sas_result.I0_from_Guinier_error 0.0600000000 _sas_result.Rg_from_PR . _sas_result.Rg_from_PR_error . _sas_result.Rg_from_Guinier 3.610 _sas_result.Rg_from_Guinier_error 0.010 _sas_result.D_max . _sas_result.Porod_volume 250.00 _sas_result.Porod_volume_error . _sas_result.estimated_volume . _sas_result.estimated_volume_error . _sas_result.estimated_volume_method . _sas_result.Guinier_point_min 19 _sas_result.Guinier_point_max 67 _sas_result.type_of_curve single_conc _sas_result.standard . _sas_result.Dmax_error . _sas_result.comments . # _sas_scan.title "AICAR/fumarate-bound human adenylosuccinate lyase (ADSL)" _sas_scan.detc_id 16 _sas_scan.id 1137 _sas_scan.measurement_date 2016-07-24 _sas_scan.storage_temperature 20.0 _sas_scan.cell_temperature 20.0 _sas_scan.exposure_time 1.000 _sas_scan.number_of_frames 10 _sas_scan.unit 1/nm _sas_scan.qmin 0.0467 _sas_scan.qmax 3.8035 _sas_scan.sample_id 1098 _sas_scan.result_id 1137 _sas_scan.beam_id 10 # _sas_beam.id 10 _sas_beam.instrument_name "ESRF BM29" _sas_beam.instrument_city Grenoble _sas_beam.instrument_country France _sas_beam.shape . _sas_beam.type_of_source "X-ray synchrotron" _sas_beam.radiation_wavelength 0.099000 _sas_beam.dist_spec_to_detc 2.86400 # _sas_detc.id 16 _sas_detc.name "Pilatus 1M" _sas_detc.type Dectris _sas_detc.pixsize_x 172.000 # _sas_sample.id 1098 _sas_sample.name "AICAR/fumarate-bound human adenylosuccinate lyase (ADSL)" _sas_sample.ext_coefficient . _sas_sample.contrast . _sas_sample.specific_vol . _sas_sample.purity_method . _sas_sample.dry_vol . _sas_sample.sample_MW . _sas_sample.specimen_concentration 5.00 _sas_sample.concentration_method . _sas_sample.entity_id 1310 # _sas_buffer.id 688 _sas_buffer.name "10 mM HEPES, 100 mM NaCl, 1 mM DTT, 1 mM 5-aminoimidazole-4-carboxamide ribonucleotide (AICAR), 1mM Fumarate" _sas_buffer.concentration . _sas_buffer.unit . _sas_buffer.pK . _sas_buffer.pH 7.500 _sas_buffer.comment . _sas_buffer.composition . _sas_buffer.sample_id 1098 # _entity.id 1310 _entity.type protein _entity.pdbx_description "Adenylosuccinate Lyase" _entity.formula_weight 55.170 _entity.pdbx_number_of_molecules 4 # _entity_name_com.entity_id 1310 _entity_name_com.name ADSL # _entity_poly.entity_id 1310 _entity_poly.pdbx_seq_one_letter_code ;GSHMAAGGDHGSPDSYRSPLASRYASPEMCFVFSDRYKFRTWR QLWLWLAEAEQTLGLPITDEQIQEMKSNLENIDFKMAAEEEKRLRHDVMAHVHTFGHCCP KAAGIIHLGATSCYVGDNTDLIILRNALDLLLPKLARVISRLADFAKERASLPTLGFTHF QPAQLTTVGKRCCLWIQDLCMDLQNLKRVRDDLRFRGVKGTTGTQASFLQLFEGDDHKVE QLDKMVTEKAGFKRAFIITGQTYTRKVDIEVLSVLASLGASVHKICTDIRLLANLKEMEE PFEKQQIGSSAMPYKRNPMRSERCCSLARHLMTLVMDPLQTASVQWFERTLDDSANRRIC LAEAFLTADTILNTLQNISEGLVVYPKVIERRIRQELPFMATENIIMAMVKAGGSRQDCH EKIRVLSQQAASVVKQEGGDNDLIERIQVDAYFSPIHSQLDHLLDPSSFTGRASQQVQRF