1fcj

CRYSTAL STRUCTURE OF OASS COMPLEXED WITH CHLORIDE AND SULFATE

Method: X-RAY DIFFRACTION Dmax: 119.1 Å Quality: GOOD

SAXS 散射曲线 SAXS Profile

SAXS profile for 1fcj

P(r) 距离分布 P(r) Distribution

P(r) distribution for 1fcj
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1. 结构基本信息 1. Structure Basics

条目编号 entry_id1fcj
沉积日期 deposition_date2000-07-18
结构标题 titleCRYSTAL STRUCTURE OF OASS COMPLEXED WITH CHLORIDE AND SULFATE
关键词 keywordshomodimer, LYASE; LYASE
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier36.06
回转半径 Rg (电子) rg_electron35.66
零角强度 I(0) i0256199000.00
分子量 molecular_weight130140.0 kDa
排除体积 excluded_volume163630 ų
包络体积 envelope_volume204170 ų
水化壳体积 shell_volume47477 ų
包络直径 envelope_diameter120.2
壳层 Rg shell_rg42.13
包络 Rg envelope_rg35.20
形状 Rg shape_rg35.67
总 Rg total_rg36.06
总原子数 total_atoms9128
残基数 n_residues1212
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax119.1
Rg (实空间) rg_real36.05
Rg 误差 (实空间) rg_real_error1.14
I(0) (实空间) i0_real2.5620e+08
I(0) 误差 (实空间) i0_real_error3.9570e+06
Rg (倒空间) rg_reciprocal36.06
I(0) (倒空间) i0_reciprocal256200000.0000
解质量估计 total_estimate0.8915
解质量评级 solution_quality GOOD a GOOD solution
P(r) 峰数 n_peaks1
主峰位置 r_peak_primary40.6
偏度 Skewness skewness0.297
峰度 Kurtosis kurtosis-0.502
角度范围 angular_range— – 0.2200 −1
当前正则化参数 α current_alpha0.0000
最高正则化参数 α highest_alpha69350000.0000
实空间数据点数 n_real_points45
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.904; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.979; Smooth: 0.894

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (5)

6. 折叠分类 (SCOP + CATH) 12 domains

SCOP 2.08 (4 domains)

结构域编号 domain_idd1fcja_
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.79 — Tryptophan synthase beta subunit-like PLP-dependent enzymes
超家族 Superfamily superfamilyc.79.1 — Tryptophan synthase beta subunit-like PLP-dependent enzymes
家族 Family familyc.79.1.1 — Tryptophan synthase beta subunit-like PLP-dependent enzymes
结构域编号 domain_idd1fcjb_
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.79 — Tryptophan synthase beta subunit-like PLP-dependent enzymes
超家族 Superfamily superfamilyc.79.1 — Tryptophan synthase beta subunit-like PLP-dependent enzymes
家族 Family familyc.79.1.1 — Tryptophan synthase beta subunit-like PLP-dependent enzymes
结构域编号 domain_idd1fcjc_
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.79 — Tryptophan synthase beta subunit-like PLP-dependent enzymes
超家族 Superfamily superfamilyc.79.1 — Tryptophan synthase beta subunit-like PLP-dependent enzymes
家族 Family familyc.79.1.1 — Tryptophan synthase beta subunit-like PLP-dependent enzymes
结构域编号 domain_idd1fcjd_
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.79 — Tryptophan synthase beta subunit-like PLP-dependent enzymes
超家族 Superfamily superfamilyc.79.1 — Tryptophan synthase beta subunit-like PLP-dependent enzymes
家族 Family familyc.79.1.1 — Tryptophan synthase beta subunit-like PLP-dependent enzymes

CATH v4.4 (8 domains)

结构域编号 domain_id1fcjA01
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily1100
结构域编号 domain_id1fcjA02
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily1100
结构域编号 domain_id1fcjB01
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily1100
结构域编号 domain_id1fcjB02
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily1100
结构域编号 domain_id1fcjC01
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily1100
结构域编号 domain_id1fcjC02
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily1100
结构域编号 domain_id1fcjD01
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily1100
结构域编号 domain_id1fcjD02
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily1100

7. 引用文献 (3)

8. 文件与曲线 (10)