CRYSTAL STRUCTURE OF SULFOLOBUS SOLFATARICUS GLYCOSYLTREHALOSE TREHALOHYDROLASE

Method: X-RAY DIFFRACTION D_max: 89.0 Å Quality: GOOD

SAXS Profile

P(r) Distribution

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1. Structure Basics

entry_id	1eh9
deposition_date	2000-02-19
title	CRYSTAL STRUCTURE OF SULFOLOBUS SOLFATARICUS GLYCOSYLTREHALOSE TREHALOHYDROLASE
keywords	trehalose, trehalohydrolase, Sulfolobus solfataricus, alpha/beta barrel, calcium binding, covalent dimer, HYDROLASE; HYDROLASE
method	X-RAY DIFFRACTION

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Download Data

SAXS curve (.dat) P(r) distribution (.pr.out) Structure (CIF)

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2. SAXS Parameters (CRYSOL)

rg_guinier	25.60 Å
rg_electron	24.77 Å
i0	63432700.00
molecular_weight	64052.0 kDa
excluded_volume	80572 Å³
envelope_volume	90414 Å³
shell_volume	30619 Å³
envelope_diameter	92.3 Å
shell_rg	32.13 Å
envelope_rg	24.98 Å
shape_rg	24.74 Å
total_rg	25.61 Å
total_atoms	4541
n_residues	557
n_harmonics	20
q_range	— – 0.5000 Å⁻¹
n_points	101
shell_type	directional
solvent_density	0.3340 e/Å³
contrast_shell	0.0300 e/Å³
crysol_version	4.1.3

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3. P(r) Analysis (GNOM)

dmax	89.0 Å
rg_real	25.63 Å
rg_real_error	0.57 Å
i0_real	6.3430e+07
i0_real_error	8.7820e+05
rg_reciprocal	25.62 Å
i0_reciprocal	63430000.0000
total_estimate	0.8501
solution_quality	GOOD a GOOD solution
n_peaks	1
r_peak_primary	87.5 Å
skewness	0.496
kurtosis	0.138
angular_range	— – 0.3100 Å⁻¹
current_alpha	0.0000
highest_alpha	14510000.0000
n_real_points	63
gnom_version	4.1.3
quality_criteria	AN1: 0.000; Oscil: 0.698; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.993; Smooth: 0.961

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4. Crystallography & Experiment

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5. Entities & Polymer Info (2)

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6. Citations (1)

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length_a	80.236 Å
length_b	80.236 Å
length_c	281.973 Å
angle_alpha	90.00 °
angle_beta	90.00 °
angle_gamma	120.00 °
z_pdb	6

space_group	P 32 2 1
int_tables_number	154
crystal_system	—

resolution	3.000 Å
resolution_low	20.000 Å
r_factor	—
r_work	—
r_free	—

description	GLYCOSYLTREHALOSE TREHALOHYDROLASE
formula_weight	64741.7 kDa
ec_number	3.2.1.1
src_method	man
entity_count	1

type	polypeptide(L)
strand_id	A
atom_count	4570

CRYSTAL STRUCTURE OF SULFOLOBUS SOLFATARICUS GLYCOSYLTREHALOSE TREHALOHYDROLASE

SAXS Profile

P(r) Distribution

1. Structure Basics

Download Data

2. SAXS Parameters (CRYSOL)

3. P(r) Analysis (GNOM)

4. Crystallography & Experiment

Unit Cell

Symmetry

Refinement

Diffraction

5. Entities & Polymer Info (2)

Entity 1 polymer

Polymer

Source

Entity 2 water

6. Citations (1)

7. Files & Curves (10)

Files (7)

Curves (3)

organism	Sulfolobus solfataricus
ncbi_taxonomy_id	2287
host_organism	Pichia jadinii

description	water
formula_weight	18.0 kDa
src_method	nat
entity_count	29

fit	/app/data/saxs_computation/eh/1eh9/1eh9.fit
pddf	/app/data/pr_computation/eh/1eh9/1eh9.pr.out
profile	/app/data/saxs_computation/eh/1eh9/1eh9.dat