LEEEVYPLLKPYESVMKVKAELCL ; # _entity_src_gen.entity_id 1310 _entity_src_gen.gene_src_common_name "Homo sapiens" # _struct_ref.id 1 _struct_ref.entity_id 1310 _struct_ref.db_name UniProt _struct_ref.db_code P30566 _struct_ref.details http://www.uniprot.org/uniprot/P30566 # _citation.id 424 _citation.title "Molecular comparison of Neanderthal and Modern Human adenylosuccinate lyase." _citation.year "2018 Dec 20" _citation.pdbx_database_id_DOI 10.1038/s41598-018-36195-5 _citation.pdbx_database_id_PubMed 30573755 _citation.journal_abbrev "Sci Rep" _citation.journal_volume 8 _citation.journal_issue 1 _citation.page_first 18008 # loop_ _citation_author.citation_id _citation_author.ordinal _citation_author.name 424 1 "Van Laer B" 424 2 "Kapp U" 424 3 "Soler-Lopez M" 424 4 "Moczulska K" 424 5 "Pääbo S" 424 6 "Leonard G" # _pdbx_contact_author.id 319 _pdbx_contact_author.name_first Bart _pdbx_contact_author.name_last "Van Laer" _pdbx_contact_author.role . _pdbx_contact_author.address_1 ESRF _pdbx_contact_author.address_2 "European Synchrotron Radiation Facility" _pdbx_contact_author.address_3 "Grenoble, France" # loop_ _sas_scan_intensity.id _sas_scan_intensity.momentum_transfer _sas_scan_intensity.intensity _sas_scan_intensity.intensity_su_counting _sas_scan_intensity.scan_id 1 4.673647E-02 1.483877E+02 9.184383E-01 1137 2 5.146200E-02 1.496176E+02 7.015046E-01 1137 3 5.618753E-02 1.495044E+02 5.769615E-01 1137 4 6.091306E-02 1.486674E+02 4.886527E-01 1137 5 6.563859E-02 1.479464E+02 4.331798E-01 1137 6 7.036412E-02 1.477698E+02 3.899048E-01 1137 7 7.508965E-02 1.476585E+02 3.576484E-01 1137 8 7.981518E-02 1.473996E+02 3.331947E-01 1137 9 8.454071E-02 1.464162E+02 3.128865E-01 1137 10 8.926623E-02 1.460664E+02 2.955500E-01 1137 11 9.399176E-02 1.458964E+02 2.811811E-01 1137 12 9.871729E-02 1.452715E+02 2.691471E-01 1137 13 1.034428E-01 1.445270E+02 2.584639E-01 1137 14 1.081684E-01 1.436985E+02 2.487570E-01 1137 15 1.128939E-01 1.431315E+02 2.401013E-01 1137 16 1.176194E-01 1.426724E+02 2.330396E-01 1137 17 1.223449E-01 1.420746E+02 2.264351E-01 1137 18 1.270705E-01 1.408547E+02 2.197315E-01 1137 19 1.317960E-01 1.403342E+02 2.138862E-01 1137 20 1.365215E-01 1.401778E+02 2.094760E-01 1137 21 1.412471E-01 1.393883E+02 2.046522E-01 1137 22 1.459726E-01 1.386740E+02 1.999935E-01 1137 23 1.506981E-01 1.377347E+02 1.951501E-01 1137 24 1.554236E-01 1.365434E+02 1.910059E-01 1137 25 1.601492E-01 1.360630E+02 1.874411E-01 1137 26 1.648747E-01 1.350691E+02 1.837019E-01 1137 27 1.696002E-01 1.340079E+02 1.796504E-01 1137 28 1.743258E-01 1.328692E+02 1.762715E-01 1137 29 1.790513E-01 1.321035E+02 1.732496E-01 1137 30 1.837768E-01 1.311422E+02 1.702446E-01 1137 