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1did

OBSERVATIONS OF REACTION INTERMEDIATES AND THE MECHANISM OF ALDOSE-KETOSE INTERCONVERSION BY D-XYLOSE ISOMERASE

Method: X-RAY DIFFRACTION Dmax: 99.1 Å Quality: GOOD

SAXS Profile

SAXS profile for 1did

P(r) Distribution

P(r) distribution for 1did

1. Structure Basics

entry_id1did
deposition_date1992-06-04
titleOBSERVATIONS OF REACTION INTERMEDIATES AND THE MECHANISM OF ALDOSE-KETOSE INTERCONVERSION BY D-XYLOSE ISOMERASE
keywordsISOMERASE(INTRAMOLECULAR OXIDOREDUCTASE); ISOMERASE(INTRAMOLECULAR OXIDOREDUCTASE)
methodX-RAY DIFFRACTION

Download Data

2. SAXS Parameters (CRYSOL)

rg_guinier30.72
rg_electron29.73
i0121961000.00
molecular_weight86146.0 kDa
excluded_volume107060 ų
envelope_volume141820 ų
shell_volume39382 ų
envelope_diameter101.4
shell_rg37.43
envelope_rg29.60
shape_rg29.73
total_rg30.43
total_atoms6080
n_residues786
n_harmonics20
q_range— – 0.5000 −1
n_points101
shell_typedirectional
solvent_density0.3340 e/ų
contrast_shell0.0300 e/ų
crysol_version4.1.3

3. P(r) Analysis (GNOM)

dmax99.1
rg_real30.64
rg_real_error0.59
i0_real1.2200e+08
i0_real_error1.5780e+06
rg_reciprocal30.68
i0_reciprocal122000000.0000
total_estimate0.8260
solution_quality GOOD a GOOD solution
n_peaks2
r_peak_primary34.3
skewness0.220
kurtosis-0.518
angular_range— – 0.2600 −1
current_alpha0.0000
highest_alpha38870000.0000
n_real_points53
gnom_version4.1.3
quality_criteria AN1: 0.000; Oscil: 0.912; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.998; Smooth: 0.000

4. Crystallography & Experiment

5. Entities & Polymer Info (4)

6. Citations (3)

7. Files & Curves (10)