data_SASDAZ3_MAIN # _sas_result.id 64 _sas_result.SASBDB_code SASDAZ3 _sas_result.experimental_MW 340.000 _sas_result.experimental_MW_error . _sas_result.MW_standard . _sas_result.MW_standard_error . _sas_result.MW_Porod . _sas_result.MW_Porod_error . _sas_result.I0_from_PR . _sas_result.I0_from_PR_error . _sas_result.I0_from_Guinier 280.0000000000 _sas_result.I0_from_Guinier_error . _sas_result.Rg_from_PR . _sas_result.Rg_from_PR_error . _sas_result.Rg_from_Guinier 8.000 _sas_result.Rg_from_Guinier_error . _sas_result.D_max . _sas_result.Porod_volume . _sas_result.Porod_volume_error . _sas_result.estimated_volume . _sas_result.estimated_volume_error . _sas_result.estimated_volume_method . _sas_result.Guinier_point_min . _sas_result.Guinier_point_max . _sas_result.type_of_curve single_conc _sas_result.standard . _sas_result.Dmax_error . _sas_result.comments . # _sas_scan.title "MutS, c=1.05" _sas_scan.detc_id 4 _sas_scan.id 64 _sas_scan.measurement_date 2011-05-12 _sas_scan.storage_temperature 10.0 _sas_scan.cell_temperature 10.0 _sas_scan.exposure_time . _sas_scan.number_of_frames . _sas_scan.unit 1/nm _sas_scan.qmin 0.0671 _sas_scan.qmax 6.0241 _sas_scan.sample_id 23 _sas_scan.result_id 64 _sas_scan.beam_id 7 # _sas_beam.id 7 _sas_beam.instrument_name "DORIS III X33" _sas_beam.instrument_city Hamburg _sas_beam.instrument_country Germany _sas_beam.shape . _sas_beam.type_of_source "X-ray synchrotron" _sas_beam.radiation_wavelength . _sas_beam.dist_spec_to_detc . # _sas_detc.id 4 _sas_detc.name "Pilatus 2M" _sas_detc.type . _sas_detc.pixsize_x . # _sas_sample.id 23 _sas_sample.name "MutS tetramer" _sas_sample.ext_coefficient . _sas_sample.contrast . _sas_sample.specific_vol . _sas_sample.purity_method . _sas_sample.dry_vol . _sas_sample.sample_MW 381.00 _sas_sample.specimen_concentration 1.05 _sas_sample.concentration_method . _sas_sample.entity_id 40 # _sas_buffer.id 1 _sas_buffer.name HEPES _sas_buffer.concentration 50.00 _sas_buffer.unit mM _sas_buffer.pK 7.000 _sas_buffer.pH 7.500 _sas_buffer.comment "4-(2-hydroxyethyl)-1-piperazineethanesulfonic acid" _sas_buffer.composition "KCl 50.000 mM" _sas_buffer.sample_id 23 # _entity.id 40 _entity.type protein _entity.pdbx_description "DNA mismatch repair protein MutS" _entity.formula_weight 95.250 _entity.pdbx_number_of_molecules 4 # _entity_name_com.entity_id 40 _entity_name_com.name "MutS tetramer" # _entity_poly.entity_id 40 _entity_poly.pdbx_seq_one_letter_code ;MSAIENFDAHTPMMQQYLRLKAQHPEILLFYRMGDFYELFYDDAKRASQLLDISLTKRGA SAGEPIPMAGIPYHAVENYLAKLVNQGESVAICEQIGDPATSKGPVERKVVRIVTPGTIS DEALLQERQDNLLAAIWQDSKGFGYATLDISSGRFRLSEPADRETMAAELQRTNPAELLY AEDFAEMSLIEGRRGLRRRPLWEFEIDTARQQLNLQFGTRDLVGFGVENAPRGLCAAGCL LQYAKDTQRTTLPHIRSITMEREQDSIIMDAATRRNLEITQNLAGGAENTLASVLDCTVT