31 1.885023E-01 1.299908E+02 1.668541E-01 1137 32 1.932279E-01 1.292480E+02 1.642185E-01 1137 33 1.979534E-01 1.281733E+02 1.614729E-01 1137 34 2.026789E-01 1.269859E+02 1.587805E-01 1137 35 2.074045E-01 1.259343E+02 1.559438E-01 1137 36 2.121300E-01 1.250512E+02 1.537054E-01 1137 37 2.168555E-01 1.238721E+02 1.513138E-01 1137 38 2.215810E-01 1.228964E+02 1.490770E-01 1137 39 2.263066E-01 1.218087E+02 1.465896E-01 1137 40 2.310321E-01 1.205297E+02 1.442879E-01 1137 41 2.357576E-01 1.193836E+02 1.421465E-01 1137 42 2.404832E-01 1.181941E+02 1.400585E-01 1137 43 2.452087E-01 1.171627E+02 1.379318E-01 1137 44 2.499342E-01 1.158864E+02 1.357820E-01 1137 45 2.546598E-01 1.144833E+02 1.337623E-01 1137 46 2.593853E-01 1.132949E+02 1.318853E-01 1137 47 2.641108E-01 1.120718E+02 1.299058E-01 1137 48 2.688363E-01 1.109920E+02 1.280623E-01 1137 49 2.735619E-01 1.097624E+02 1.262737E-01 1137 50 2.782874E-01 1.085674E+02 1.245481E-01 1137 51 2.830129E-01 1.072232E+02 1.227375E-01 1137 52 2.877385E-01 1.060592E+02 1.210429E-01 1137 53 2.924640E-01 1.046533E+02 1.193477E-01 1137 54 2.971895E-01 1.033373E+02 1.176905E-01 1137 55 3.019150E-01 1.020489E+02 1.160221E-01 1137 56 3.066406E-01 1.008113E+02 1.143632E-01 1137 57 3.113661E-01 9.949685E+01 1.128217E-01 1137 58 3.160916E-01 9.826644E+01 1.113289E-01 1137 59 3.208172E-01 9.694837E+01 1.097867E-01 1137 60 3.255427E-01 9.602761E+01 1.086017E-01 1137 61 3.302682E-01 9.473657E+01 1.094549E-01 1137 62 3.349937E-01 9.325205E+01 1.093560E-01 1137 63 3.397193E-01 9.165042E+01 1.087838E-01 1137 64 3.444448E-01 9.072442E+01 1.085602E-01 1137 65 3.491703E-01 8.951354E+01 1.104798E-01 1137 66 3.538959E-01 8.798045E+01 1.112963E-01 1137 67 3.586214E-01 8.685189E+01 1.118449E-01 1137 68 3.633469E-01 8.549301E+01 1.119964E-01 1137 69 3.680724E-01 8.416319E+01 1.120359E-01 1137 70 3.727980E-01 8.287378E+01 1.120540E-01 1137 71 3.775235E-01 8.160913E+01 1.118107E-01 1137 72 3.822490E-01 8.030843E+01 1.115277E-01 1137 73 3.869746E-01 7.882661E+01 1.111347E-01 1137 74 3.917001E-01 7.778137E+01 1.108962E-01 1137 75 3.964256E-01 7.663455E+01 1.126381E-01 1137 76 4.011511E-01 7.500849E+01 1.150746E-01 1137 77 4.058767E-01 7.365887E+01 1.165163E-01 1137 78 4.106022E-01 7.218711E+01 1.176466E-01 1137 79 4.153277E-01 7.081775E+01 1.187339E-01 1137 80 4.200533E-01 6.949432E+01 1.195558E-01 1137 81 4.247788E-01 6.826181E+01 1.203914E-01 1137 82 4.295043E-01 6.712606E+01 1.212135E-01 1137 83 4.342299E-01 6.570404E+01 1.219025E-01 1137 84 4.389554E-01 6.435614E+01 1.226248E-01 1137 85 4.436809E-01 6.326298E+01 1.232878E-01 1137 86 4.484064E-01 6.204018E+01 1.238028E-01 1137 87 4.531320E-01 6.067109E+01 1.239927E-01 1137 88 4.578575E-01 5.944472E+01 1.237514E-01 