REMARK 265 REMARK 265 EXPERIMENT TYPE : X-RAY SOLUTION SCATTERING REMARK 265 DATA ACQUISITION REMARK 265 RADIATION SOURCE : BENDING MAGNET REMARK 265 SYNCHROTRON (Y/N) : Y REMARK 265 BEAMLINE : B21 DIAMOND LIGHT SOURCE REMARK 265 REMARK 265 DATA REDUCTION SOFTWARE : SCATTER (v 3.1q) REMARK 265 SOFTWARE AUTHOR : RP RAMBO REMARK 265 DATA ANALYSIS SOFTWARE : SCATTER (v 3.1q) REMARK 265 SOFTWARE AUTHOR : RP RAMBO REMARK 265 REMARK 265 EXPERIMENTAL INFO REMARK 265 INFORMATION CAN BE ADDED BY DUPLICATING THE NOTE LINE BELOW REMARK 265 REMARK 265 NOTE : SEC-SAXS Signal Plot. 10.0 mg/ml of protein was injected into a into a 4.6 ml Shodex KW403-4F size exclusion column at a flow rate of 0.16 mL min−1. ) REMARK 265 NOTE : Two-second frames in B21 using a Pilatus 2M pixel detector (DECTRIS) REMARK 265 REMARK 265 EXPERIMENTAL DETAILS REMARK 265 BUFFER COMPOSITION REMARK 265 TEMPERATURE (KELVIN) : 283 K REMARK 265 PH : 7.6 REMARK 265 SAMPLE BUFFER : 50 mM Tris-HCl REMARK 265 SAMPLE BUFFER :150 mM NaCl REMARK 265 SAMPLE BUFFER : 2 mM TCEP REMARK 265 REMARK 265 COLUMNS : q, I(q), error REMARK 265 q : defined in inverse Angstroms 3.200000e-03 1.491330e+04 1.012260e-01 3.420831e-03 3.131170e-01 5.857080e-02 3.641662e-03 -4.802840e+00 1.175000e-01 3.862493e-03 -1.238760e+01 2.214930e-01 4.083323e-03 -4.924620e+00 1.028260e-01 4.304154e-03 -6.248960e-01 3.162970e-02 4.524985e-03 3.908980e-02 1.584930e-02 4.745816e-03 5.859820e-02 1.383180e-02 4.966647e-03 5.909100e-02 1.282530e-02 5.187477e-03 8.542510e-02 1.112930e-02 5.408308e-03 8.156500e-02 1.044050e-02 5.629139e-03 8.239560e-02 9.544220e-03 5.849970e-03 8.984490e-02 9.143910e-03 6.070801e-03 7.274960e-02 8.516940e-03 6.291632e-03 8.940060e-02 7.792600e-03 6.512462e-03 8.070900e-02 7.609480e-03 6.733293e-03 8.596190e-02 7.199680e-03 6.954124e-03 8.332430e-02 6.558380e-03 7.174955e-03 7.418460e-02 6.473760e-03 7.395786e-03 6.927040e-02 6.274080e-03 7.616617e-03 9.007850e-02 5.491080e-03 7.837447e-03 7.838460e-02 5.446520e-03 8.058278e-03 9.072890e-02 5.313050e-03 8.279109e-03 7.983670e-02 5.057090e-03 8.499940e-03 8.862330e-02 4.895860e-03 8.720771e-03 8.499080e-02 4.560220e-03 8.941601e-03 7.372240e-02 4.419770e-03 9.162432e-03 8.373860e-02 4.139180e-03 9.383263e-03 8.547380e-02 3.947950e-03 9.604094e-03 8.977070e-02 3.874230e-03 9.824925e-03 8.454430e-02 3.852880e-03 1.004576e-02 8.542290e-02 3.564980e-03 1.026659e-02 8.373270e-02 3.436310e-03 1.048742e-02 8.877860e-02 3.264320e-03 1.070825e-02 8.324680e-02 3.125280e-03 1.092908e-02 8.625160e-02 3.047820e-03 1.114991e-02 8.988990e-02 2.899340e-03 1.137074e-02 8.105370e-02 2.801130e-03 1.159157e-02 8.527480e-02 2.776730e-03 1.181240e-02 8.343960e-02 2.546490e-03 1.203323e-02 7.894290e-02 2.502200e-03 1.225406e-02 8.263040e-02 2.419680e-03 1.247489e-02 8.822010e-02 2.295220e-03 1.269572e-02 8.210550e-02 2.264590e-03 1.291656e-02 8.180180e-02 2.172570e-03 1.313739e-02 7.890030e-02 2.056730e-03 1.335822e-02 8.513600e-02 2.062030e-03 1.357905e-02 8.224700e-02 1.958130e-03 