PMGSRMLKRWLHMPVRDTRVLLERQQTIGALQDFTAGLQPVLRQVGDLERILARLALRTA RPRDLARMRHAFQQLPELRAQLETVDSAPVQALREKMGEFAELRDLLERAIIDTPPVLVR DGGVIASGYNEELDEWRALADGATDYLERLEVRERERTGLDTLKVGFNAVHGYYIQISRG QSHLAPINYMRRQTLKNAERYIIPELKEYEDKVLTSKGKALALEKQLYEELFDLLLPHLE ALQQSASALAELDVLVNLAERAYTLNYTCPTFIDKPGIRITEGRHPVVEQVLNEPFIANP LNLSPQRRMLIITGPNMGGKSTYMRQTALIALMAYIGSYVPAQKVEIGPIDRIFTRVGAA DDLASGRSTFMVEMTETANILHNATEYSLVLMDEIGRGTSTYDGLSLAWACAENLANKIK ALTLFATHYFELTQLPEKMEGVANVHLDALEHGDTIAFMHSVQDGAASKSYGLAVAALAG VPKEVIKRARQKLRELESISPNAAATQVDGTQMSLLSVPEETSPAVEALENLDPDSLTPR QALEWIYRLKSLV ; # _entity_src_gen.entity_id 40 _entity_src_gen.gene_src_common_name "Escherichia coli" # _struct_ref.id 1 _struct_ref.entity_id 40 _struct_ref.db_name UniProt _struct_ref.db_code P23909 _struct_ref.details http://www.uniprot.org/uniprot/P23909 # _citation.id 36 _citation.title "Using stable MutS dimers and tetramers to quantitatively analyze DNA mismatch recognition and sliding clamp formation." _citation.year "2013 Sep" _citation.pdbx_database_id_DOI 10.1093/nar/gkt582 _citation.pdbx_database_id_PubMed 23821665 _citation.journal_abbrev "Nucleic Acids Res" _citation.journal_volume 41 _citation.journal_issue 17 _citation.page_first 8166 _citation.page_last 8181 # loop_ _citation_author.citation_id _citation_author.ordinal _citation_author.name 36 1 "Groothuizen FS" 36 2 "Fish A" 36 3 "Petoukhov MV" 36 4 "Reumer A" 36 5 "Manelyte L" 36 6 "Winterwerp HH" 36 7 "Marinus MG" 36 8 "Lebbink JH" 36 9 "Svergun DI" 36 10 "Friedhoff P" # _pdbx_contact_author.id 7 _pdbx_contact_author.name_first Maxim _pdbx_contact_author.name_last Petoukhov _pdbx_contact_author.role . _pdbx_contact_author.address_1 EMBL-Hamburg _pdbx_contact_author.address_2 "European Molecular Biology Laboratory (EMBL) - Hamburg outstation" _pdbx_contact_author.address_3 "Notkestraße 85, Geb. 25A, 22607 Hamburg, Deutschland, Germany" # loop_ _sas_scan_intensity.id _sas_scan_intensity.momentum_transfer _sas_scan_intensity.intensity _sas_scan_intensity.intensity_su_counting _sas_scan_intensity.scan_id 1 6.710100E-02 2.573330E+02 8.402240E+01 64 2 6.983610E-02 2.571430E+02 6.603420E+01 64 3 7.257120E-02 2.682190E+02 5.675690E+01 64 4 7.530620E-02 2.725140E+02 4.862230E+01 64 5 7.804130E-02 2.429140E+02 4.300460E+01 64 6 8.077640E-02 2.543330E+02 3.823360E+01 64 7 8.351150E-02 2.484760E+02 3.414100E+01 64 8 8.624660E-02 2.398100E+02 3.031660E+01 64 9 8.898170E-02 2.462950E+02 2.684790E+01 64 10 9.171680E-02 2.267710E+02 2.430030E+01 64 11 9.445180E-02 2.357240E+02 2.211620E+01 64 12 9.718690E-02 2.449430E+02 1.958970E+01 64 13 9.992200E-02 2.447330E+02 1.795330E+01 64 14 1.026570E-01 2.110670E+02 1.622340E+01 64 15 1.053920E-01 2.273050E+02 1.469680E+01 64 16 1.081270E-01 2.065520E+02 1.347020E+01 64 17 1.108620E-01 2.063620E+02 1.223490E+01 64 18 1.135970E-01 