1137 89 4.625830E-01 5.884877E+01 1.186656E-01 1137 90 4.673086E-01 5.766086E+01 1.147781E-01 1137 91 4.720341E-01 5.641105E+01 1.120197E-01 1137 92 4.767596E-01 5.532041E+01 1.098291E-01 1137 93 4.814851E-01 5.420641E+01 1.078490E-01 1137 94 4.862107E-01 5.305745E+01 1.060555E-01 1137 95 4.909362E-01 5.188255E+01 1.043678E-01 1137 96 4.956617E-01 5.076420E+01 1.027852E-01 1137 97 5.003873E-01 4.967154E+01 1.012004E-01 1137 98 5.051128E-01 4.856812E+01 9.978694E-02 1137 99 5.098383E-01 4.756945E+01 9.844680E-02 1137 100 5.145638E-01 4.633243E+01 9.676418E-02 1137 101 5.192894E-01 4.539963E+01 9.513249E-02 1137 102 5.240149E-01 4.444948E+01 9.362623E-02 1137 103 5.287404E-01 4.331312E+01 9.194473E-02 1137 104 5.334660E-01 4.219355E+01 9.030646E-02 1137 105 5.381915E-01 4.131228E+01 8.879458E-02 1137 106 5.429170E-01 4.035805E+01 8.742975E-02 1137 107 5.476425E-01 3.930041E+01 8.593784E-02 1137 108 5.523681E-01 3.839634E+01 8.458158E-02 1137 109 5.570936E-01 3.745521E+01 8.317275E-02 1137 110 5.618191E-01 3.662584E+01 8.193766E-02 1137 111 5.665447E-01 3.579685E+01 8.086087E-02 1137 112 5.712702E-01 3.487593E+01 7.985276E-02 1137 113 5.759957E-01 3.381294E+01 7.861452E-02 1137 114 5.807213E-01 3.294355E+01 7.761057E-02 1137 115 5.854468E-01 3.205320E+01 7.656318E-02 1137 116 5.901723E-01 3.126489E+01 7.564587E-02 1137 117 5.948978E-01 3.061397E+01 7.478486E-02 1137 118 5.996234E-01 2.975786E+01 7.375966E-02 1137 119 6.043489E-01 2.899333E+01 7.286727E-02 1137 120 6.090744E-01 2.821740E+01 7.196677E-02 1137 121 6.138000E-01 2.728201E+01 7.087489E-02 1137 122 6.185255E-01 2.657456E+01 7.004514E-02 1137 123 6.232510E-01 2.583764E+01 6.911251E-02 1137 124 6.279765E-01 2.514925E+01 6.823395E-02 1137 125 6.327021E-01 2.457460E+01 6.751034E-02 1137 126 6.374276E-01 2.379981E+01 6.650577E-02 1137 127 6.421531E-01 2.317411E+01 6.568769E-02 1137 128 6.468787E-01 2.252452E+01 6.489310E-02 1137 129 6.516042E-01 2.188163E+01 6.402841E-02 1137 130 6.563297E-01 2.116412E+01 6.314237E-02 1137 131 6.610552E-01 2.045286E+01 6.225605E-02 1137 132 6.657808E-01 1.986398E+01 6.146704E-02 1137 133 6.705063E-01 1.932450E+01 6.074182E-02 1137 134 6.752318E-01 1.882985E+01 5.998190E-02 1137 135 6.799574E-01 1.821868E+01 5.923413E-02 1137 136 6.846829E-01 1.767849E+01 5.848469E-02 1137 137 6.894084E-01 1.716087E+01 5.777977E-02 1137 138 6.941339E-01 1.662355E+01 5.699696E-02 1137 139 6.988595E-01 1.618062E+01 5.638449E-02 1137 140 7.035850E-01 1.556992E+01 5.553913E-02 1137 141 7.083105E-01 1.511759E+01 5.493476E-02 1137 142 7.130361E-01 1.472960E+01 5.434072E-02 1137 143 7.177616E-01 1.417728E+01 5.359021E-02 1137 144 7.224871E-01 1.373465E+01 5.293151E-02 1137 145 7.272127E-01 1.331977E+01 