2jsc

NMR structure of the cadmium metal-sensor CMTR from Mycobacterium tuberculosis

Method: SOLUTION NMR Dmax: 72.8 Å Quality: REASONABLE

SAXS 散射曲线 SAXS Profile

SAXS profile for 2jsc

P(r) 距离分布 P(r) Distribution

P(r) distribution for 2jsc
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1. 结构基本信息 1. Structure Basics

条目编号 entry_id2jsc
沉积日期 deposition_date2007-07-02
结构标题 titleNMR structure of the cadmium metal-sensor CMTR from Mycobacterium tuberculosis
关键词 keywordsCADMIUM, TRANSCRIPTIONAL REPRESSOR, SOLUTION STRUCTURE, STRUCTURAL GENOMICS, STRUCTURAL PROTEOMICS IN EUROPE, SPINE, TRANSCRIPTION; TRANSCRIPTION
实验方法 methodSOLUTION NMR

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier18.94
回转半径 Rg (电子) rg_electron18.81
零角强度 I(0) i05851350000.00
分子量 molecular_weight625160.0 kDa
排除体积 excluded_volume772770 ų
包络体积 envelope_volume55564 ų
水化壳体积 shell_volume22369 ų
包络直径 envelope_diameter84.0
壳层 Rg shell_rg27.90
包络 Rg envelope_rg21.74
形状 Rg shape_rg18.89
总 Rg total_rg18.65
总原子数 total_atoms87890
残基数 n_residues5819
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax72.8
Rg (实空间) rg_real19.08
Rg 误差 (实空间) rg_real_error0.88
I(0) (实空间) i0_real5.8510e+09
I(0) 误差 (实空间) i0_real_error9.0510e+07
Rg (倒空间) rg_reciprocal19.06
I(0) (倒空间) i0_reciprocal5851000000.0000
解质量估计 total_estimate0.6931
解质量评级 solution_quality REASONABLE a REASONABLE solution
P(r) 峰数 n_peaks3
主峰位置 r_peak_primary20.2
偏度 Skewness skewness0.605
峰度 Kurtosis kurtosis0.196
角度范围 angular_range— – 0.4200 −1
当前正则化参数 α current_alpha0.0000
最高正则化参数 α highest_alpha732800.0000
实空间数据点数 n_real_points73
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.443; Stabil: 0.998; Sysdev: 1.000; Positv: 1.000; Valcen: 0.685; Smooth: 0.000

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (2)

6. 折叠分类 (SCOP + CATH) 4 domains

SCOP 2.08 (2 domains)

结构域编号 domain_idd2jsca_
类 Class classa — All alpha proteins
折叠类型 Fold folda.4 — DNA/RNA-binding 3-helical bundle
超家族 Superfamily superfamilya.4.5 — 'Winged helix' DNA-binding domain
家族 Family familya.4.5.0 — automated matches
结构域编号 domain_idd2jscb_
类 Class classa — All alpha proteins
折叠类型 Fold folda.4 — DNA/RNA-binding 3-helical bundle
超家族 Superfamily superfamilya.4.5 — 'Winged helix' DNA-binding domain
家族 Family familya.4.5.0 — automated matches

CATH v4.4 (2 domains)

结构域编号 domain_id2jscA01
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology10 — Arc Repressor Mutant, subunit A
同源超家族 H-superfamily homologous superfamily10 — Winged helix-like DNA-binding domain superfamily/Winged helix DNA-binding domain
结构域编号 domain_id2jscB01
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology10 — Arc Repressor Mutant, subunit A
同源超家族 H-superfamily homologous superfamily10 — Winged helix-like DNA-binding domain superfamily/Winged helix DNA-binding domain

7. 引用文献 (1)

8. 文件与曲线 (10)