1y1l

Crystal structure of arsenate reductase from Archaeoglobus fulgidus DSM 4304, structural genomics

Method: X-RAY DIFFRACTION Dmax: 79.3 Å Quality: REASONABLE

SAXS 散射曲线 SAXS Profile

SAXS profile for 1y1l

P(r) 距离分布 P(r) Distribution

P(r) distribution for 1y1l
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1. 结构基本信息 1. Structure Basics

条目编号 entry_id1y1l
沉积日期 deposition_date2004-11-18
结构标题 titleCrystal structure of arsenate reductase from Archaeoglobus fulgidus DSM 4304, structural genomics
关键词 keywords;ARSENATE REDUCTASE, DETOXIFICATION, CADMIUM, OXIDIZED FORM, Structural Genomics, PSI, Protein Structure Initiative, New York SGX Research Center for Structural Genomics, NYSGXRC, TRANSFERASE ;; TRANSFERASE
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier25.63
回转半径 Rg (电子) rg_electron24.80
零角强度 I(0) i056671400.00
分子量 molecular_weight56704.0 kDa
排除体积 excluded_volume70241 ų
包络体积 envelope_volume86982 ų
水化壳体积 shell_volume28909 ų
包络直径 envelope_diameter79.4
壳层 Rg shell_rg32.33
包络 Rg envelope_rg24.75
形状 Rg shape_rg24.86
总 Rg total_rg25.46
总原子数 total_atoms3920
残基数 n_residues496
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax79.3
Rg (实空间) rg_real25.55
Rg 误差 (实空间) rg_real_error0.37
I(0) (实空间) i0_real5.6670e+07
I(0) 误差 (实空间) i0_real_error7.3030e+05
Rg (倒空间) rg_reciprocal25.57
I(0) (倒空间) i0_reciprocal56670000.0000
解质量估计 total_estimate0.7161
解质量评级 solution_quality REASONABLE a REASONABLE solution
P(r) 峰数 n_peaks0
主峰位置 r_peak_primary
偏度 Skewness skewness0.214
峰度 Kurtosis kurtosis-0.556
角度范围 angular_range— – 0.3100 −1
当前正则化参数 α current_alpha0.0000
最高正则化参数 α highest_alpha49390000.0000
实空间数据点数 n_real_points63
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.949; Stabil: 1.000; Sysdev: 0.164; Positv: 1.000; Valcen: 1.000; Smooth: 0.966

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (2)

6. 折叠分类 (SCOP + CATH) 8 domains

SCOP 2.08 (4 domains)

结构域编号 domain_idd1y1la_
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.44 — Phosphotyrosine protein phosphatases I-like
超家族 Superfamily superfamilyc.44.1 — Phosphotyrosine protein phosphatases I
家族 Family familyc.44.1.1 — Low-molecular-weight phosphotyrosine protein phosphatases
结构域编号 domain_idd1y1lb_
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.44 — Phosphotyrosine protein phosphatases I-like
超家族 Superfamily superfamilyc.44.1 — Phosphotyrosine protein phosphatases I
家族 Family familyc.44.1.1 — Low-molecular-weight phosphotyrosine protein phosphatases
结构域编号 domain_idd1y1lc_
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.44 — Phosphotyrosine protein phosphatases I-like
超家族 Superfamily superfamilyc.44.1 — Phosphotyrosine protein phosphatases I
家族 Family familyc.44.1.1 — Low-molecular-weight phosphotyrosine protein phosphatases
结构域编号 domain_idd1y1ld_
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.44 — Phosphotyrosine protein phosphatases I-like
超家族 Superfamily superfamilyc.44.1 — Phosphotyrosine protein phosphatases I
家族 Family familyc.44.1.1 — Low-molecular-weight phosphotyrosine protein phosphatases

CATH v4.4 (4 domains)

结构域编号 domain_id1y1lA00
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily2300 — Response regulator
结构域编号 domain_id1y1lB00
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily2300 — Response regulator
结构域编号 domain_id1y1lC00
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily2300 — Response regulator
结构域编号 domain_id1y1lD00
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily2300 — Response regulator

7. 引用文献 (1)

8. 文件与曲线 (10)