5.230468E-02 1137 146 7.319382E-01 1.291392E+01 5.162883E-02 1137 147 7.366637E-01 1.250344E+01 5.105873E-02 1137 148 7.413892E-01 1.203276E+01 5.041366E-02 1137 149 7.461148E-01 1.160730E+01 4.977136E-02 1137 150 7.508403E-01 1.128773E+01 4.923459E-02 1137 151 7.555658E-01 1.094494E+01 4.869579E-02 1137 152 7.602914E-01 1.061266E+01 4.815207E-02 1137 153 7.650169E-01 1.027000E+01 4.761831E-02 1137 154 7.697424E-01 9.953187E+00 4.708611E-02 1137 155 7.744679E-01 9.579906E+00 4.654294E-02 1137 156 7.791935E-01 9.220704E+00 4.601075E-02 1137 157 7.839190E-01 9.022802E+00 4.563788E-02 1137 158 7.886445E-01 8.686326E+00 4.508044E-02 1137 159 7.933701E-01 8.459856E+00 4.465054E-02 1137 160 7.980956E-01 8.147893E+00 4.419506E-02 1137 161 8.028211E-01 7.842712E+00 4.379906E-02 1137 162 8.075466E-01 7.572036E+00 4.323294E-02 1137 163 8.122722E-01 7.400132E+00 4.291620E-02 1137 164 8.169977E-01 7.112262E+00 4.240319E-02 1137 165 8.217232E-01 6.865932E+00 4.197397E-02 1137 166 8.264488E-01 6.674847E+00 4.166061E-02 1137 167 8.311743E-01 6.460731E+00 4.127965E-02 1137 168 8.358998E-01 6.265235E+00 4.095801E-02 1137 169 8.406253E-01 6.133742E+00 4.059142E-02 1137 170 8.453509E-01 5.857247E+00 4.014562E-02 1137 171 8.500764E-01 5.731786E+00 3.988053E-02 1137 172 8.548019E-01 5.615038E+00 3.964074E-02 1137 173 8.595275E-01 5.356652E+00 3.919827E-02 1137 174 8.642530E-01 5.212237E+00 3.886276E-02 1137 175 8.689785E-01 4.990018E+00 3.851830E-02 1137 176 8.737041E-01 4.822313E+00 3.821750E-02 1137 177 8.784296E-01 4.691209E+00 3.793215E-02 1137 178 8.831551E-01 4.573467E+00 3.770848E-02 1137 179 8.878806E-01 4.398748E+00 3.733972E-02 1137 180 8.926062E-01 4.408623E+00 3.724763E-02 1137 181 8.973317E-01 4.242744E+00 3.697666E-02 1137 182 9.020572E-01 4.130228E+00 3.676978E-02 1137 183 9.067828E-01 3.925051E+00 3.639440E-02 1137 184 9.115083E-01 3.858631E+00 3.620277E-02 1137 185 9.162338E-01 3.789568E+00 3.603472E-02 1137 186 9.209593E-01 3.711122E+00 3.581719E-02 1137 187 9.256849E-01 3.596047E+00 3.552374E-02 1137 188 9.304104E-01 3.443541E+00 3.532795E-02 1137 189 9.351359E-01 3.382168E+00 3.514959E-02 1137 190 9.398615E-01 3.281558E+00 3.490535E-02 1137 191 9.445870E-01 3.205075E+00 3.474870E-02 1137 192 9.493125E-01 3.156628E+00 3.457759E-02 1137 193 9.540380E-01 3.047419E+00 3.438440E-02 1137 194 9.587636E-01 3.011056E+00 3.426381E-02 1137 195 9.634891E-01 2.941241E+00 3.408455E-02 1137 196 9.682146E-01 2.867153E+00 3.387120E-02 1137 197 9.729402E-01 2.849683E+00 3.378761E-02 1137 198 9.776657E-01 2.750646E+00 3.357764E-02 1137 199 9.823912E-01 2.661026E+00 3.341771E-02 1137 200 9.871167E-01 2.674064E+00 3.335854E-02 1137 201 9.918423E-01 2.589506E+00 3.316682E-02 1137 202 