1k3w

Crystal structure of a trapped reaction intermediate of the DNA Repair Enzyme Endonuclease VIII with DNA

Method: X-RAY DIFFRACTION Dmax: 65.7 Å Quality: EXCELLENT

SAXS 散射曲线 SAXS Profile

SAXS profile for 1k3w

P(r) 距离分布 P(r) Distribution

P(r) distribution for 1k3w
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1. 结构基本信息 1. Structure Basics

条目编号 entry_id1k3w
沉积日期 deposition_date2001-10-04
结构标题 titleCrystal structure of a trapped reaction intermediate of the DNA Repair Enzyme Endonuclease VIII with DNA
关键词 keywordsHYDROLASE/DNA, HYDROLASE-DNA complex; HYDROLASE/DNA
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier21.19
回转半径 Rg (电子) rg_electron20.23
零角强度 I(0) i026048100.00
分子量 molecular_weight34985.0 kDa
排除体积 excluded_volume42055 ų
包络体积 envelope_volume49889 ų
水化壳体积 shell_volume20777 ų
包络直径 envelope_diameter66.5
壳层 Rg shell_rg26.28
包络 Rg envelope_rg20.30
形状 Rg shape_rg20.17
总 Rg total_rg21.11
总原子数 total_atoms2437
残基数 n_residues272
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax65.7
Rg (实空间) rg_real21.09
Rg 误差 (实空间) rg_real_error0.35
I(0) (实空间) i0_real2.6050e+07
I(0) 误差 (实空间) i0_real_error3.5030e+05
Rg (倒空间) rg_reciprocal21.11
I(0) (倒空间) i0_reciprocal26050000.0000
解质量估计 total_estimate0.9063
解质量评级 solution_quality EXCELLENT a EXCELLENT solution
P(r) 峰数 n_peaks2
主峰位置 r_peak_primary26.1
偏度 Skewness skewness0.208
峰度 Kurtosis kurtosis-0.398
角度范围 angular_range— – 0.3750 −1
当前正则化参数 α current_alpha0.0000
最高正则化参数 α highest_alpha2582000.0000
实空间数据点数 n_real_points69
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.930; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.996; Smooth: 0.992

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (6)

6. 折叠分类 (SCOP + CATH) 5 domains

SCOP 2.08 (3 domains)

结构域编号 domain_idd1k3wa1
类 Class classa — All alpha proteins
折叠类型 Fold folda.156 — S13-like H2TH domain
超家族 Superfamily superfamilya.156.1 — S13-like H2TH domain
家族 Family familya.156.1.2 — Middle domain of MutM-like DNA repair proteins
结构域编号 domain_idd1k3wa2
类 Class classb — All beta proteins
折叠类型 Fold foldb.113 — N-terminal domain of MutM-like DNA repair proteins
超家族 Superfamily superfamilyb.113.1 — N-terminal domain of MutM-like DNA repair proteins
家族 Family familyb.113.1.1 — N-terminal domain of MutM-like DNA repair proteins
结构域编号 domain_idd1k3wa3
类 Class classg — Small proteins
折叠类型 Fold foldg.39 — Glucocorticoid receptor-like (DNA-binding domain)
超家族 Superfamily superfamilyg.39.1 — Glucocorticoid receptor-like (DNA-binding domain)
家族 Family familyg.39.1.8 — C-terminal, Zn-finger domain of MutM-like DNA repair proteins

CATH v4.4 (2 domains)

结构域编号 domain_id1k3wA01
类 Class class3 — Alpha Beta
架构 Architecture architecture20 — Alpha-Beta Barrel
拓扑 Topology topology190 — N-terminal domain of MutM-like DNA repair proteins
同源超家族 H-superfamily homologous superfamily10 — MutM-like, N-terminal
结构域编号 domain_id1k3wA02
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology8 — Helicase, Ruva Protein; domain 3
同源超家族 H-superfamily homologous superfamily50

7. 引用文献 (1)

8. 文件与曲线 (10)