1.379988e-02 8.059530e-02 1.862070e-03 1.402071e-02 8.438930e-02 1.852290e-03 1.424154e-02 8.192460e-02 1.723150e-03 1.446237e-02 8.443540e-02 1.705220e-03 1.468320e-02 8.281700e-02 1.679910e-03 1.490403e-02 7.953010e-02 1.596280e-03 1.512486e-02 8.215680e-02 1.543100e-03 1.534569e-02 8.077480e-02 1.518800e-03 1.556653e-02 8.192770e-02 1.475520e-03 1.578736e-02 8.097790e-02 1.409140e-03 1.600819e-02 8.171720e-02 1.387920e-03 1.622902e-02 8.121330e-02 1.332860e-03 1.644985e-02 8.088000e-02 1.335820e-03 1.667068e-02 8.046540e-02 1.285740e-03 1.689151e-02 7.960290e-02 1.265650e-03 1.711234e-02 8.296140e-02 1.217750e-03 1.733317e-02 8.102380e-02 1.179210e-03 1.755400e-02 7.907300e-02 1.143370e-03 1.777483e-02 7.908440e-02 1.132790e-03 1.799567e-02 7.956690e-02 1.106430e-03 1.821650e-02 8.113020e-02 1.114630e-03 1.843733e-02 7.925390e-02 1.073200e-03 1.865816e-02 8.003400e-02 1.036990e-03 1.887899e-02 7.961300e-02 1.022970e-03 1.909982e-02 7.990850e-02 1.001830e-03 1.932065e-02 8.195360e-02 9.898760e-04 1.954148e-02 7.784000e-02 9.826120e-04 1.976231e-02 8.015750e-02 9.483130e-04 1.998314e-02 8.078600e-02 9.451960e-04 2.020397e-02 7.927030e-02 9.058200e-04 2.042480e-02 7.946270e-02 9.134920e-04 2.064563e-02 7.966400e-02 8.946410e-04 2.086647e-02 7.963960e-02 8.921680e-04 2.108730e-02 7.770760e-02 8.512140e-04 2.130813e-02 7.932440e-02 8.503790e-04 2.152896e-02 8.154090e-02 8.440940e-04 2.174979e-02 7.740390e-02 8.337540e-04 2.197062e-02 7.794680e-02 8.209500e-04 2.219145e-02 7.946640e-02 8.131220e-04 2.241228e-02 7.926830e-02 7.992710e-04 2.263311e-02 7.777190e-02 7.699660e-04 2.285394e-02 7.770650e-02 7.707510e-04 2.307477e-02 7.780810e-02 7.673220e-04 2.329561e-02 7.759030e-02 7.654230e-04 2.351644e-02 7.755390e-02 7.580140e-04 2.373727e-02 7.665200e-02 7.359060e-04 2.395810e-02 7.898310e-02 7.243870e-04 2.417893e-02 7.838680e-02 7.193650e-04 2.439976e-02 7.598530e-02 7.150430e-04 2.462059e-02 7.500810e-02 7.025490e-04 2.484142e-02 7.642240e-02 7.098890e-04 2.506225e-02 7.551310e-02 6.936030e-04 2.528308e-02 7.586760e-02 6.828860e-04 2.550391e-02 7.679760e-02 6.740320e-04 2.572474e-02 7.642150e-02 6.784650e-04 2.594557e-02 7.614010e-02 6.689850e-04 2.616641e-02 7.453070e-02 6.641650e-04 2.638724e-02 7.551090e-02 6.572680e-04 2.660807e-02 7.614700e-02 6.522030e-04 2.682890e-02 7.666320e-02 6.451480e-04 2.704973e-02 7.619080e-02 6.398960e-04 2.727056e-02 7.477910e-02 6.345970e-04 2.749139e-02 7.379150e-02 6.291030e-04 2.771222e-02 7.500640e-02 6.191030e-04 2.793305e-02 7.450040e-02 6.107840e-04 2.815388e-02 7.505710e-02 6.149400e-04 2.837471e-02 7.355490e-02 6.132370e-04 2.859554e-02 7.427800e-02 6.039660e-04 2.881638e-02 7.387310e-02 5.995070e-04 2.903721e-02 7.329100e-02 5.977260e-04 2.925804e-02 7.419640e-02 5.849220e-04 2.947887e-02 7.282820e-02 5.799480e-04 2.969970e-02 7.352210e-02 5.800340e-04 2.992053e-02 7.340520e-02 5.784930e-04 3.014136e-02 7.222110e-02 5.785090e-04 3.036219e-02 7.216580e-02 5.726710e-04 3.058302e-02 7.157520e-02 5.590860e-04 3.080385e-02 