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1euf

BOVINE DUODENASE(NEW SERINE PROTEASE), CRYSTAL STRUCTURE

Method: X-RAY DIFFRACTION D_max: 54.4 Å Quality: GOOD

SAXS Profile

P(r) Distribution

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1. Structure Basics

entry_id	1euf
deposition_date	2000-04-14
title	BOVINE DUODENASE(NEW SERINE PROTEASE), CRYSTAL STRUCTURE
keywords	bovine duodenase, serine protease, dual specificity, HYDROLASE; HYDROLASE
method	X-RAY DIFFRACTION

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Download Data

SAXS curve (.dat) P(r) distribution (.pr.out) Structure (CIF)

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2. SAXS Parameters (CRYSOL)

rg_guinier	17.71 Å
rg_electron	16.50 Å
i0	11764400.00
molecular_weight	24961.0 kDa
excluded_volume	31017 Å³
envelope_volume	35075 Å³
shell_volume	17418 Å³
envelope_diameter	55.3 Å
shell_rg	22.98 Å
envelope_rg	16.76 Å
shape_rg	16.46 Å
total_rg	17.58 Å
total_atoms	1747
n_residues	224
n_harmonics	20
q_range	— – 0.5000 Å⁻¹
n_points	101
shell_type	directional
solvent_density	0.3340 e/Å³
contrast_shell	0.0300 e/Å³
crysol_version	4.1.3

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3. P(r) Analysis (GNOM)

dmax	54.4 Å
rg_real	17.56 Å
rg_real_error	0.31 Å
i0_real	1.1760e+07
i0_real_error	1.3100e+05
rg_reciprocal	17.58 Å
i0_reciprocal	11760000.0000
total_estimate	0.8190
solution_quality	GOOD a GOOD solution
n_peaks	3
r_peak_primary	22.5 Å
skewness	0.083
kurtosis	-0.462
angular_range	— – 0.4500 Å⁻¹
current_alpha	0.0000
highest_alpha	3097000.0000
n_real_points	76
gnom_version	4.1.3
quality_criteria	AN1: 0.000; Oscil: 0.887; Stabil: 0.998; Sysdev: 1.000; Positv: 1.000; Valcen: 0.987; Smooth: 0.000

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4. Crystallography & Experiment

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5. Entities & Polymer Info (4)

Entity 1 polymer

description	DUODENASE
formula_weight	25156.9 kDa
ec_number	3.4.21.-
src_method	nat
entity_count	1

Polymer

type	polypeptide(L)
strand_id	A
atom_count	1816

IIGGHEAKPHSRPYMAFLLFKTSGKSHICGGFLVREDFVLTAAHCLGSSINVTLGAHNIMERERTQQVIPVRRPIPHPDYNDETLANDIMLLKLTRKADITDKVSPINLPRSLAEVKPGMMCSVAGWGRLGVNMPSTDKLQEVDLEVQSEEKCIARFKNYIPFTQICAGDPSKRKNSFSGDSGGPLVCNGVAQGIVSYGRNDGTTPDVYTRISSFLSWIHSTMRRYK

Entity 2 non-polymer

description	2-acetamido-2-deoxy-beta-D-glucopyranose
formula_weight	221.2 kDa
src_method	man
entity_count	1

Entity 3 non-polymer

description	PHOSPHATE ION
formula_weight	95.0 kDa
src_method	syn
entity_count	1

Entity 4 water

description	water
formula_weight	18.0 kDa
src_method	nat
entity_count	69

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6. Citations (1)

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length_a	100.117 Å
length_b	100.117 Å
length_c	39.753 Å
angle_alpha	90.00 °
angle_beta	90.00 °
angle_gamma	120.00 °
z_pdb	6

space_group	P 64
int_tables_number	172
crystal_system	—

resolution	2.400 Å
resolution_low	99.000 Å
r_factor	—
r_work	0.1790
r_free	0.2230

fit	/app/data/saxs_computation/eu/1euf/1euf.fit
pddf	/app/data/pr_computation/eu/1euf/1euf.pr.out
profile	/app/data/saxs_computation/eu/1euf/1euf.dat

BOVINE DUODENASE(NEW SERINE PROTEASE), CRYSTAL STRUCTURE

SAXS Profile

P(r) Distribution

1. Structure Basics

Download Data

2. SAXS Parameters (CRYSOL)

3. P(r) Analysis (GNOM)

4. Crystallography & Experiment

Unit Cell

Symmetry

Refinement

Diffraction