1vdz

Crystal structure of A-type ATPase catalytic subunit A from Pyrococcus horikoshii OT3

Method: X-RAY DIFFRACTION Dmax: 93.8 Å Quality: GOOD

SAXS 散射曲线 SAXS Profile

SAXS profile for 1vdz

P(r) 距离分布 P(r) Distribution

P(r) distribution for 1vdz
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1. 结构基本信息 1. Structure Basics

条目编号 entry_id1vdz
沉积日期 deposition_date2004-03-26
结构标题 titleCrystal structure of A-type ATPase catalytic subunit A from Pyrococcus horikoshii OT3
关键词 keywordsA-type ATPase, catalytic subunit, Archaea, HYDROLASE; HYDROLASE
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier26.97
回转半径 Rg (电子) rg_electron26.39
零角强度 I(0) i051101700.00
分子量 molecular_weight57245.0 kDa
排除体积 excluded_volume72339 ų
包络体积 envelope_volume86232 ų
水化壳体积 shell_volume28306 ų
包络直径 envelope_diameter96.3
壳层 Rg shell_rg32.69
包络 Rg envelope_rg26.88
形状 Rg shape_rg26.37
总 Rg total_rg27.12
总原子数 total_atoms4033
残基数 n_residues513
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax93.8
Rg (实空间) rg_real27.13
Rg 误差 (实空间) rg_real_error0.73
I(0) (实空间) i0_real5.1100e+07
I(0) 误差 (实空间) i0_real_error7.4790e+05
Rg (倒空间) rg_reciprocal27.08
I(0) (倒空间) i0_reciprocal51100000.0000
解质量估计 total_estimate0.8454
解质量评级 solution_quality GOOD a GOOD solution
P(r) 峰数 n_peaks2
主峰位置 r_peak_primary28.6
偏度 Skewness skewness0.543
峰度 Kurtosis kurtosis-0.105
角度范围 angular_range— – 0.2950 −1
当前正则化参数 α current_alpha0.0000
最高正则化参数 α highest_alpha10640000.0000
实空间数据点数 n_real_points60
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.735; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.846; Smooth: 0.937

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (2)

6. 折叠分类 (SCOP + CATH) 6 domains

SCOP 2.08 (3 domains)

结构域编号 domain_idd1vdza1
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.37 — P-loop containing nucleoside triphosphate hydrolases
超家族 Superfamily superfamilyc.37.1 — P-loop containing nucleoside triphosphate hydrolases
家族 Family familyc.37.1.11 — RecA protein-like (ATPase-domain)
结构域编号 domain_idd1vdza2
类 Class classb — All beta proteins
折叠类型 Fold foldb.84 — Barrel-sandwich hybrid
超家族 Superfamily superfamilyb.84.5 — V1 ATP synthase A subunit, bulge domain-like
家族 Family familyb.84.5.1 — V1 ATP synthase A subunit, bulge domain-like
结构域编号 domain_idd1vdza3
类 Class classa — All alpha proteins
折叠类型 Fold folda.69 — Left-handed superhelix
超家族 Superfamily superfamilya.69.1 — C-terminal domain of alpha and beta (or A/B) subunits of rotary ATPases
家族 Family familya.69.1.2 — C-terminal domain of A and B subunits of V1 ATP synthase and A1 ATP sythase

CATH v4.4 (3 domains)

结构域编号 domain_id1vdzA01
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily300 — P-loop containing nucleotide triphosphate hydrolases
结构域编号 domain_id1vdzA02
类 Class class2 — Mainly Beta
架构 Architecture architecture40 — Beta Barrel
拓扑 Topology topology50 — OB fold (Dihydrolipoamide Acetyltransferase, E2P)
同源超家族 H-superfamily homologous superfamily100 — RNA polymerase II/Efflux pump adaptor protein, barrel-sandwich hybrid domain
结构域编号 domain_id1vdzA03
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology1140 — Bovine Mitochondrial F1-ATPase, ATP Synthase Beta Chain; Chain D, domain3
同源超家族 H-superfamily homologous superfamily10 — Bovine Mitochondrial F1-atpase; Atp Synthase Beta Chain; Chain D, domain 3

7. 引用文献 (1)

8. 文件与曲线 (10)