7.133050e-02 5.564760e-04 3.102468e-02 7.153230e-02 5.520510e-04 3.124552e-02 7.119070e-02 5.477030e-04 3.146635e-02 7.091740e-02 5.530320e-04 3.168718e-02 7.109560e-02 5.554830e-04 3.190801e-02 7.151210e-02 5.391960e-04 3.212884e-02 7.100310e-02 5.374300e-04 3.234967e-02 7.149390e-02 5.349220e-04 3.257050e-02 7.082050e-02 5.356710e-04 3.279133e-02 6.999860e-02 5.284890e-04 3.301216e-02 7.091460e-02 5.304960e-04 3.323299e-02 7.045760e-02 5.249590e-04 3.345382e-02 6.935060e-02 5.208560e-04 3.367465e-02 6.955580e-02 5.114850e-04 3.389549e-02 6.997750e-02 5.172560e-04 3.411632e-02 6.914900e-02 5.102850e-04 3.433715e-02 6.939890e-02 5.118840e-04 3.455798e-02 6.955420e-02 5.036430e-04 3.477881e-02 6.781680e-02 5.008850e-04 3.499964e-02 6.911910e-02 5.033110e-04 3.522047e-02 6.837910e-02 4.994690e-04 3.544130e-02 6.880230e-02 4.960160e-04 3.566213e-02 6.813610e-02 4.959870e-04 3.588296e-02 6.886020e-02 4.910760e-04 3.610379e-02 6.819370e-02 4.798610e-04 3.632462e-02 6.756450e-02 4.875180e-04 3.654545e-02 6.695720e-02 4.795820e-04 3.676629e-02 6.762710e-02 4.839660e-04 3.698712e-02 6.644310e-02 4.849850e-04 3.720795e-02 6.702130e-02 4.680160e-04 3.742878e-02 6.628230e-02 4.707260e-04 3.764961e-02 6.694100e-02 4.703730e-04 3.787044e-02 6.606770e-02 4.645000e-04 3.809127e-02 6.664480e-02 4.678260e-04 3.831210e-02 6.616770e-02 4.762080e-04 3.853293e-02 6.575670e-02 4.569970e-04 3.875376e-02 6.443600e-02 4.552360e-04 3.897459e-02 6.538470e-02 4.550680e-04 3.919542e-02 6.566490e-02 4.547240e-04 3.941625e-02 6.519710e-02 4.547700e-04 3.963709e-02 6.551810e-02 4.539860e-04 3.985792e-02 6.435870e-02 4.459620e-04 4.007875e-02 6.398570e-02 4.505560e-04 4.029958e-02 6.461610e-02 4.418680e-04 4.052041e-02 6.454450e-02 4.415250e-04 4.074124e-02 6.396460e-02 4.458480e-04 4.096207e-02 6.417970e-02 4.419540e-04 4.118290e-02 6.439130e-02 4.355920e-04 4.140373e-02 6.359750e-02 4.341480e-04 4.162456e-02 6.311170e-02 4.313180e-04 4.184539e-02 6.307630e-02 4.352240e-04 4.206622e-02 6.237610e-02 4.273550e-04 4.228706e-02 6.263430e-02 4.323810e-04 4.250789e-02 6.279790e-02 4.265470e-04 4.272872e-02 6.193870e-02 4.208110e-04 4.294955e-02 6.201580e-02 4.189880e-04 4.317038e-02 6.185060e-02 4.230680e-04 4.339121e-02 6.156190e-02 4.205080e-04 4.361204e-02 6.104300e-02 4.177930e-04 4.383287e-02 6.138190e-02 4.167840e-04 4.405370e-02 6.082520e-02 4.087720e-04 4.427453e-02 6.010560e-02 4.135460e-04 4.449536e-02 6.066000e-02 4.066450e-04 4.471620e-02 6.087610e-02 4.095980e-04 4.493703e-02 6.024490e-02 4.104950e-04 4.515786e-02 5.962010e-02 4.073560e-04 4.537869e-02 5.980210e-02 4.004510e-04 4.559952e-02 5.919880e-02 3.992080e-04 4.582035e-02 5.920030e-02 3.999090e-04 4.604118e-02 5.856230e-02 3.972160e-04 4.626201e-02 5.880610e-02 3.993780e-04 4.648284e-02 5.841270e-02 3.931500e-04 4.670367e-02 5.827750e-02 3.950310e-04 4.692450e-02 5.821520e-02 3.921890e-04 4.714533e-02 5.835830e-02 3.895330e-04 4.736617e-02 5.758790e-02 3.897460e-04 4.758700e-02 5.786080e-02 3.891780e-04 4.780783e-02 5.769980e-02 