STRUCTURE OF ADENYLOSUCCINATE SYNTHETASE PH 7 AT 25 DEGREES CELSIUS

Method: X-RAY DIFFRACTION D_max: 89.6 Å Quality: REASONABLE

SAXS Profile

P(r) Distribution

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1. Structure Basics

entry_id	1ade
deposition_date	1995-09-14
title	STRUCTURE OF ADENYLOSUCCINATE SYNTHETASE PH 7 AT 25 DEGREES CELSIUS
keywords	PURINE NUCLEOTIDE BIOSYNTHESIS, LIGASE, GTP-HYDROLYZING ENZYMES, LIGASE (SYNTHETASE); LIGASE (SYNTHETASE)
method	X-RAY DIFFRACTION

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Download Data

SAXS curve (.dat) P(r) distribution (.pr.out) Structure (CIF)

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2. SAXS Parameters (CRYSOL)

rg_guinier	28.46 Å
rg_electron	27.50 Å
i0	143448000.00
molecular_weight	94408.0 kDa
excluded_volume	118210 Å³
envelope_volume	142390 Å³
shell_volume	41577 Å³
envelope_diameter	95.7 Å
shell_rg	36.15 Å
envelope_rg	27.51 Å
shape_rg	27.49 Å
total_rg	28.34 Å
total_atoms	8128
n_residues	862
n_harmonics	20
q_range	— – 0.5000 Å⁻¹
n_points	101
shell_type	directional
solvent_density	0.3340 e/Å³
contrast_shell	0.0300 e/Å³
crysol_version	4.1.3

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3. P(r) Analysis (GNOM)

dmax	89.6 Å
rg_real	28.27 Å
rg_real_error	0.33 Å
i0_real	1.4340e+08
i0_real_error	1.6450e+06
rg_reciprocal	28.33 Å
i0_reciprocal	143500000.0000
total_estimate	0.7222
solution_quality	REASONABLE a REASONABLE solution
n_peaks	2
r_peak_primary	35.2 Å
skewness	0.188
kurtosis	-0.427
angular_range	— – 0.2800 Å⁻¹
current_alpha	0.0001
highest_alpha	55960000.0000
n_real_points	57
gnom_version	4.1.3
quality_criteria	AN1: 0.000; Oscil: 0.892; Stabil: 1.000; Sysdev: 0.242; Positv: 1.000; Valcen: 0.990; Smooth: 0.991

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4. Crystallography & Experiment

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5. Entities & Polymer Info (2)

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6. Citations (2)

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length_a	73.260 Å
length_b	72.180 Å
length_c	82.900 Å
angle_alpha	90.00 °
angle_beta	108.17 °
angle_gamma	90.00 °
z_pdb	4

space_group	P 1 21 1
int_tables_number	4
crystal_system	—

resolution	2.000 Å
resolution_low	5.000 Å
r_factor	0.1990
r_work	0.1990
r_free	—

description	ADENYLOSUCCINATE SYNTHETASE
formula_weight	47269.6 kDa
ec_number	6.3.4.4
src_method	nat
entity_count	2

type	polypeptide(L)
strand_id	A,B
atom_count	9988

STRUCTURE OF ADENYLOSUCCINATE SYNTHETASE PH 7 AT 25 DEGREES CELSIUS

SAXS Profile

P(r) Distribution

1. Structure Basics

Download Data

2. SAXS Parameters (CRYSOL)

3. P(r) Analysis (GNOM)

4. Crystallography & Experiment

Unit Cell

Symmetry

Refinement

Diffraction

5. Entities & Polymer Info (2)

Entity 1 polymer

Polymer

Entity 2 water

6. Citations (2)

7. Files & Curves (10)

Files (7)

Curves (3)

description	water
formula_weight	18.0 kDa
src_method	nat
entity_count	574

fit	/app/data/saxs_computation/ad/1ade/1ade.fit
pddf	/app/data/pr_computation/ad/1ade/1ade.pr.out
profile	/app/data/saxs_computation/ad/1ade/1ade.dat