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1buq

SOLUTION STRUCTURE OF DELTA-5-3-KETOSTEROID ISOMERASE COMPLEXED WITH THE STEROID 19-NORTESTOSTERONE-HEMISUCCINATE

Method: SOLUTION NMR Dmax: 62.8 Å Quality: GOOD

SAXS Profile

SAXS profile for 1buq

P(r) Distribution

P(r) distribution for 1buq

1. Structure Basics

entry_id1buq
deposition_date1998-09-04
titleSOLUTION STRUCTURE OF DELTA-5-3-KETOSTEROID ISOMERASE COMPLEXED WITH THE STEROID 19-NORTESTOSTERONE-HEMISUCCINATE
keywordsKETOSTEROID ISOMERASE-19NTHS, ENZYME-SUBSTRATE COMPLEX, ENZYMES, ISOMERASE; ISOMERASE
methodSOLUTION NMR

Download Data

2. SAXS Parameters (CRYSOL)

rg_guinier19.19
rg_electron18.68
i02265440000.00
molecular_weight412100.0 kDa
excluded_volume518300 ų
envelope_volume59144 ų
shell_volume23747 ų
envelope_diameter72.3
shell_rg27.73
envelope_rg20.76
shape_rg18.66
total_rg18.91
total_atoms57870
n_residues3750
n_harmonics20
q_range— – 0.5000 −1
n_points101
shell_typedirectional
solvent_density0.3340 e/ų
contrast_shell0.0300 e/ų
crysol_version4.1.3

3. P(r) Analysis (GNOM)

dmax62.8
rg_real19.13
rg_real_error0.36
i0_real2.2650e+09
i0_real_error2.9610e+07
rg_reciprocal19.14
i0_reciprocal2265000000.0000
total_estimate0.8137
solution_quality GOOD a GOOD solution
n_peaks1
r_peak_primary62.0
skewness0.260
kurtosis-0.348
angular_range— – 0.4150 −1
current_alpha0.0000
highest_alpha2061000.0000
n_real_points73
gnom_version4.1.3
quality_criteria AN1: 0.000; Oscil: 0.859; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.998; Smooth: 0.000

4. Crystallography & Experiment

5. Entities & Polymer Info (2)

6. Citations (1)

7. Files & Curves (10)