3.875590e-04 4.802866e-02 5.738300e-02 3.847240e-04 4.824949e-02 5.685820e-02 3.809660e-04 4.847032e-02 5.746970e-02 3.854950e-04 4.869115e-02 5.667800e-02 3.819420e-04 4.891198e-02 5.605840e-02 3.777560e-04 4.913281e-02 5.634650e-02 3.784230e-04 4.935364e-02 5.633520e-02 3.771240e-04 4.957447e-02 5.503220e-02 3.696670e-04 4.979530e-02 5.521810e-02 3.724560e-04 5.001614e-02 5.549190e-02 3.702080e-04 5.023697e-02 5.382300e-02 3.736780e-04 5.045780e-02 5.404400e-02 3.680840e-04 5.067863e-02 5.449790e-02 3.632600e-04 5.089946e-02 5.396570e-02 3.652060e-04 5.112029e-02 5.455510e-02 3.644910e-04 5.134112e-02 5.337240e-02 3.618290e-04 5.156195e-02 5.357690e-02 3.615200e-04 5.178278e-02 5.308380e-02 3.679330e-04 5.200361e-02 5.293940e-02 3.540060e-04 5.222444e-02 5.298400e-02 3.586970e-04 5.244527e-02 5.273800e-02 3.544750e-04 5.266610e-02 5.277620e-02 3.552410e-04 5.288694e-02 5.224480e-02 3.528860e-04 5.310777e-02 5.173070e-02 3.537220e-04 5.332860e-02 5.245250e-02 3.525770e-04 5.354943e-02 5.191710e-02 3.529590e-04 5.377026e-02 5.120350e-02 3.560680e-04 5.399109e-02 5.141140e-02 3.621660e-04 5.421192e-02 5.103570e-02 3.662030e-04 5.443275e-02 5.067400e-02 3.625760e-04 5.465358e-02 5.049260e-02 3.698070e-04 5.487441e-02 5.107610e-02 3.721550e-04 5.509524e-02 5.050040e-02 3.694220e-04 5.531607e-02 5.011990e-02 3.755680e-04 5.553690e-02 5.031360e-02 3.719320e-04 5.575774e-02 4.908880e-02 3.711240e-04 5.597857e-02 4.932140e-02 3.774340e-04 5.619940e-02 4.892500e-02 3.736850e-04 5.642023e-02 4.900500e-02 3.762360e-04 5.664106e-02 4.837810e-02 3.758840e-04 5.686189e-02 4.802290e-02 3.765990e-04 5.708272e-02 4.791330e-02 3.815400e-04 5.730355e-02 4.823060e-02 3.832920e-04 5.752438e-02 4.777890e-02 3.830730e-04 5.774521e-02 4.745940e-02 3.902890e-04 5.796605e-02 4.723530e-02 3.849380e-04 5.818687e-02 4.724730e-02 3.835480e-04 5.840771e-02 4.698690e-02 3.839300e-04 5.862854e-02 4.758390e-02 3.749480e-04 5.884937e-02 4.644480e-02 3.631780e-04 5.907020e-02 4.607630e-02 3.626960e-04 5.929103e-02 4.655650e-02 3.578950e-04 5.951186e-02 4.651230e-02 3.563920e-04 5.973269e-02 4.546630e-02 3.562260e-04 5.995352e-02 4.562900e-02 3.490060e-04 6.017435e-02 4.528030e-02 3.456690e-04 6.039518e-02 4.470900e-02 3.412910e-04 6.061601e-02 4.482580e-02 3.411050e-04 6.083685e-02 4.442740e-02 3.418580e-04 6.105768e-02 4.432850e-02 3.360710e-04 6.127851e-02 4.414460e-02 3.377180e-04 6.149934e-02 4.417410e-02 3.336570e-04 6.172017e-02 4.344640e-02 3.276230e-04 6.194100e-02 4.346550e-02 3.332800e-04 6.216183e-02 4.354690e-02 3.291040e-04 6.238266e-02 4.322310e-02 3.279610e-04 6.260349e-02 4.278310e-02 3.265380e-04 6.282432e-02 4.223560e-02 3.201190e-04 6.304515e-02 4.242800e-02 3.216640e-04 6.326598e-02 4.230210e-02 3.221290e-04 6.348682e-02 4.253300e-02 3.198110e-04 6.370765e-02 4.240330e-02 3.210620e-04 6.392848e-02 4.146110e-02 3.160320e-04 6.414931e-02 4.139700e-02 3.130080e-04 6.437014e-02 4.112430e-02 3.120020e-04 6.459097e-02 4.143490e-02 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