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1deh

;CRYSTALLIZATION OF HUMAN BETA1 ALCOHOL DEHYDROGENASE (15 MG/ML) IN 50 MM SODIUM PHOSPHATE (PH 7.5), 2.0 MM NAD+ AND 1 MM 4-IODOPYRAZOLE AT 25 OC, 13% (W/V) PEG 8000 ;

Method: X-RAY DIFFRACTION Dmax: 103.4 Å Quality: GOOD

SAXS Profile

SAXS profile for 1deh

P(r) Distribution

P(r) distribution for 1deh
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1. Structure Basics

entry_id1deh
deposition_date1995-10-14
title;CRYSTALLIZATION OF HUMAN BETA1 ALCOHOL DEHYDROGENASE (15 MG/ML) IN 50 MM SODIUM PHOSPHATE (PH 7.5), 2.0 MM NAD+ AND 1 MM 4-IODOPYRAZOLE AT 25 OC, 13% (W/V) PEG 8000 ;
keywordsNAD+ DEPENDENT ALCOHOL DEHYDROGENASE, OXIDOREDUCTASE; OXIDOREDUCTASE
methodX-RAY DIFFRACTION
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Download Data

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2. SAXS Parameters (CRYSOL)

rg_guinier29.65 Å
rg_electron29.70 Å
i0105222000.00
molecular_weight81473.0 kDa
excluded_volume102040 ų
envelope_volume119480 ų
shell_volume34355 ų
envelope_diameter109.5 Å
shell_rg36.10 Å
envelope_rg29.90 Å
shape_rg29.73 Å
total_rg30.13 Å
total_atoms5667
n_residues748
n_harmonics20
q_range— – 0.5000 Å−1
n_points101
shell_typedirectional
solvent_density0.3340 e/ų
contrast_shell0.0300 e/ų
crysol_version4.1.3
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3. P(r) Analysis (GNOM)

dmax103.4 Å
rg_real29.80 Å
rg_real_error1.02 Å
i0_real1.0520e+08
i0_real_error1.6870e+06
rg_reciprocal29.74 Å
i0_reciprocal105200000.0000
total_estimate0.8493
solution_quality GOOD a GOOD solution
n_peaks2
r_peak_primary29.3 Å
skewness0.502
kurtosis-0.273
angular_range— – 0.2650 Å−1
current_alpha0.0000
highest_alpha52610000.0000
n_real_points54
gnom_version4.1.3
quality_criteria AN1: 0.000; Oscil: 0.731; Stabil: 0.999; Sysdev: 1.000; Positv: 1.000; Valcen: 0.863; Smooth: 0.985
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4. Crystallography & Experiment

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5. Entities & Polymer Info (6)

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6. Citations (2)

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7. Files & Curves (10)