CRYSTAL STRUCTURE OF A HETERODIMERIC COMPLEX OF RAR AND RXR LIGAND-BINDING DOMAINS

entry_id	1dkf
deposition_date	1999-12-07
title	CRYSTAL STRUCTURE OF A HETERODIMERIC COMPLEX OF RAR AND RXR LIGAND-BINDING DOMAINS
keywords	;HELICAL SANDWICH, HETERODIMER, PROTEIN-LIGAND COMPLEX, HORMONE/GROWTH FACTOR RECEPTOR, Structural Proteomics in Europe, SPINE, Structural Genomics, HORMONE-GROWTH FACTOR RECEPTOR complex ;; HORMONE/GROWTH FACTOR RECEPTOR
method	X-RAY DIFFRACTION

rg_guinier	23.50 Å
rg_electron	22.28 Å
i0	40596100.00
molecular_weight	51146.0 kDa
excluded_volume	64885 ų
envelope_volume	74784 ų
shell_volume	27268 ų
envelope_diameter	70.9 Å
shell_rg	29.75 Å
envelope_rg	22.37 Å
shape_rg	22.31 Å
total_rg	23.09 Å
total_atoms	3586
n_residues	449
n_harmonics	20
q_range	— – 0.5000 Å−1
n_points	101
shell_type	directional
solvent_density	0.3340 e/ų
contrast_shell	0.0300 e/ų
crysol_version	4.1.3

dmax	69.2 Å
rg_real	23.34 Å
rg_real_error	0.37 Å
i0_real	4.0600e+07
i0_real_error	4.9860e+05
rg_reciprocal	23.38 Å
i0_reciprocal	40600000.0000
total_estimate	0.9146
solution_quality	EXCELLENT a EXCELLENT solution
n_peaks	2
r_peak_primary	29.8 Å
skewness	0.110
kurtosis	-0.573
angular_range	— – 0.3400 Å−1
current_alpha	0.0000
highest_alpha	9223000.0000
n_real_points	66
gnom_version	4.1.3
quality_criteria	AN1: 0.000; Oscil: 0.970; Stabil: 0.999; Sysdev: 1.000; Positv: 1.000; Valcen: 0.987; Smooth: 0.992

Unit Cell

length_a	116.600 Å
length_b	116.600 Å
length_c	207.800 Å
angle_alpha	90.00 °
angle_beta	90.00 °
angle_gamma	120.00 °
z_pdb	12

Symmetry

space_group	P 61 2 2
int_tables_number	178
crystal_system	—

Refinement

resolution	2.500 Å
resolution_low	20.000 Å
r_factor	0.2030
r_work	0.2030
r_free	0.2620

Diffraction

temperature

120.0 K

Files (7)

• pr_distribution /app/data/pr_computation/dk/1dkf/pr_distribution.json
• pr_output /app/data/pr_computation/dk/1dkf/1dkf.pr.out
• pr_plot /app/data/visualization/pr_computation/dk/1dkf/1dkf_pr_distribution.png
• saxs_curve_dat /app/data/saxs_computation/dk/1dkf/1dkf.dat
• saxs_fit /app/data/saxs_computation/dk/1dkf/1dkf.fit
• saxs_log /app/data/saxs_computation/dk/1dkf/1dkf.log
• saxs_plot /app/data/visualization/saxs_computation/dk/1dkf/1dkf_saxs_profile.png

Curves (3)

fit	/app/data/saxs_computation/dk/1dkf/1dkf.fit
pddf	/app/data/pr_computation/dk/1dkf/1dkf.pr.out
profile	/app/data/saxs_computation/dk/1dkf/1dkf.dat