COVALENT ADDUCT OF D-AMINO ACID OXIDASE FROM PIG KIDNEY WITH 3-METHYL-2-OXO-VALERIC ACID

Method: X-RAY DIFFRACTION D_max: 174.7 Å Quality: GOOD

SAXS Profile

P(r) Distribution

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1. Structure Basics

entry_id	1dao
deposition_date	1997-01-16
title	COVALENT ADDUCT OF D-AMINO ACID OXIDASE FROM PIG KIDNEY WITH 3-METHYL-2-OXO-VALERIC ACID
keywords	FLAVOENZYME, FAD COFACTOR, OXIDOREDUCTASE; FLAVOENZYME
method	X-RAY DIFFRACTION

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Download Data

SAXS curve (.dat) P(r) distribution (.pr.out) Structure (CIF)

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2. SAXS Parameters (CRYSOL)

rg_guinier	50.69 Å
rg_electron	50.45 Å
i0	1388240000.00
molecular_weight	314370.0 kDa
excluded_volume	394250 Å³
envelope_volume	511710 Å³
shell_volume	84462 Å³
envelope_diameter	186.3 Å
shell_rg	54.20 Å
envelope_rg	49.67 Å
shape_rg	50.44 Å
total_rg	50.60 Å
total_atoms	22224
n_residues	2712
n_harmonics	20
q_range	— – 0.5000 Å⁻¹
n_points	101
shell_type	directional
solvent_density	0.3340 e/Å³
contrast_shell	0.0300 e/Å³
crysol_version	4.1.3

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3. P(r) Analysis (GNOM)

dmax	174.7 Å
rg_real	50.79 Å
rg_real_error	1.84 Å
i0_real	1.3880e+09
i0_real_error	2.9120e+07
rg_reciprocal	50.59 Å
i0_reciprocal	1388000000.0000
total_estimate	0.8591
solution_quality	GOOD a GOOD solution
n_peaks	2
r_peak_primary	56.4 Å
skewness	0.426
kurtosis	-0.281
angular_range	— – 0.1550 Å⁻¹
current_alpha	0.0000
highest_alpha	66270000.0000
n_real_points	32
gnom_version	4.1.3
quality_criteria	AN1: 0.000; Oscil: 0.811; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.976; Smooth: 0.756

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4. Crystallography & Experiment

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5. Entities & Polymer Info (3)

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6. Citations (1)

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length_a	326.400 Å
length_b	136.900 Å
length_c	196.500 Å
angle_alpha	90.00 °
angle_beta	90.00 °
angle_gamma	90.00 °
z_pdb	64

space_group	C 2 2 21
int_tables_number	20
crystal_system	—

resolution	3.200 Å
resolution_low	20.000 Å
r_factor	0.2320
r_work	0.2320
r_free	0.2600

description	D-AMINO ACID OXIDASE
formula_weight	39377.8 kDa
ec_number	1.4.3.3
src_method	nat
entity_count	8

type	polypeptide(L)
strand_id	A,B,C,D,E,F,G,H
atom_count	22232

COVALENT ADDUCT OF D-AMINO ACID OXIDASE FROM PIG KIDNEY WITH 3-METHYL-2-OXO-VALERIC ACID

SAXS Profile

P(r) Distribution

1. Structure Basics

Download Data

2. SAXS Parameters (CRYSOL)

3. P(r) Analysis (GNOM)

4. Crystallography & Experiment

Unit Cell

Symmetry

Refinement

Diffraction

5. Entities & Polymer Info (3)

Entity 1 polymer

Polymer

Entity 2 non-polymer

Entity 3 water

6. Citations (1)

7. Files & Curves (10)

Files (7)

Curves (3)

description	FLAVIN-ADENINE DINUCLEOTIDE-N5-ISOBUTYL KETONE
formula_weight	855.6 kDa
src_method	syn
entity_count	8

description	water
formula_weight	18.0 kDa
src_method	nat
entity_count	8

fit	/app/data/saxs_computation/da/1dao/1dao.fit
pddf	/app/data/pr_computation/da/1dao/1dao.pr.out
profile	/app/data/saxs_computation/da/1dao/1dao.dat