2.049140E+02 1.137200E+01 64 19 1.163330E-01 2.176670E+02 1.059660E+01 64 20 1.190680E-01 2.098480E+02 9.460150E+00 64 21 1.218030E-01 2.018860E+02 9.013790E+00 64 22 1.245380E-01 1.986380E+02 8.213480E+00 64 23 1.272730E-01 1.952760E+02 7.823890E+00 64 24 1.300080E-01 1.914270E+02 7.276710E+00 64 25 1.327430E-01 1.937890E+02 6.603850E+00 64 26 1.354780E-01 1.909850E+02 6.433670E+00 64 27 1.382130E-01 1.839950E+02 5.873060E+00 64 28 1.409480E-01 1.887630E+02 5.590740E+00 64 29 1.436830E-01 1.779360E+02 5.289380E+00 64 30 1.464180E-01 1.725770E+02 4.899190E+00 64 31 1.491540E-01 1.759100E+02 4.824360E+00 64 32 1.518890E-01 1.766700E+02 4.448140E+00 64 33 1.546240E-01 1.715780E+02 4.134210E+00 64 34 1.573590E-01 1.625350E+02 3.961300E+00 64 35 1.600940E-01 1.627850E+02 3.769770E+00 64 36 1.628290E-01 1.581400E+02 3.736620E+00 64 37 1.655640E-01 1.557680E+02 3.389450E+00 64 38 1.682990E-01 1.565680E+02 3.306060E+00 64 39 1.710340E-01 1.519970E+02 3.140920E+00 64 40 1.737690E-01 1.452470E+02 3.023710E+00 64 41 1.765040E-01 1.487260E+02 2.948630E+00 64 42 1.792400E-01 1.407700E+02 2.706030E+00 64 43 1.819750E-01 1.405850E+02 2.720730E+00 64 44 1.847100E-01 1.394880E+02 2.571800E+00 64 45 1.874450E-01 1.353570E+02 2.507980E+00 64 46 1.901800E-01 1.314830E+02 2.339870E+00 64 47 1.929150E-01 1.326170E+02 2.297840E+00 64 48 1.956500E-01 1.304920E+02 2.290230E+00 64 49 1.983850E-01 1.274360E+02 2.154040E+00 64 50 2.011200E-01 1.257840E+02 2.072790E+00 64 51 2.038550E-01 1.185010E+02 2.030710E+00 64 52 2.065900E-01 1.224020E+02 1.916450E+00 64 53 2.093250E-01 1.190880E+02 1.864590E+00 64 54 2.120610E-01 1.138360E+02 1.775220E+00 64 55 2.147960E-01 1.154700E+02 1.743150E+00 64 56 2.175310E-01 1.098510E+02 1.690100E+00 64 57 2.202660E-01 1.090310E+02 1.654200E+00 64 58 2.230010E-01 1.098530E+02 1.609410E+00 64 59 2.257360E-01 1.080610E+02 1.575950E+00 64 60 2.284710E-01 1.065050E+02 1.554880E+00 64 61 2.312060E-01 1.022620E+02 1.509020E+00 64 62 2.339410E-01 1.047730E+02 1.498230E+00 64 63 2.366760E-01 9.926210E+01 1.432690E+00 64 64 2.394110E-01 1.003390E+02 1.440470E+00 64 65 2.421460E-01 9.689090E+01 1.423170E+00 64 66 2.448820E-01 9.566530E+01 1.376160E+00 64 67 2.476170E-01 9.454590E+01 1.369830E+00 64 68 2.503520E-01 9.238730E+01 1.326750E+00 64 69 2.530870E-01 9.221470E+01 1.342630E+00 64 70 2.558220E-01 8.868580E+01 1.300590E+00 64 71 2.585570E-01 8.820850E+01 1.274700E+00 64 72 2.612920E-01 8.780080E+01 1.277460E+00 64 73 2.640270E-01 8.698640E+01 1.258700E+00 64 74 2.667620E-01 8.446450E+01 1.237570E+00 64 75 2.694970E-01 8.370220E+01 1.216480E+00 64 76 2.722320E-01 8.319730E+01 1.202320E+00 64 77 2.749680E-01 7.996770E+01 1.203070E+00 64 78 2.777030E-01 8.091070E+01 1.182010E+00 64 79 2.804380E-01 7.752440E+01 1.177780E+00 64 80 