1dlc

CRYSTAL STRUCTURE OF INSECTICIDAL DELTA-ENDOTOXIN FROM BACILLUS THURINGIENSIS AT 2.5 ANGSTROMS RESOLUTION

Method: X-RAY DIFFRACTION Dmax: 88.8 Å Quality: GOOD

SAXS 散射曲线 SAXS Profile

SAXS profile for 1dlc

P(r) 距离分布 P(r) Distribution

P(r) distribution for 1dlc
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1. 结构基本信息 1. Structure Basics

条目编号 entry_id1dlc
沉积日期 deposition_date1994-06-22
结构标题 titleCRYSTAL STRUCTURE OF INSECTICIDAL DELTA-ENDOTOXIN FROM BACILLUS THURINGIENSIS AT 2.5 ANGSTROMS RESOLUTION
关键词 keywordsTOXIN; TOXIN
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier26.75
回转半径 Rg (电子) rg_electron25.56
零角强度 I(0) i069821300.00
分子量 molecular_weight66241.0 kDa
排除体积 excluded_volume83080 ų
包络体积 envelope_volume97729 ų
水化壳体积 shell_volume31831 ų
包络直径 envelope_diameter93.4
壳层 Rg shell_rg32.92
包络 Rg envelope_rg25.76
形状 Rg shape_rg25.57
总 Rg total_rg26.29
总原子数 total_atoms4690
残基数 n_residues584
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax88.8
Rg (实空间) rg_real26.68
Rg 误差 (实空间) rg_real_error0.67
I(0) (实空间) i0_real6.9820e+07
I(0) 误差 (实空间) i0_real_error1.0610e+06
Rg (倒空间) rg_reciprocal26.70
I(0) (倒空间) i0_reciprocal69820000.0000
解质量估计 total_estimate0.8822
解质量评级 solution_quality GOOD a GOOD solution
P(r) 峰数 n_peaks2
主峰位置 r_peak_primary31.6
偏度 Skewness skewness0.288
峰度 Kurtosis kurtosis-0.294
角度范围 angular_range— – 0.2950 −1
当前正则化参数 α current_alpha0.0000
最高正则化参数 α highest_alpha15750000.0000
实空间数据点数 n_real_points60
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.853; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.990; Smooth: 0.917

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (2)

6. 折叠分类 (SCOP + CATH) 6 domains

SCOP 2.08 (3 domains)

结构域编号 domain_idd1dlca1
类 Class classb — All beta proteins
折叠类型 Fold foldb.18 — Galactose-binding domain-like
超家族 Superfamily superfamilyb.18.1 — Galactose-binding domain-like
家族 Family familyb.18.1.3 — delta-Endotoxin, C-terminal domain
结构域编号 domain_idd1dlca2
类 Class classb — All beta proteins
折叠类型 Fold foldb.77 — beta-Prism I
超家族 Superfamily superfamilyb.77.2 — delta-Endotoxin (insectocide), middle domain
家族 Family familyb.77.2.1 — delta-Endotoxin (insectocide), middle domain
结构域编号 domain_idd1dlca3
类 Class classf — Membrane and cell surface proteins and peptides
折叠类型 Fold foldf.1 — Toxins' membrane translocation domains
超家族 Superfamily superfamilyf.1.3 — delta-Endotoxin (insectocide), N-terminal domain
家族 Family familyf.1.3.1 — delta-Endotoxin (insectocide), N-terminal domain

CATH v4.4 (3 domains)

结构域编号 domain_id1dlcA01
类 Class class1 — Mainly Alpha
架构 Architecture architecture20 — Up-down Bundle
拓扑 Topology topology190 — Delta-Endotoxin; domain 1
同源超家族 H-superfamily homologous superfamily10 — Pesticidal crystal protein, N-terminal domain
结构域编号 domain_id1dlcA02
类 Class class2 — Mainly Beta
架构 Architecture architecture60 — Sandwich
拓扑 Topology topology120 — Jelly Rolls
同源超家族 H-superfamily homologous superfamily260 — Galactose-binding domain-like
结构域编号 domain_id1dlcA03
类 Class class2 — Mainly Beta
架构 Architecture architecture100 — Aligned Prism
拓扑 Topology topology10 — Vitelline Membrane Outer Layer Protein I, subunit A
同源超家族 H-superfamily homologous superfamily10 — Pesticidal crystal protein, central domain

7. 引用文献 (2)

8. 文件与曲线 (10)