1ig0

Crystal Structure of yeast Thiamin Pyrophosphokinase

Method: X-RAY DIFFRACTION Dmax: 87.2 Å Quality: GOOD

SAXS 散射曲线 SAXS Profile

SAXS profile for 1ig0

P(r) 距离分布 P(r) Distribution

P(r) distribution for 1ig0
下载 Download

1. 结构基本信息 1. Structure Basics

条目编号 entry_id1ig0
沉积日期 deposition_date2001-04-16
结构标题 titleCrystal Structure of yeast Thiamin Pyrophosphokinase
关键词 keywordsProtein-substrate complex, compound active site, alpha-beta-alpha, beta sandwich, TRANSFERASE; TRANSFERASE
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier26.77
回转半径 Rg (电子) rg_electron25.57
零角强度 I(0) i082882600.00
分子量 molecular_weight73332.0 kDa
排除体积 excluded_volume92694 ų
包络体积 envelope_volume108900 ų
水化壳体积 shell_volume34414 ų
包络直径 envelope_diameter94.9
壳层 Rg shell_rg33.77
包络 Rg envelope_rg25.73
形状 Rg shape_rg25.56
总 Rg total_rg26.45
总原子数 total_atoms5160
残基数 n_residues636
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax87.2
Rg (实空间) rg_real26.62
Rg 误差 (实空间) rg_real_error0.63
I(0) (实空间) i0_real8.2880e+07
I(0) 误差 (实空间) i0_real_error1.2090e+06
Rg (倒空间) rg_reciprocal26.67
I(0) (倒空间) i0_reciprocal82890000.0000
解质量估计 total_estimate0.8084
解质量评级 solution_quality GOOD a GOOD solution
P(r) 峰数 n_peaks3
主峰位置 r_peak_primary34.0
偏度 Skewness skewness0.170
峰度 Kurtosis kurtosis-0.387
角度范围 angular_range— – 0.2950 −1
当前正则化参数 α current_alpha0.0000
最高正则化参数 α highest_alpha20570000.0000
实空间数据点数 n_real_points60
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.836; Stabil: 0.999; Sysdev: 1.000; Positv: 1.000; Valcen: 1.000; Smooth: 0.000

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (3)

6. 折叠分类 (SCOP + CATH) 8 domains

SCOP 2.08 (4 domains)

结构域编号 domain_idd1ig0a1
类 Class classb — All beta proteins
折叠类型 Fold foldb.82 — Double-stranded beta-helix
超家族 Superfamily superfamilyb.82.6 — Thiamin pyrophosphokinase, substrate-binding domain
家族 Family familyb.82.6.1 — Thiamin pyrophosphokinase, substrate-binding domain
结构域编号 domain_idd1ig0a2
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.100 — Thiamin pyrophosphokinase, catalytic domain
超家族 Superfamily superfamilyc.100.1 — Thiamin pyrophosphokinase, catalytic domain
家族 Family familyc.100.1.1 — Thiamin pyrophosphokinase, catalytic domain
结构域编号 domain_idd1ig0b1
类 Class classb — All beta proteins
折叠类型 Fold foldb.82 — Double-stranded beta-helix
超家族 Superfamily superfamilyb.82.6 — Thiamin pyrophosphokinase, substrate-binding domain
家族 Family familyb.82.6.1 — Thiamin pyrophosphokinase, substrate-binding domain
结构域编号 domain_idd1ig0b2
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.100 — Thiamin pyrophosphokinase, catalytic domain
超家族 Superfamily superfamilyc.100.1 — Thiamin pyrophosphokinase, catalytic domain
家族 Family familyc.100.1.1 — Thiamin pyrophosphokinase, catalytic domain

CATH v4.4 (4 domains)

结构域编号 domain_id1ig0A01
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily10240 — Thiamin pyrophosphokinase, catalytic domain
结构域编号 domain_id1ig0A02
类 Class class2 — Mainly Beta
架构 Architecture architecture60 — Sandwich
拓扑 Topology topology120 — Jelly Rolls
同源超家族 H-superfamily homologous superfamily320 — Thiamin pyrophosphokinase, thiamin-binding domain
结构域编号 domain_id1ig0B01
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily10240 — Thiamin pyrophosphokinase, catalytic domain
结构域编号 domain_id1ig0B02
类 Class class2 — Mainly Beta
架构 Architecture architecture60 — Sandwich
拓扑 Topology topology120 — Jelly Rolls
同源超家族 H-superfamily homologous superfamily320 — Thiamin pyrophosphokinase, thiamin-binding domain

7. 引用文献 (1)

8. 文件与曲线 (10)