{ "code": "SASDAN4", "status": "Published", "type_of_curve": "Merged", "angular_unit": "1/nm", "project": { "title": "Interaction between the C-terminal region of human myelin basic protein and calmodulin: analysis of complex formation and solution structure.", "publication": { "title": "Interaction between the C-terminal region of human myelin basic protein and calmodulin: analysis of complex formation and solution structure.", "author_list": "Majava V, Petoukhov MV, Hayashi N, Pirilä P, Svergun DI, Kursula P", "journal": "BMC Struct Biol", "doi": "10.1186/1472-6807-8-10", "pmid": "18284662", "published_date": "2008 Feb 19" }, "status": "released", "submitted_date": null, "released_date": "2015-07-07" }, "pddf_data": "https://www.sasbdb.org/media/p_of_R_files/SASDAN4.out", "intensities_data": "https://www.sasbdb.org/media/intensities_files/SASDAN4.dat", "intensities_log_plot": "https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDAN4_dat_img.png", "intensities_kratky_plot": "https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDAN4_kratky_img.png", "pddf_plot": "https://www.sasbdb.org/media/p_of_R_files/pofr_images/SASDAN4_pofr_img.png", "intensities_guinier_plot": "https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDAN4_guinier_img.png", "sascif_data": "https://www.sasbdb.org/media/sascif/sascif_files/SASDAN4.sascif", "experiment": { "instrument": { "detector": { "type": null, "name": "MAR 345 Image Plate", "resolution": null }, "name": "DORIS III, DESY", "city": "Hamburg", "country": "Germany", "beamline_name": "EMBL X33", "beam_geometry": null, "type_of_source": "X-ray synchrotron", "point_source": null, "line_collimation": null, "sample_path_length": null, "line_collimation_slitlength": null, "line_collimation_integrationwidth": null, "xray_energy": null, "beam_profile_ah": null, "beam_profile_al": null }, "sample": { "molecule": [ { "long_name": "Calmodulin", "short_name": null, "sequence": ">sp|P62158|CALM_HUMAN Calmodulin OS=Homo sapiens GN=CALM1 PE=1 SV=2\nMADQLTEEQIAEFKEAFSLFDKDGDGTITTKELGTVMRSLGQNPTEAELQDMINEVDADG\nNGTIDFPEFLTMMARKMKDTDSEEEIREAFRVFDKDGNGYISAAELRHVMTNLGEKLTDE\nEVDEMIREADIDGDGQVNYEEFVQMMTAK\n\n", "organism": "Homo sapiens", "uniprot_code": "P62158", "uniprot_range_first": null, "uniprot_range_last": null, "oligomerization": "monomer", "molecular_type": "protein", "uniprot_sequence": null, "mw": 16.84, "total_mw": 16.84, "number_molecules": 1, "complex_state": null, "deuteration": null, "molecule_source": "biological", "molecule_description": null }, { "long_name": "C-terminal region of human myelin basic protein", "short_name": "peptide", "sequence": "HKGFKGVDAQGTLSKIFKL", "organism": "Homo sapiens", "uniprot_code": null, "uniprot_range_first": null, "uniprot_range_last": null, "oligomerization": "monomer", "molecular_type": "protein", "uniprot_sequence": null, "mw": 2.0, "total_mw": 2.0, "number_molecules": 1, "complex_state": null, "deuteration": null, "molecule_source": "biological", "molecule_description": null } ], "buffer": { "name": "25 mM Tris75 200 mM NaCl", "concentration_unit": "mM", "comment": null, "additive": "NaCl 200.000 mM", "concentration": 25.0, "pka": null, "ph": 7.5, "deuteration": null }, "purity_method": null, "name": "Calmodulin:peptide complex", "ext_coefficient": null, "contrast": null, "specific_vol": null, "dry_vol": null, "absorbption": null, "deuteration": null, "mixture": null }, "contributor": [ { "affiliation": [ { "short_name": "EMBL-Hamburg", "address": "Notkestraße 85, Geb. 25A, 22607 Hamburg, Deutschland, Germany", "full_name": "European Molecular Biology Laboratory (EMBL) - Hamburg outstation", "webpage": "http://www.embl-hamburg.de/index.php" } ], "contributor_name": "Maxim", "contributor_surname": "Petoukhov", "orcid": null } ], "concentration_method": null, "concentration_unit": null, "date": "2006-11-28", "storage_temperature": null, "cell_temperature": null, "exposure_time": null, "number_of_frames": null, "wavelength": null, "sample_detector_distance": null, "concentration_min": 5.3, "concentration_max": 20.0, "sample_volume": null, "flow_rate": null, "s_min": 0.32, "s_max": 5.01, "total_exposure_time": null, "seccolumn": null }, "fits": [ { "models": [ { "model_plot": "https://www.sasbdb.org/media/pdb_file/images/SASDAN4_fit1_model1_img.png", "software": "SASREF", "pdb_link": [], "model_title": null, "type_of_model": "atomic", "software_version": "", "model_data": "https://www.sasbdb.org/media/pdb_file/SASDAN4_fit1_model1.pdb", "model_mw": 18.63, "bead_radius": 0.0, "log": null, "symmetry": "", "comment": "", "user": 102 } ], "fit_unit": "1/A", "fit_plot": "https://www.sasbdb.org/media/fitting_files/scattering_plots/SASDAN4_fit1_fit_img.png", "software": null, "chi_square_value": 4.7524, "p_value": 0.0, "fit_residual_plot": "SASDAN4_fit1_fitresiduals_img.png", "fit_data": "https://www.sasbdb.org/media/fitting_files/SASDAN4_fit1.fit", "fit_log": null, "software_version": null, "description": null } ], "estimated_volume_method": null, "pddf_software": "ATSAS GNOM", "pddf_software_version": null, "i0_calibration_standard": null, "description": null, "experiment_description": null, "tags": [ "X33" ], "intensity_unit": null, "experimental_mw": 20.0, "experimental_mw_error": null, "guinier_i0_mw": null, "guinier_i0_mw_error": null, "porod_mw": null, "porod_mw_error": null, "pddf_i0": null, "pddf_i0_error": null, "guinier_i0": 107.587, "guinier_i0_error": null, "pddf_rg": null, "pddf_rg_error": null, "guinier_rg": 2.1, "guinier_rg_error": null, "pddf_dmax": 7.0, "pddf_dmax_error": null, "porod_volume": 36.0, "porod_volume_error": null, "estimated_volume": null, "estimated_volume_error": null, "guinier_point_first": 1, "guinier_point_last": 85, "pddf_point_first": null, "pddf_point_last": null, "i0_calibration_standard_data": null, "intensities_log_log_plot": "SASDAN4_datloglog_img.png", "symmetry": null, "last_modified": "2023-05-25T11:22:16.556436+02:00", "bragg_peak": [] }