2.831730E-01 7.602580E+01 1.116370E+00 64 81 2.859080E-01 7.421500E+01 1.138320E+00 64 82 2.886430E-01 7.187790E+01 1.125660E+00 64 83 2.913780E-01 7.270360E+01 1.085220E+00 64 84 2.941130E-01 7.070100E+01 1.101680E+00 64 85 2.968480E-01 7.024610E+01 1.070320E+00 64 86 2.995830E-01 7.061690E+01 1.094290E+00 64 87 3.023180E-01 7.116900E+01 1.075940E+00 64 88 3.050530E-01 6.873110E+01 1.047640E+00 64 89 3.077890E-01 6.761310E+01 1.060700E+00 64 90 3.105240E-01 6.597630E+01 1.033510E+00 64 91 3.132590E-01 6.469430E+01 1.050000E+00 64 92 3.159940E-01 6.465700E+01 1.021390E+00 64 93 3.187290E-01 6.235910E+01 1.005660E+00 64 94 3.214640E-01 6.454340E+01 1.043920E+00 64 95 3.241990E-01 6.346040E+01 9.984130E-01 64 96 3.269340E-01 5.999380E+01 1.004550E+00 64 97 3.296690E-01 6.088290E+01 9.912190E-01 64 98 3.324040E-01 5.903100E+01 9.660270E-01 64 99 3.351390E-01 5.799460E+01 9.963340E-01 64 100 3.378750E-01 5.757700E+01 9.750240E-01 64 101 3.406100E-01 5.634100E+01 9.579290E-01 64 102 3.433450E-01 5.701850E+01 9.647360E-01 64 103 3.460800E-01 5.301980E+01 9.467680E-01 64 104 3.488150E-01 5.529070E+01 9.518920E-01 64 105 3.515500E-01 5.480740E+01 9.366100E-01 64 106 3.542850E-01 5.359020E+01 9.333680E-01 64 107 3.570200E-01 5.314100E+01 9.316360E-01 64 108 3.597550E-01 5.163210E+01 9.345600E-01 64 109 3.624900E-01 5.227300E+01 9.108880E-01 64 110 3.652250E-01 5.149680E+01 9.099200E-01 64 111 3.679600E-01 5.155650E+01 9.256340E-01 64 112 3.706960E-01 5.082050E+01 9.081360E-01 64 113 3.734310E-01 4.992050E+01 9.028910E-01 64 114 3.761660E-01 4.898740E+01 8.798620E-01 64 115 3.789010E-01 4.820290E+01 8.940700E-01 64 116 3.816360E-01 4.663390E+01 8.799910E-01 64 117 3.843710E-01 4.626780E+01 8.875370E-01 64 118 3.871060E-01 4.688540E+01 8.728150E-01 64 119 3.898410E-01 4.435360E+01 8.674270E-01 64 120 3.925760E-01 4.455380E+01 8.810770E-01 64 121 3.953110E-01 4.530040E+01 8.627450E-01 64 122 3.980460E-01 4.357350E+01 8.584310E-01 64 123 4.007810E-01 4.450850E+01 8.593910E-01 64 124 4.035170E-01 4.251890E+01 8.354440E-01 64 125 4.062520E-01 4.367800E+01 8.734730E-01 64 126 4.089870E-01 4.148620E+01 8.293360E-01 64 127 4.117220E-01 4.157020E+01 8.334560E-01 64 128 4.144570E-01 4.117480E+01 8.381470E-01 64 129 4.171920E-01 4.038800E+01 8.265330E-01 64 130 4.199270E-01 4.033640E+01 8.332010E-01 64 131 4.226620E-01 3.892970E+01 8.105810E-01 64 132 4.253970E-01 3.941470E+01 8.175230E-01 64 133 4.281320E-01 3.955200E+01 8.168120E-01 64 134 4.308670E-01 3.921270E+01 8.068160E-01 64 135 4.336030E-01 3.813730E+01 8.079810E-01 64 136 4.363380E-01 3.735570E+01 7.940990E-01 64 137 4.390730E-01 3.728450E+01 8.131720E-01 64 138 4.418080E-01 3.517020E+01 7.821740E-01 64 139 4.445430E-01 3.555270E+01 7.788140E-01 64 140 4.472780E-01 3.535030E+01 7.954500E-01 64 141 