;HUMAN LYSOZYME L63 MUTANT LABELLED WITH 2',3'-EPOXYPROPYL N,N'-DIACETYLCHITOBIOSE ;

entry_id	1d6p
deposition_date	1999-10-15
title	;HUMAN LYSOZYME L63 MUTANT LABELLED WITH 2',3'-EPOXYPROPYL N,N'-DIACETYLCHITOBIOSE ;
keywords	;LYSOZYME, MURAMIDASE, HYDROLASE (O-GLYCOSYL), SITE-DIRECTED MUTAGENESIS, N, N'-DIACETYLCHITOBIOSE, AFFINITY LABELING, HYDROLASE ;; HYDROLASE
method	X-RAY DIFFRACTION

rg_guinier	15.40 Å
rg_electron	14.06 Å
i0	5051270.00
molecular_weight	15142.0 kDa
excluded_volume	18522 ų
envelope_volume	20270 ų
shell_volume	12325 ų
envelope_diameter	49.8 Å
shell_rg	19.79 Å
envelope_rg	14.34 Å
shape_rg	14.04 Å
total_rg	15.15 Å
total_atoms	1058
n_residues	130
n_harmonics	20
q_range	— – 0.5000 Å−1
n_points	101
shell_type	directional
solvent_density	0.3340 e/ų
contrast_shell	0.0300 e/ų
crysol_version	4.1.3

dmax	50.4 Å
rg_real	15.32 Å
rg_real_error	0.22 Å
i0_real	5.0510e+06
i0_real_error	4.5980e+04
rg_reciprocal	15.33 Å
i0_reciprocal	5051000.0000
total_estimate	0.8810
solution_quality	GOOD a GOOD solution
n_peaks	1
r_peak_primary	49.8 Å
skewness	0.201
kurtosis	-0.288
angular_range	— – 0.5000 Å−1
current_alpha	0.0000
highest_alpha	881200.0000
n_real_points	80
gnom_version	4.1.3
quality_criteria	AN1: 0.000; Oscil: 0.833; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 1.000; Smooth: 0.950

Unit Cell

length_a	58.200 Å
length_b	60.780 Å
length_c	32.730 Å
angle_alpha	90.00 °
angle_beta	90.00 °
angle_gamma	90.00 °
z_pdb	4

Symmetry

space_group	P 21 21 21
int_tables_number	19
crystal_system	—

Refinement

resolution	2.230 Å
resolution_low	8.000 Å
r_factor	0.1810
r_work	0.1810
r_free	0.2160

Diffraction

temperature

288.0 K

Files (7)

• pr_distribution /app/data/pr_computation/d6/1d6p/pr_distribution.json
• pr_output /app/data/pr_computation/d6/1d6p/1d6p.pr.out
• pr_plot /app/data/visualization/pr_computation/d6/1d6p/1d6p_pr_distribution.png
• saxs_curve_dat /app/data/saxs_computation/d6/1d6p/1d6p.dat
• saxs_fit /app/data/saxs_computation/d6/1d6p/1d6p.fit
• saxs_log /app/data/saxs_computation/d6/1d6p/1d6p.log
• saxs_plot /app/data/visualization/saxs_computation/d6/1d6p/1d6p_saxs_profile.png

Curves (3)

fit	/app/data/saxs_computation/d6/1d6p/1d6p.fit
pddf	/app/data/pr_computation/d6/1d6p/1d6p.pr.out
profile	/app/data/saxs_computation/d6/1d6p/1d6p.dat