1smr

;The 3-d structure of mouse submaxillary renin complexed with a decapeptide inhibitor ch-66 based on the 4-16 fragment of rat angiotensinogen ;

Method: X-RAY DIFFRACTION Dmax: 233.6 Å Quality: REASONABLE

SAXS 散射曲线 SAXS Profile

SAXS profile for 1smr

P(r) 距离分布 P(r) Distribution

P(r) distribution for 1smr
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1. 结构基本信息 1. Structure Basics

条目编号 entry_id1smr
沉积日期 deposition_date1992-03-11
结构标题 title;The 3-d structure of mouse submaxillary renin complexed with a decapeptide inhibitor ch-66 based on the 4-16 fragment of rat angiotensinogen ;
关键词 keywordsASPARTIC PROTEINASE, HYDROLASE-HYDROLASE INHIBITOR complex; HYDROLASE/HYDROLASE INHIBITOR
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier79.29
回转半径 Rg (电子) rg_electron78.89
零角强度 I(0) i0282643000.00
分子量 molecular_weight147450.0 kDa
排除体积 excluded_volume185980 ų
包络体积 envelope_volume336550 ų
水化壳体积 shell_volume36191 ų
包络直径 envelope_diameter207.0
壳层 Rg shell_rg84.00
包络 Rg envelope_rg70.79
形状 Rg shape_rg78.89
总 Rg total_rg78.92
总原子数 total_atoms10404
残基数 n_residues1340
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax233.6
Rg (实空间) rg_real79.16
Rg 误差 (实空间) rg_real_error1.94
I(0) (实空间) i0_real2.8260e+08
I(0) 误差 (实空间) i0_real_error5.4840e+06
Rg (倒空间) rg_reciprocal78.88
I(0) (倒空间) i0_reciprocal282300000.0000
解质量估计 total_estimate0.5895
解质量评级 solution_quality REASONABLE a REASONABLE solution
P(r) 峰数 n_peaks2
主峰位置 r_peak_primary140.2
偏度 Skewness skewness-0.345
峰度 Kurtosis kurtosis-1.402
角度范围 angular_range— – 0.1000 −1
当前正则化参数 α current_alpha0.0005
最高正则化参数 α highest_alpha6031000.0000
实空间数据点数 n_real_points21
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.001; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.657; Smooth: 0.000

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (3)

6. 折叠分类 (SCOP + CATH) 12 domains

SCOP 2.08 (4 domains)

结构域编号 domain_idd1smra_
类 Class classb — All beta proteins
折叠类型 Fold foldb.50 — Acid proteases
超家族 Superfamily superfamilyb.50.1 — Acid proteases
家族 Family familyb.50.1.2 — Pepsin-like
结构域编号 domain_idd1smrc_
类 Class classb — All beta proteins
折叠类型 Fold foldb.50 — Acid proteases
超家族 Superfamily superfamilyb.50.1 — Acid proteases
家族 Family familyb.50.1.2 — Pepsin-like
结构域编号 domain_idd1smre_
类 Class classb — All beta proteins
折叠类型 Fold foldb.50 — Acid proteases
超家族 Superfamily superfamilyb.50.1 — Acid proteases
家族 Family familyb.50.1.2 — Pepsin-like
结构域编号 domain_idd1smrg_
类 Class classb — All beta proteins
折叠类型 Fold foldb.50 — Acid proteases
超家族 Superfamily superfamilyb.50.1 — Acid proteases
家族 Family familyb.50.1.2 — Pepsin-like

CATH v4.4 (8 domains)

结构域编号 domain_id1smrA01
类 Class class2 — Mainly Beta
架构 Architecture architecture40 — Beta Barrel
拓扑 Topology topology70 — Cathepsin D, subunit A; domain 1
同源超家族 H-superfamily homologous superfamily10 — Acid Proteases
结构域编号 domain_id1smrA02
类 Class class2 — Mainly Beta
架构 Architecture architecture40 — Beta Barrel
拓扑 Topology topology70 — Cathepsin D, subunit A; domain 1
同源超家族 H-superfamily homologous superfamily10 — Acid Proteases
结构域编号 domain_id1smrC01
类 Class class2 — Mainly Beta
架构 Architecture architecture40 — Beta Barrel
拓扑 Topology topology70 — Cathepsin D, subunit A; domain 1
同源超家族 H-superfamily homologous superfamily10 — Acid Proteases
结构域编号 domain_id1smrC02
类 Class class2 — Mainly Beta
架构 Architecture architecture40 — Beta Barrel
拓扑 Topology topology70 — Cathepsin D, subunit A; domain 1
同源超家族 H-superfamily homologous superfamily10 — Acid Proteases
结构域编号 domain_id1smrE01
类 Class class2 — Mainly Beta
架构 Architecture architecture40 — Beta Barrel
拓扑 Topology topology70 — Cathepsin D, subunit A; domain 1
同源超家族 H-superfamily homologous superfamily10 — Acid Proteases
结构域编号 domain_id1smrE02
类 Class class2 — Mainly Beta
架构 Architecture architecture40 — Beta Barrel
拓扑 Topology topology70 — Cathepsin D, subunit A; domain 1
同源超家族 H-superfamily homologous superfamily10 — Acid Proteases
结构域编号 domain_id1smrG01
类 Class class2 — Mainly Beta
架构 Architecture architecture40 — Beta Barrel
拓扑 Topology topology70 — Cathepsin D, subunit A; domain 1
同源超家族 H-superfamily homologous superfamily10 — Acid Proteases
结构域编号 domain_id1smrG02
类 Class class2 — Mainly Beta
架构 Architecture architecture40 — Beta Barrel
拓扑 Topology topology70 — Cathepsin D, subunit A; domain 1
同源超家族 H-superfamily homologous superfamily10 — Acid Proteases

7. 引用文献 (3)

8. 文件与曲线 (10)