4.500130E-01 3.378340E+01 7.712080E-01 64 142 4.527480E-01 3.497000E+01 7.880740E-01 64 143 4.554830E-01 3.340320E+01 7.707450E-01 64 144 4.582180E-01 3.383720E+01 7.646920E-01 64 145 4.609530E-01 3.242080E+01 7.689420E-01 64 146 4.636880E-01 3.294420E+01 7.637380E-01 64 147 4.664240E-01 3.221390E+01 7.596410E-01 64 148 4.691590E-01 3.118750E+01 7.548410E-01 64 149 4.718940E-01 3.096650E+01 7.621710E-01 64 150 4.746290E-01 3.064180E+01 7.490690E-01 64 151 4.773640E-01 2.984350E+01 7.526050E-01 64 152 4.800990E-01 2.996580E+01 7.403420E-01 64 153 4.828340E-01 2.983520E+01 7.384310E-01 64 154 4.855690E-01 2.820030E+01 7.379670E-01 64 155 4.883040E-01 2.895350E+01 7.394860E-01 64 156 4.910390E-01 2.851130E+01 7.167590E-01 64 157 4.937740E-01 2.880500E+01 7.280960E-01 64 158 4.965090E-01 2.734920E+01 7.261890E-01 64 159 4.992450E-01 2.638440E+01 7.210180E-01 64 160 5.019800E-01 2.736550E+01 7.132280E-01 64 161 5.047150E-01 2.662210E+01 7.206390E-01 64 162 5.074500E-01 2.605810E+01 7.128320E-01 64 163 5.101850E-01 2.458590E+01 7.084980E-01 64 164 5.129200E-01 2.545520E+01 7.017160E-01 64 165 5.156550E-01 2.470410E+01 6.975720E-01 64 166 5.183900E-01 2.490670E+01 7.050590E-01 64 167 5.211250E-01 2.390820E+01 7.043500E-01 64 168 5.238600E-01 2.372640E+01 7.006990E-01 64 169 5.265950E-01 2.234660E+01 6.832950E-01 64 170 5.293310E-01 2.262010E+01 6.867090E-01 64 171 5.320660E-01 2.198780E+01 6.852660E-01 64 172 5.348010E-01 2.189440E+01 6.854060E-01 64 173 5.375360E-01 2.348880E+01 6.795420E-01 64 174 5.402710E-01 2.229950E+01 6.752860E-01 64 175 5.430060E-01 2.103580E+01 6.774730E-01 64 176 5.457410E-01 2.121900E+01 6.810540E-01 64 177 5.484760E-01 2.033670E+01 6.666290E-01 64 178 5.512110E-01 2.103330E+01 6.753100E-01 64 179 5.539460E-01 1.986160E+01 6.620910E-01 64 180 5.566810E-01 2.029690E+01 6.737530E-01 64 181 5.594160E-01 1.894300E+01 6.580280E-01 64 182 5.621520E-01 1.936400E+01 6.506510E-01 64 183 5.648870E-01 1.839330E+01 6.695240E-01 64 184 5.676220E-01 1.730040E+01 6.512220E-01 64 185 5.703570E-01 1.840750E+01 6.630530E-01 64 186 5.730920E-01 1.774880E+01 6.510360E-01 64 187 5.758270E-01 1.702130E+01 6.318070E-01 64 188 5.785620E-01 1.686530E+01 6.503560E-01 64 189 5.812970E-01 1.558930E+01 6.286120E-01 64 190 5.840320E-01 1.688480E+01 6.643740E-01 64 191 5.867670E-01 1.645500E+01 6.351970E-01 64 192 5.895020E-01 1.665000E+01 6.459490E-01 64 193 5.922380E-01 1.525690E+01 6.435180E-01 64 194 5.949730E-01 1.538590E+01 6.178400E-01 64 195 5.977080E-01 1.660530E+01 6.358250E-01 64 196 6.004430E-01 1.525190E+01 6.273880E-01 64 197 6.031780E-01 1.514980E+01 6.362180E-01 64 198 6.059130E-01 1.536700E+01 6.332410E-01 64 199 6.086480E-01 1.415880E+01 6.353480E-01 64 200 6.113830E-01 1.474260E+01 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