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1b9q

NMR STRUCTURE OF HEPARIN BINDING SITE OF NON COLLAGENOUS DOMAIN I (NC1) OF COLLAGEN FACIT XIV

Method: SOLUTION NMR Dmax: 41.4 Å Quality: REASONABLE

SAXS Profile

SAXS profile for 1b9q

P(r) Distribution

P(r) distribution for 1b9q

1. Structure Basics

entry_id1b9q
deposition_date1999-02-15
titleNMR STRUCTURE OF HEPARIN BINDING SITE OF NON COLLAGENOUS DOMAIN I (NC1) OF COLLAGEN FACIT XIV
keywordsCOLLAGEN FACIT XIV, HEPARIN-BINDING SITE, NC1; COLLAGEN FACIT XIV
methodSOLUTION NMR

Download Data

2. SAXS Parameters (CRYSOL)

rg_guinier15.35
rg_electron15.25
i090524700.00
molecular_weight76300.0 kDa
excluded_volume95253 ų
envelope_volume23353 ų
shell_volume11293 ų
envelope_diameter62.4
shell_rg23.49
envelope_rg19.45
shape_rg15.19
total_rg15.81
total_atoms11172
n_residues646
n_harmonics20
q_range— – 0.5000 −1
n_points101
shell_typedirectional
solvent_density0.3340 e/ų
contrast_shell0.0300 e/ų
crysol_version4.1.3

3. P(r) Analysis (GNOM)

dmax41.4
rg_real14.35
rg_real_error0.10
i0_real8.6370e+07
i0_real_error7.5820e+05
rg_reciprocal15.73
i0_reciprocal90520000.0000
total_estimate0.6186
solution_quality REASONABLE a REASONABLE solution
n_peaks1
r_peak_primary10.5
skewness0.371
kurtosis-0.831
angular_range— – 0.5000 −1
current_alpha4.6350
highest_alpha19780.0000
n_real_points80
gnom_version4.1.3
quality_criteria AN1: 0.002; Oscil: 0.927; Stabil: 0.975; Sysdev: 0.000; Positv: 1.000; Valcen: 0.339; Smooth: 0.000

4. Crystallography & Experiment

5. Entities & Polymer Info (1)

6. Citations (2)

7. Files & Curves (10)