R16-24 human dystrophin fragment

{
  "code": "SASDFZ4",
  "status": "Published",
  "type_of_curve": "Single concentration",
  "angular_unit": "1/A",
  "project": {
    "title": "Dystrophin SAXS data",
    "publication": null,
    "status": "released",
    "submitted_date": "2019-03-30",
    "released_date": "2023-03-30"
  },
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  "intensities_data": "https://www.sasbdb.org/media/intensities_files/SASDFZ4.dat",
  "intensities_log_plot": "https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDFZ4_dat_img.png",
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  "sascif_data": "https://www.sasbdb.org/media/sascif/sascif_files/SASDFZ4.sascif",
  "experiment": {
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      "detector": {
        "type": "CCD",
        "name": "AVIEX PCCD170170",
        "resolution": null
      },
      "name": "SOLEIL",
      "city": "Saint-Aubin",
      "country": "France",
      "beamline_name": "SWING",
      "beam_geometry": "",
      "type_of_source": "X-ray synchrotron",
      "point_source": null,
      "line_collimation": null,
      "sample_path_length": null,
      "line_collimation_slitlength": null,
      "line_collimation_integrationwidth": null,
      "xray_energy": null,
      "beam_profile_ah": null,
      "beam_profile_al": null
    },
    "sample": {
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        {
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          "short_name": null,
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          "organism": null,
          "uniprot_code": "P11532",
          "uniprot_range_first": 1990,
          "uniprot_range_last": 3040,
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          "molecular_type": "protein",
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          "mw": 126.616,
          "total_mw": 126.616,
          "number_molecules": 1,
          "complex_state": false,
          "deuteration": null,
          "molecule_source": "biological",
          "molecule_description": null
        }
      ],
      "buffer": {
        "name": "NaP 20 mM, NaCl 300 mM, EDTA 1 mM, Glycérol 2%",
        "concentration_unit": null,
        "comment": null,
        "additive": null,
        "concentration": null,
        "pka": null,
        "ph": 7.5,
        "deuteration": null
      },
      "purity_method": null,
      "name": "R16-24 human dystrophin fragment",
      "ext_coefficient": null,
      "contrast": null,
      "specific_vol": null,
      "dry_vol": null,
      "absorbption": null,
      "deuteration": null,
      "mixture": null
    },
    "contributor": [
      {
        "affiliation": [
          {
            "short_name": null,
            "address": "France",
            "full_name": "University of Lorraine",
            "webpage": "http://welcome.univ-lorraine.fr/"
          }
        ],
        "contributor_name": "Raphael",
        "contributor_surname": "Dos Santos Morais",
        "orcid": ""
      }
    ],
    "concentration_method": null,
    "concentration_unit": null,
    "date": "2016-12-17",
    "storage_temperature": null,
    "cell_temperature": 20.0,
    "exposure_time": 0.75,
    "number_of_frames": 51,
    "wavelength": 0.1033,
    "sample_detector_distance": 2.0,
    "concentration_min": null,
    "concentration_max": null,
    "sample_volume": null,
    "flow_rate": null,
    "s_min": 0.041,
    "s_max": 5.953,
    "total_exposure_time": null,
    "seccolumn": null
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  "fits": [],
  "estimated_volume_method": null,
  "pddf_software": "ATSAS GNOM",
  "pddf_software_version": "4.6",
  "i0_calibration_standard": null,
  "description": "SEC-SAXS was performed at 20°C using the following parameters: Column: BioSEC5-500Å (4.6 mm id * 300 mm); Flow rate: 0.3 mL/min; Sample injection concentration: 4.5 mg/mL; Injection volume: 50μL. The data were collected through the SEC peak of the protein as a series of 38 x 0.75 second exposures.\r\nThe experimental molecular weight was determined from SEC-MALS (130 kDa).",
  "experiment_description": "Synchrotron SAXS data from solutions of the R16-24 human dystrophin fragment in NaP 20 mM, NaCl 300 mM, EDTA 1 mM, glycerol 2%, pH 7.5 were collected using size-exclusion chromatography SAXS (SEC-SAXS) on the SWING beam line SOLEIL (Saint-Aubin, France) using a CCD AVIEX PCCD170170 detector at a sample-detector distance of 2 m and at a wavelength of λ = 0.1033 nm (l(s) vs s, where s = 4πsinθ/λ, and 2θ is the scattering angle). The data were normalized to the intensity of the transmitted beam and radially averaged; the scattering of the solvent-blank was subtracted.",
  "tags": [],
  "intensity_unit": "arbitrary",
  "experimental_mw": 130.0,
  "experimental_mw_error": null,
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  "guinier_i0_mw_error": null,
  "porod_mw": null,
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  "pddf_i0_error": null,
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  "pddf_rg_error": null,
  "guinier_rg": 9.28,
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  "pddf_dmax": 34.0,
  "pddf_dmax_error": null,
  "porod_volume": null,
  "porod_volume_error": null,
  "estimated_volume": null,
  "estimated_volume_error": null,
  "guinier_point_first": null,
  "guinier_point_last": null,
  "pddf_point_first": null,
  "pddf_point_last": null,
  "i0_calibration_standard_data": null,
  "intensities_log_log_plot": "SASDFZ4_datloglog_img.png",
  "symmetry": null,
  "last_modified": "2023-06-20T14:43:31.013409+02:00",
  "bragg_peak": []
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