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1dcq

CRYSTAL STRUCTURE OF THE ARF-GAP DOMAIN AND ANKYRIN REPEATS OF PAPBETA.

Method: X-RAY DIFFRACTION D_max: 67.4 Å Quality: GOOD

SAXS Profile

P(r) Distribution

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1. Structure Basics

entry_id	1dcq
deposition_date	1999-11-05
title	CRYSTAL STRUCTURE OF THE ARF-GAP DOMAIN AND ANKYRIN REPEATS OF PAPBETA.
keywords	ZINC-BINDING MODULE, ANKYRIN REPEATS, METAL BINDING PROTEIN; METAL BINDING PROTEIN
method	X-RAY DIFFRACTION

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Download Data

SAXS curve (.dat) P(r) distribution (.pr.out) Structure (CIF)

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2. SAXS Parameters (CRYSOL)

rg_guinier	19.96 Å
rg_electron	18.98 Å
i0	16407300.00
molecular_weight	29691.0 kDa
excluded_volume	36775 Å³
envelope_volume	41818 Å³
shell_volume	18717 Å³
envelope_diameter	68.0 Å
shell_rg	24.99 Å
envelope_rg	19.17 Å
shape_rg	18.98 Å
total_rg	19.80 Å
total_atoms	2074
n_residues	276
n_harmonics	20
q_range	— – 0.5000 Å⁻¹
n_points	101
shell_type	directional
solvent_density	0.3340 e/Å³
contrast_shell	0.0300 e/Å³
crysol_version	4.1.3

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3. P(r) Analysis (GNOM)

dmax	67.4 Å
rg_real	19.91 Å
rg_real_error	0.44 Å
i0_real	1.6410e+07
i0_real_error	2.0010e+05
rg_reciprocal	19.92 Å
i0_reciprocal	16410000.0000
total_estimate	0.8055
solution_quality	GOOD a GOOD solution
n_peaks	2
r_peak_primary	22.8 Å
skewness	0.292
kurtosis	-0.350
angular_range	— – 0.4000 Å⁻¹
current_alpha	0.0000
highest_alpha	3630000.0000
n_real_points	72
gnom_version	4.1.3
quality_criteria	AN1: 0.000; Oscil: 0.832; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.972; Smooth: 0.000

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4. Crystallography & Experiment

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5. Entities & Polymer Info (3)

Entity 1 polymer

description	PYK2-ASSOCIATED PROTEIN BETA
formula_weight	30889.3 kDa
src_method	man
entity_count	1

Polymer

type	polypeptide(L)
strand_id	A
atom_count	2169

MELTKEIISEVQRMTGNDVCCDCGAPDPTWLSTNLGILTCIECSGIHRELGVHYSRMQSLTLDVLGTSELLLAKNIGNAGFNEIMECCLPSEDPVKPNPGSDMIARKDYITAKYMERRYARKKHADTAAKLHSLCEAVKTRDIFGLLQAYADGVDLTEKIPLANGHEPDETALHLAVRSVDRTSLHIVDFLVQNSGNLDKQTGKGSTALHYCCLTDNAECLKLLLRGKASIEIANESGETPLDIAKRLKHEHCEELLTQALSGRFNSHVHVEYEWRLL

Source

organism	Mus musculus
common_name	house mouse
ncbi_taxonomy_id	10090
host_organism	Escherichia coli

Entity 2 non-polymer

description	ZINC ION
formula_weight	65.4 kDa
src_method	syn
entity_count	1

Entity 3 water

description	water
formula_weight	18.0 kDa
src_method	nat
entity_count	95

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6. Citations (2)

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length_a	73.935 Å
length_b	132.208 Å
length_c	59.817 Å
angle_alpha	90.00 °
angle_beta	90.00 °
angle_gamma	90.00 °
z_pdb	8

space_group	C 2 2 21
int_tables_number	20
crystal_system	—

resolution	2.100 Å
resolution_low	25.000 Å
r_factor	0.2300
r_work	0.2130
r_free	0.2660

fit	/app/data/saxs_computation/dc/1dcq/1dcq.fit
pddf	/app/data/pr_computation/dc/1dcq/1dcq.pr.out
profile	/app/data/saxs_computation/dc/1dcq/1dcq.dat

CRYSTAL STRUCTURE OF THE ARF-GAP DOMAIN AND ANKYRIN REPEATS OF PAPBETA.

SAXS Profile

P(r) Distribution

1. Structure Basics

Download Data

2. SAXS Parameters (CRYSOL)

3. P(r) Analysis (GNOM)

4. Crystallography & Experiment

Unit Cell

Symmetry

Refinement

Diffraction