1krh

X-ray Structure of Benzoate Dioxygenase Reductase

Method: X-RAY DIFFRACTION Dmax: 108.8 Å Quality: GOOD

SAXS 散射曲线 SAXS Profile

SAXS profile for 1krh

P(r) 距离分布 P(r) Distribution

P(r) distribution for 1krh
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1. 结构基本信息 1. Structure Basics

条目编号 entry_id1krh
沉积日期 deposition_date2002-01-09
结构标题 titleX-ray Structure of Benzoate Dioxygenase Reductase
关键词 keywordsalpha-beta, FAD-binding, ferredoxin, NADH-binding, OXIDOREDUCTASE; OXIDOREDUCTASE
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier32.58
回转半径 Rg (电子) rg_electron32.25
零角强度 I(0) i0104552000.00
分子量 molecular_weight77359.0 kDa
排除体积 excluded_volume94887 ų
包络体积 envelope_volume121050 ų
水化壳体积 shell_volume32526 ų
包络直径 envelope_diameter114.0
壳层 Rg shell_rg37.57
包络 Rg envelope_rg31.95
形状 Rg shape_rg32.26
总 Rg total_rg32.63
总原子数 total_atoms5409
残基数 n_residues674
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax108.8
Rg (实空间) rg_real32.83
Rg 误差 (实空间) rg_real_error0.86
I(0) (实空间) i0_real1.0460e+08
I(0) 误差 (实空间) i0_real_error1.7530e+06
Rg (倒空间) rg_reciprocal32.73
I(0) (倒空间) i0_reciprocal104500000.0000
解质量估计 total_estimate0.8490
解质量评级 solution_quality GOOD a GOOD solution
P(r) 峰数 n_peaks1
主峰位置 r_peak_primary31.1
偏度 Skewness skewness0.456
峰度 Kurtosis kurtosis-0.448
角度范围 angular_range— – 0.2450 −1
当前正则化参数 α current_alpha0.0000
最高正则化参数 α highest_alpha16090000.0000
实空间数据点数 n_real_points50
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.809; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.863; Smooth: 0.742

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (5)

6. 折叠分类 (SCOP + CATH) 12 domains

SCOP 2.08 (6 domains)

结构域编号 domain_idd1krha1
类 Class classb — All beta proteins
折叠类型 Fold foldb.43 — Reductase/isomerase/elongation factor common domain
超家族 Superfamily superfamilyb.43.4 — Riboflavin synthase domain-like
家族 Family familyb.43.4.2 — Ferredoxin reductase FAD-binding domain-like
结构域编号 domain_idd1krha2
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.25 — Ferredoxin reductase-like, C-terminal NADP-linked domain
超家族 Superfamily superfamilyc.25.1 — Ferredoxin reductase-like, C-terminal NADP-linked domain
家族 Family familyc.25.1.2 — Aromatic dioxygenase reductase-like
结构域编号 domain_idd1krha3
类 Class classd — Alpha and beta proteins (a+b)
折叠类型 Fold foldd.15 — beta-Grasp (ubiquitin-like)
超家族 Superfamily superfamilyd.15.4 — 2Fe-2S ferredoxin-like
家族 Family familyd.15.4.2 — 2Fe-2S ferredoxin domains from multidomain proteins
结构域编号 domain_idd1krhb1
类 Class classb — All beta proteins
折叠类型 Fold foldb.43 — Reductase/isomerase/elongation factor common domain
超家族 Superfamily superfamilyb.43.4 — Riboflavin synthase domain-like
家族 Family familyb.43.4.2 — Ferredoxin reductase FAD-binding domain-like
结构域编号 domain_idd1krhb2
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.25 — Ferredoxin reductase-like, C-terminal NADP-linked domain
超家族 Superfamily superfamilyc.25.1 — Ferredoxin reductase-like, C-terminal NADP-linked domain
家族 Family familyc.25.1.2 — Aromatic dioxygenase reductase-like
结构域编号 domain_idd1krhb3
类 Class classd — Alpha and beta proteins (a+b)
折叠类型 Fold foldd.15 — beta-Grasp (ubiquitin-like)
超家族 Superfamily superfamilyd.15.4 — 2Fe-2S ferredoxin-like
家族 Family familyd.15.4.2 — 2Fe-2S ferredoxin domains from multidomain proteins

CATH v4.4 (6 domains)

结构域编号 domain_id1krhA01
类 Class class3 — Alpha Beta
架构 Architecture architecture10 — Roll
拓扑 Topology topology20 — Ubiquitin-like (UB roll)
同源超家族 H-superfamily homologous superfamily30 — Beta-grasp domain
结构域编号 domain_id1krhA02
类 Class class2 — Mainly Beta
架构 Architecture architecture40 — Beta Barrel
拓扑 Topology topology30 — Elongation Factor Tu (Ef-tu); domain 3
同源超家族 H-superfamily homologous superfamily10 — Translation factors
结构域编号 domain_id1krhA03
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily80 — Nucleotide-binding domain of ferredoxin-NADP reductase (FNR) module
结构域编号 domain_id1krhB01
类 Class class3 — Alpha Beta
架构 Architecture architecture10 — Roll
拓扑 Topology topology20 — Ubiquitin-like (UB roll)
同源超家族 H-superfamily homologous superfamily30 — Beta-grasp domain
结构域编号 domain_id1krhB02
类 Class class2 — Mainly Beta
架构 Architecture architecture40 — Beta Barrel
拓扑 Topology topology30 — Elongation Factor Tu (Ef-tu); domain 3
同源超家族 H-superfamily homologous superfamily10 — Translation factors
结构域编号 domain_id1krhB03
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily80 — Nucleotide-binding domain of ferredoxin-NADP reductase (FNR) module

7. 引用文献 (1)

8. 文件与曲线 (10)