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1bku

EFFECTS OF GLYCOSYLATION ON THE STRUCTURE AND DYNAMICS OF EEL CALCITONIN, NMR, 10 STRUCTURES

Method: SOLUTION NMR Dmax: 54.2 Å Quality: REASONABLE

SAXS Profile

SAXS profile for 1bku

P(r) Distribution

P(r) distribution for 1bku

1. Structure Basics

entry_id1bku
deposition_date1998-07-13
titleEFFECTS OF GLYCOSYLATION ON THE STRUCTURE AND DYNAMICS OF EEL CALCITONIN, NMR, 10 STRUCTURES
keywordsHORMONE, CALCIUM-REGULATING HORMONE; HORMONE
methodSOLUTION NMR

Download Data

2. SAXS Parameters (CRYSOL)

rg_guinier12.73
rg_electron12.69
i019432200.00
molecular_weight34179.0 kDa
excluded_volume42343 ų
envelope_volume13304 ų
shell_volume8446 ų
envelope_diameter55.9
shell_rg19.15
envelope_rg15.98
shape_rg12.63
total_rg13.33
total_atoms4810
n_residues320
n_harmonics20
q_range— – 0.5000 −1
n_points101
shell_typedirectional
solvent_density0.3340 e/ų
contrast_shell0.0300 e/ų
crysol_version4.1.3

3. P(r) Analysis (GNOM)

dmax54.2
rg_real13.04
rg_real_error0.77
i0_real1.9430e+07
i0_real_error2.4500e+05
rg_reciprocal13.02
i0_reciprocal19430000.0000
total_estimate0.5900
solution_quality REASONABLE a REASONABLE solution
n_peaks3
r_peak_primary8.2
skewness0.644
kurtosis-0.101
angular_range— – 0.5000 −1
current_alpha0.0000
highest_alpha12000.0000
n_real_points80
gnom_version4.1.3
quality_criteria AN1: 0.000; Oscil: 0.219; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.011; Smooth: 0.000

4. Crystallography & Experiment

5. Entities & Polymer Info (1)

6. Citations (1)

7. Files & Curves (10)