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1dfz

NMR STRUCTURE OF CONTRYPHAN-SM CYCLIC PEPTIDE (MINOR FORM-TRANS)

Method: SOLUTION NMR Dmax: 19.1 Å Quality: REASONABLE

SAXS Profile

SAXS profile for 1dfz

P(r) Distribution

P(r) distribution for 1dfz

1. Structure Basics

entry_id1dfz
deposition_date1999-11-22
titleNMR STRUCTURE OF CONTRYPHAN-SM CYCLIC PEPTIDE (MINOR FORM-TRANS)
keywordsCYCLIC PEPTIDE, DISULFIDE BRIDGE, D-TRYPTOPHAN, CIS-TRANS ISOMERISM, CONTRYPHAN, TOXIN; TOXIN
methodSOLUTION NMR

Download Data

2. SAXS Parameters (CRYSOL)

rg_guinier4.42
rg_electron5.49
i06411940.00
molecular_weight19884.0 kDa
excluded_volume24302 ų
envelope_volume2046 ų
shell_volume3179 ų
envelope_diameter20.6
shell_rg10.62
envelope_rg6.85
shape_rg5.52
total_rg5.72
total_atoms2520
n_residues100
n_harmonics20
q_range— – 0.5000 −1
n_points101
shell_typedirectional
solvent_density0.3340 e/ų
contrast_shell0.0300 e/ų
crysol_version4.1.3

3. P(r) Analysis (GNOM)

dmax19.1
rg_real4.38
rg_real_error0.39
i0_real6.4120e+06
i0_real_error5.3320e+04
rg_reciprocal4.38
i0_reciprocal6412000.0000
total_estimate0.7305
solution_quality REASONABLE a REASONABLE solution
n_peaks3
r_peak_primary5.8
skewness-0.114
kurtosis-0.919
angular_range— – 0.5000 −1
current_alpha0.0000
highest_alpha201.9000
n_real_points80
gnom_version4.1.3
quality_criteria AN1: 0.000; Oscil: 0.455; Stabil: 0.984; Sysdev: 1.000; Positv: 1.000; Valcen: 0.492; Smooth: 0.685

4. Crystallography & Experiment

5. Entities & Polymer Info (1)

6. Citations (1)

7. Files & Curves (10)