1h1p

Structure of human Thr160-phospho CDK2/cyclin A complexed with the inhibitor NU2058

Method: X-RAY DIFFRACTION Dmax: 116.4 Å Quality: REASONABLE

SAXS 散射曲线 SAXS Profile

SAXS profile for 1h1p

P(r) 距离分布 P(r) Distribution

P(r) distribution for 1h1p
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1. 结构基本信息 1. Structure Basics

条目编号 entry_id1h1p
沉积日期 deposition_date2002-07-21
结构标题 titleStructure of human Thr160-phospho CDK2/cyclin A complexed with the inhibitor NU2058
关键词 keywordsKINASE, TRANSFERASE, SERINE/THREONINE-PROTEIN KINASE, ATP-BINDING, CELL CYCLE, CELL DIVISION, MITOSIS, PHOSPHORYLATION; TRANSFERASE
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier35.56
回转半径 Rg (电子) rg_electron34.89
零角强度 I(0) i0222856000.00
分子量 molecular_weight127260.0 kDa
排除体积 excluded_volume162080 ų
包络体积 envelope_volume199940 ų
水化壳体积 shell_volume47347 ų
包络直径 envelope_diameter122.7
壳层 Rg shell_rg41.90
包络 Rg envelope_rg34.46
形状 Rg shape_rg34.93
总 Rg total_rg35.26
总原子数 total_atoms8978
残基数 n_residues1108
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax116.4
Rg (实空间) rg_real35.51
Rg 误差 (实空间) rg_real_error1.06
I(0) (实空间) i0_real2.2290e+08
I(0) 误差 (实空间) i0_real_error3.7590e+06
Rg (倒空间) rg_reciprocal35.54
I(0) (倒空间) i0_reciprocal222900000.0000
解质量估计 total_estimate0.6803
解质量评级 solution_quality REASONABLE a REASONABLE solution
P(r) 峰数 n_peaks2
主峰位置 r_peak_primary47.6
偏度 Skewness skewness0.273
峰度 Kurtosis kurtosis-0.376
角度范围 angular_range— – 0.2200 −1
当前正则化参数 α current_alpha0.0000
最高正则化参数 α highest_alpha102500000.0000
实空间数据点数 n_real_points45
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.897; Stabil: 1.000; Sysdev: 0.101; Positv: 1.000; Valcen: 0.994; Smooth: 0.851

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (4)

6. 折叠分类 (SCOP + CATH) 16 domains

SCOP 2.08 (8 domains)

结构域编号 domain_idd1h1pa1
类 Class classd — Alpha and beta proteins (a+b)
折叠类型 Fold foldd.144 — Protein kinase-like (PK-like)
超家族 Superfamily superfamilyd.144.1 — Protein kinase-like (PK-like)
家族 Family familyd.144.1.7 — Protein kinases, catalytic subunit
结构域编号 domain_idd1h1pa2
类 Class classl — Artifacts
折叠类型 Fold foldl.1 — Tags
超家族 Superfamily superfamilyl.1.1 — Tags
家族 Family familyl.1.1.1 — Tags
结构域编号 domain_idd1h1pb1
类 Class classa — All alpha proteins
折叠类型 Fold folda.74 — Cyclin-like
超家族 Superfamily superfamilya.74.1 — Cyclin-like
家族 Family familya.74.1.1 — Cyclin
结构域编号 domain_idd1h1pb2
类 Class classa — All alpha proteins
折叠类型 Fold folda.74 — Cyclin-like
超家族 Superfamily superfamilya.74.1 — Cyclin-like
家族 Family familya.74.1.1 — Cyclin
结构域编号 domain_idd1h1pc1
类 Class classd — Alpha and beta proteins (a+b)
折叠类型 Fold foldd.144 — Protein kinase-like (PK-like)
超家族 Superfamily superfamilyd.144.1 — Protein kinase-like (PK-like)
家族 Family familyd.144.1.7 — Protein kinases, catalytic subunit
结构域编号 domain_idd1h1pc2
类 Class classl — Artifacts
折叠类型 Fold foldl.1 — Tags
超家族 Superfamily superfamilyl.1.1 — Tags
家族 Family familyl.1.1.1 — Tags
结构域编号 domain_idd1h1pd1
类 Class classa — All alpha proteins
折叠类型 Fold folda.74 — Cyclin-like
超家族 Superfamily superfamilya.74.1 — Cyclin-like
家族 Family familya.74.1.1 — Cyclin
结构域编号 domain_idd1h1pd2
类 Class classa — All alpha proteins
折叠类型 Fold folda.74 — Cyclin-like
超家族 Superfamily superfamilya.74.1 — Cyclin-like
家族 Family familya.74.1.1 — Cyclin

CATH v4.4 (8 domains)

结构域编号 domain_id1h1pA01
类 Class class3 — Alpha Beta
架构 Architecture architecture30 — 2-Layer Sandwich
拓扑 Topology topology200 — Phosphorylase Kinase; domain 1
同源超家族 H-superfamily homologous superfamily20 — Phosphorylase Kinase; domain 1
结构域编号 domain_id1h1pA02
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology510 — Transferase(Phosphotransferase); domain 1
同源超家族 H-superfamily homologous superfamily10 — Transferase(Phosphotransferase) domain 1
结构域编号 domain_id1h1pB01
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology472 — Cyclin A; domain 1
同源超家族 H-superfamily homologous superfamily10 — Cyclin-like
结构域编号 domain_id1h1pB02
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology472 — Cyclin A; domain 1
同源超家族 H-superfamily homologous superfamily10 — Cyclin-like
结构域编号 domain_id1h1pC01
类 Class class3 — Alpha Beta
架构 Architecture architecture30 — 2-Layer Sandwich
拓扑 Topology topology200 — Phosphorylase Kinase; domain 1
同源超家族 H-superfamily homologous superfamily20 — Phosphorylase Kinase; domain 1
结构域编号 domain_id1h1pC02
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology510 — Transferase(Phosphotransferase); domain 1
同源超家族 H-superfamily homologous superfamily10 — Transferase(Phosphotransferase) domain 1
结构域编号 domain_id1h1pD01
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology472 — Cyclin A; domain 1
同源超家族 H-superfamily homologous superfamily10 — Cyclin-like
结构域编号 domain_id1h1pD02
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology472 — Cyclin A; domain 1
同源超家族 H-superfamily homologous superfamily10 — Cyclin-like

7. 引用文献 (1)

8. 文件与曲线 (10)