TRIGONAL CRYSTAL FORM OF HEAT SHOCK LOCUS U (HSLU) FROM ESCHERICHIA COLI

Method: X-RAY DIFFRACTION D_max: 221.2 Å Quality: REASONABLE

SAXS Profile

P(r) Distribution

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1. Structure Basics

entry_id	1do2
deposition_date	1999-12-18
title	TRIGONAL CRYSTAL FORM OF HEAT SHOCK LOCUS U (HSLU) FROM ESCHERICHIA COLI
keywords	HSLU, CLPY, AAA-ATPASE, ATP-DEPENDENT PROTEOLYSIS, PROTEASOME, CHAPERONE; CHAPERONE
method	X-RAY DIFFRACTION

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Download Data

SAXS curve (.dat) P(r) distribution (.pr.out) Structure (CIF)

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2. SAXS Parameters (CRYSOL)

rg_guinier	66.02 Å
rg_electron	66.36 Å
i0	488586000.00
molecular_weight	184120.0 kDa
excluded_volume	230000 Å³
envelope_volume	423310 Å³
shell_volume	51987 Å³
envelope_diameter	218.9 Å
shell_rg	72.24 Å
envelope_rg	62.81 Å
shape_rg	66.37 Å
total_rg	66.45 Å
total_atoms	12926
n_residues	1628
n_harmonics	20
q_range	— – 0.5000 Å⁻¹
n_points	101
shell_type	directional
solvent_density	0.3340 e/Å³
contrast_shell	0.0300 e/Å³
crysol_version	4.1.3

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3. P(r) Analysis (GNOM)

dmax	221.2 Å
rg_real	66.60 Å
rg_real_error	2.74 Å
i0_real	4.8860e+08
i0_real_error	1.0850e+07
rg_reciprocal	65.33 Å
i0_reciprocal	487400000.0000
total_estimate	0.6479
solution_quality	REASONABLE a REASONABLE solution
n_peaks	2
r_peak_primary	36.9 Å
skewness	0.130
kurtosis	-1.279
angular_range	— – 0.1200 Å⁻¹
current_alpha	0.0000
highest_alpha	17280000.0000
n_real_points	25
gnom_version	4.1.3
quality_criteria	AN1: 0.000; Oscil: 0.067; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.467; Smooth: 0.751

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4. Crystallography & Experiment

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5. Entities & Polymer Info (2)

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6. Citations (4)

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length_a	201.777 Å
length_b	201.777 Å
length_c	171.628 Å
angle_alpha	90.00 °
angle_beta	90.00 °
angle_gamma	120.00 °
z_pdb	24

space_group	P 3 2 1
int_tables_number	150
crystal_system	—

resolution	4.000 Å
resolution_low	15.000 Å
r_factor	0.2290
r_work	0.2290
r_free	0.2850

description	PROTEIN (HEAT SHOCK LOCUS U)
formula_weight	49528.5 kDa
src_method	man
entity_count	4

type	polypeptide(L)
strand_id	A,B,C,D
atom_count	12926

TRIGONAL CRYSTAL FORM OF HEAT SHOCK LOCUS U (HSLU) FROM ESCHERICHIA COLI

SAXS Profile

P(r) Distribution

1. Structure Basics

Download Data

2. SAXS Parameters (CRYSOL)

3. P(r) Analysis (GNOM)

4. Crystallography & Experiment

Unit Cell

Symmetry

Refinement

Diffraction

5. Entities & Polymer Info (2)

Entity 1 polymer

Polymer

Source

Entity 2 non-polymer

6. Citations (4)

7. Files & Curves (10)

Files (7)

Curves (3)

organism	Escherichia coli
ncbi_taxonomy_id	562
host_organism	Escherichia coli BL21(DE3)

description	PHOSPHOAMINOPHOSPHONIC ACID-ADENYLATE ESTER
formula_weight	506.2 kDa
src_method	syn
entity_count	2

fit	/app/data/saxs_computation/do/1do2/1do2.fit
pddf	/app/data/pr_computation/do/1do2/1do2.pr.out
profile	/app/data/saxs_computation/do/1do2/1do2.dat