9.965678E-01 2.561287E+00 3.303484E-02 1137 203 1.001293E+00 2.507784E+00 3.287554E-02 1137 204 1.006019E+00 2.433996E+00 3.274867E-02 1137 205 1.010744E+00 2.456807E+00 3.276634E-02 1137 206 1.015470E+00 2.354656E+00 3.254678E-02 1137 207 1.020195E+00 2.372007E+00 3.248463E-02 1137 208 1.024921E+00 2.329125E+00 3.236424E-02 1137 209 1.029647E+00 2.287118E+00 3.221738E-02 1137 210 1.034372E+00 2.240322E+00 3.210503E-02 1137 211 1.039098E+00 2.241939E+00 3.203262E-02 1137 212 1.043823E+00 2.193723E+00 3.188052E-02 1137 213 1.048549E+00 2.158219E+00 3.180050E-02 1137 214 1.053274E+00 2.112469E+00 3.170611E-02 1137 215 1.058000E+00 2.076601E+00 3.156186E-02 1137 216 1.062725E+00 2.027739E+00 3.148628E-02 1137 217 1.067451E+00 2.064239E+00 3.146270E-02 1137 218 1.072176E+00 2.082144E+00 3.135776E-02 1137 219 1.076902E+00 2.029184E+00 3.127360E-02 1137 220 1.081627E+00 1.993149E+00 3.115029E-02 1137 221 1.086353E+00 1.938361E+00 3.115718E-02 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1.679055E-01 2.145332E-02 1137 762 3.642864E+00 1.474649E-01 2.156778E-02 1137 763 3.647590E+00 1.647785E-01 2.172318E-02 1137 764 3.652315E+00 1.641791E-01 2.184258E-02 1137 765 3.657041E+00 1.484466E-01 2.193029E-02 1137 766 3.661766E+00 1.763694E-01 2.205393E-02 1137 767 3.666492E+00 1.464121E-01 2.216651E-02 1137 768 3.671217E+00 1.572224E-01 2.226507E-02 1137 769 3.675943E+00 1.506809E-01 2.236467E-02 1137 770 3.680668E+00 1.559478E-01 2.249402E-02 1137 771 3.685394E+00 1.492964E-01 2.258906E-02 1137 772 3.690119E+00 1.426396E-01 2.264573E-02 1137 773 3.694845E+00 1.366159E-01 2.276331E-02 1137 774 3.699570E+00 1.236318E-01 2.283521E-02 1137 775 3.704296E+00 1.120823E-01 2.294802E-02 1137 776 3.709021E+00 1.288128E-01 2.306910E-02 1137 777 3.713747E+00 1.263604E-01 2.316649E-02 1137 778 3.718473E+00 1.618252E-01 2.328278E-02 1137 779 3.723198E+00 1.748191E-01 2.336379E-02 1137 780 3.727924E+00 1.625641E-01 2.343112E-02 1137 781 3.732649E+00 1.721060E-01 2.355046E-02 1137 782 3.737375E+00 1.742671E-01 2.362926E-02 1137 783 3.742100E+00 1.686896E-01 2.371827E-02 1137 784 3.746826E+00 1.600609E-01 2.382122E-02 1137 785 3.751551E+00 1.784147E-01 2.390351E-02 1137 786 3.756277E+00 1.779639E-01 2.400739E-02 1137 787 3.761002E+00 1.228092E-01 2.403410E-02 1137 788 3.765728E+00 1.091654E-01 2.409447E-02 1137 789 3.770453E+00 1.105341E-01 2.418623E-02 1137 790 3.775179E+00 1.802187E-01 2.431080E-02 1137 791 3.779904E+00 1.962394E-01 2.443246E-02 1137 792 3.784630E+00 1.741018E-01 2.450486E-02 1137 793 3.789355E+00 1.548688E-01 2.459395E-02 1137 794 3.794081E+00 1.160275E-01 2.463183E-02 1137 795 3.798807E+00 1.468513E-01 2.473711E-02 1137 796 3.803532E+00 1.550178E-01 2.484995E-02 1137 #