1kke

Crystal Structure of Reovirus Attachment Protein Sigma1 Trimer

Method: X-RAY DIFFRACTION Dmax: 118.7 Å Quality: REASONABLE

SAXS 散射曲线 SAXS Profile

SAXS profile for 1kke

P(r) 距离分布 P(r) Distribution

P(r) distribution for 1kke
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1. 结构基本信息 1. Structure Basics

条目编号 entry_id1kke
沉积日期 deposition_date2001-12-07
结构标题 titleCrystal Structure of Reovirus Attachment Protein Sigma1 Trimer
关键词 keywordsreovirus, sigma1, fiber, beta-spiral, beta-barrel, trimer, receptor-binding, Viral protein; VIRAL PROTEIN
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier32.60
回转半径 Rg (电子) rg_electron33.01
零角强度 I(0) i071774200.00
分子量 molecular_weight66796.0 kDa
排除体积 excluded_volume83465 ų
包络体积 envelope_volume105190 ų
水化壳体积 shell_volume30287 ų
包络直径 envelope_diameter123.1
壳层 Rg shell_rg34.65
包络 Rg envelope_rg34.13
形状 Rg shape_rg32.92
总 Rg total_rg33.46
总原子数 total_atoms4710
残基数 n_residues617
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax118.7
Rg (实空间) rg_real33.41
Rg 误差 (实空间) rg_real_error1.51
I(0) (实空间) i0_real7.1770e+07
I(0) 误差 (实空间) i0_real_error1.3440e+06
Rg (倒空间) rg_reciprocal33.07
I(0) (倒空间) i0_reciprocal71750000.0000
解质量估计 total_estimate0.7002
解质量评级 solution_quality REASONABLE a REASONABLE solution
P(r) 峰数 n_peaks3
主峰位置 r_peak_primary29.1
偏度 Skewness skewness0.798
峰度 Kurtosis kurtosis-0.058
角度范围 angular_range— – 0.2450 −1
当前正则化参数 α current_alpha0.0000
最高正则化参数 α highest_alpha15210000.0000
实空间数据点数 n_real_points50
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.293; Stabil: 0.999; Sysdev: 1.000; Positv: 1.000; Valcen: 0.448; Smooth: 0.775

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (2)

6. 折叠分类 (SCOP + CATH) 12 domains

SCOP 2.08 (6 domains)

结构域编号 domain_idd1kkea1
类 Class classb — All beta proteins
折叠类型 Fold foldb.83 — Triple beta-spiral
超家族 Superfamily superfamilyb.83.1 — Fibre shaft of virus attachment proteins
家族 Family familyb.83.1.2 — Reovirus attachment protein sigma 1
结构域编号 domain_idd1kkea2
类 Class classb — All beta proteins
折叠类型 Fold foldb.21 — Virus attachment protein globular domain
超家族 Superfamily superfamilyb.21.1 — Virus attachment protein globular domain
家族 Family familyb.21.1.2 — Reovirus attachment protein sigma 1 head domain
结构域编号 domain_idd1kkeb1
类 Class classb — All beta proteins
折叠类型 Fold foldb.83 — Triple beta-spiral
超家族 Superfamily superfamilyb.83.1 — Fibre shaft of virus attachment proteins
家族 Family familyb.83.1.2 — Reovirus attachment protein sigma 1
结构域编号 domain_idd1kkeb2
类 Class classb — All beta proteins
折叠类型 Fold foldb.21 — Virus attachment protein globular domain
超家族 Superfamily superfamilyb.21.1 — Virus attachment protein globular domain
家族 Family familyb.21.1.2 — Reovirus attachment protein sigma 1 head domain
结构域编号 domain_idd1kkec1
类 Class classb — All beta proteins
折叠类型 Fold foldb.83 — Triple beta-spiral
超家族 Superfamily superfamilyb.83.1 — Fibre shaft of virus attachment proteins
家族 Family familyb.83.1.2 — Reovirus attachment protein sigma 1
结构域编号 domain_idd1kkec2
类 Class classb — All beta proteins
折叠类型 Fold foldb.21 — Virus attachment protein globular domain
超家族 Superfamily superfamilyb.21.1 — Virus attachment protein globular domain
家族 Family familyb.21.1.2 — Reovirus attachment protein sigma 1 head domain

CATH v4.4 (6 domains)

结构域编号 domain_id1kkeA01
类 Class class2 — Mainly Beta
架构 Architecture architecture10 — Ribbon
拓扑 Topology topology25 — Laminin
同源超家族 H-superfamily homologous superfamily20 — reovirus attachment protein sigma1; domain 1
结构域编号 domain_id1kkeA02
类 Class class2 — Mainly Beta
架构 Architecture architecture60 — Sandwich
拓扑 Topology topology90 — Adenovirus Type 5 Fiber Protein (Receptor Binding Domain)
同源超家族 H-superfamily homologous superfamily20 — Virus attachment protein , globular domain
结构域编号 domain_id1kkeB01
类 Class class2 — Mainly Beta
架构 Architecture architecture10 — Ribbon
拓扑 Topology topology25 — Laminin
同源超家族 H-superfamily homologous superfamily20 — reovirus attachment protein sigma1; domain 1
结构域编号 domain_id1kkeB02
类 Class class2 — Mainly Beta
架构 Architecture architecture60 — Sandwich
拓扑 Topology topology90 — Adenovirus Type 5 Fiber Protein (Receptor Binding Domain)
同源超家族 H-superfamily homologous superfamily20 — Virus attachment protein , globular domain
结构域编号 domain_id1kkeC01
类 Class class2 — Mainly Beta
架构 Architecture architecture10 — Ribbon
拓扑 Topology topology25 — Laminin
同源超家族 H-superfamily homologous superfamily20 — reovirus attachment protein sigma1; domain 1
结构域编号 domain_id1kkeC02
类 Class class2 — Mainly Beta
架构 Architecture architecture60 — Sandwich
拓扑 Topology topology90 — Adenovirus Type 5 Fiber Protein (Receptor Binding Domain)
同源超家族 H-superfamily homologous superfamily20 — Virus attachment protein , globular domain

7. 引用文献 (1)

8. 文件与曲线 (10)