1qlu

STRUCTURE OF THE H422A MUTANT VANILLYL-ALCOHOL OXIDASE IN COMPLEX WITH ISOEUGENOL

Method: X-RAY DIFFRACTION Dmax: 98.4 Å Quality: GOOD

SAXS 散射曲线 SAXS Profile

SAXS profile for 1qlu

P(r) 距离分布 P(r) Distribution

P(r) distribution for 1qlu
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1. 结构基本信息 1. Structure Basics

条目编号 entry_id1qlu
沉积日期 deposition_date1999-09-16
结构标题 titleSTRUCTURE OF THE H422A MUTANT VANILLYL-ALCOHOL OXIDASE IN COMPLEX WITH ISOEUGENOL
关键词 keywordsOXIDOREDUCTASE, FLAVOPROTEIN, METHANOL UTILIZATION, PEROXISOME, FLAVOENZYME, OXIDASE, CATALYSIS; OXIDOREDUCTASE
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier30.27
回转半径 Rg (电子) rg_electron29.41
零角强度 I(0) i0238006000.00
分子量 molecular_weight125150.0 kDa
排除体积 excluded_volume157140 ų
包络体积 envelope_volume178840 ų
水化壳体积 shell_volume48195 ų
包络直径 envelope_diameter99.3
壳层 Rg shell_rg38.62
包络 Rg envelope_rg29.65
形状 Rg shape_rg29.40
总 Rg total_rg30.19
总原子数 total_atoms8820
残基数 n_residues1100
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax98.4
Rg (实空间) rg_real30.12
Rg 误差 (实空间) rg_real_error0.53
I(0) (实空间) i0_real2.3800e+08
I(0) 误差 (实空间) i0_real_error3.3270e+06
Rg (倒空间) rg_reciprocal30.18
I(0) (倒空间) i0_reciprocal238000000.0000
解质量估计 total_estimate0.8882
解质量评级 solution_quality GOOD a GOOD solution
P(r) 峰数 n_peaks1
主峰位置 r_peak_primary37.8
偏度 Skewness skewness0.215
峰度 Kurtosis kurtosis-0.411
角度范围 angular_range— – 0.2600 −1
当前正则化参数 α current_alpha0.0000
最高正则化参数 α highest_alpha122600000.0000
实空间数据点数 n_real_points53
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.853; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.996; Smooth: 0.987

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (4)

6. 折叠分类 (SCOP + CATH) 12 domains

SCOP 2.08 (4 domains)

结构域编号 domain_idd1qlua1
类 Class classd — Alpha and beta proteins (a+b)
折叠类型 Fold foldd.58 — Ferredoxin-like
超家族 Superfamily superfamilyd.58.32 — FAD-linked oxidases, C-terminal domain
家族 Family familyd.58.32.1 — Vanillyl-alcohol oxidase-like
结构域编号 domain_idd1qlua2
类 Class classd — Alpha and beta proteins (a+b)
折叠类型 Fold foldd.145 — FAD-binding/transporter-associated domain-like
超家族 Superfamily superfamilyd.145.1 — FAD-binding/transporter-associated domain-like
家族 Family familyd.145.1.1 — FAD-linked oxidases, N-terminal domain
结构域编号 domain_idd1qlub1
类 Class classd — Alpha and beta proteins (a+b)
折叠类型 Fold foldd.58 — Ferredoxin-like
超家族 Superfamily superfamilyd.58.32 — FAD-linked oxidases, C-terminal domain
家族 Family familyd.58.32.1 — Vanillyl-alcohol oxidase-like
结构域编号 domain_idd1qlub2
类 Class classd — Alpha and beta proteins (a+b)
折叠类型 Fold foldd.145 — FAD-binding/transporter-associated domain-like
超家族 Superfamily superfamilyd.145.1 — FAD-binding/transporter-associated domain-like
家族 Family familyd.145.1.1 — FAD-linked oxidases, N-terminal domain

CATH v4.4 (8 domains)

结构域编号 domain_id1qluA01
类 Class class3 — Alpha Beta
架构 Architecture architecture30 — 2-Layer Sandwich
拓扑 Topology topology43 — Uridine Diphospho-n-acetylenolpyruvylglucosamine Reductase; domain 2
同源超家族 H-superfamily homologous superfamily10 — Uridine Diphospho-n-acetylenolpyruvylglucosamine Reductase, domain 2
结构域编号 domain_id1qluA02
类 Class class3 — Alpha Beta
架构 Architecture architecture30 — 2-Layer Sandwich
拓扑 Topology topology465 — Uridine Diphospho-n-acetylenolpyruvylglucosamine Reductase; domain 3
同源超家族 H-superfamily homologous superfamily10
结构域编号 domain_id1qluA03
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology462 — Vanillyl-alcohol Oxidase; Chain A, domain 3
同源超家族 H-superfamily homologous superfamily10 — FAD-linked oxidases, C-terminal domain
结构域编号 domain_id1qluA04
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology45 — Vanillyl-alcohol Oxidase; Chain A, domain 4
同源超家族 H-superfamily homologous superfamily10 — Vanillyl-alcohol Oxidase; Chain A, domain 4
结构域编号 domain_id1qluB01
类 Class class3 — Alpha Beta
架构 Architecture architecture30 — 2-Layer Sandwich
拓扑 Topology topology43 — Uridine Diphospho-n-acetylenolpyruvylglucosamine Reductase; domain 2
同源超家族 H-superfamily homologous superfamily10 — Uridine Diphospho-n-acetylenolpyruvylglucosamine Reductase, domain 2
结构域编号 domain_id1qluB02
类 Class class3 — Alpha Beta
架构 Architecture architecture30 — 2-Layer Sandwich
拓扑 Topology topology465 — Uridine Diphospho-n-acetylenolpyruvylglucosamine Reductase; domain 3
同源超家族 H-superfamily homologous superfamily10
结构域编号 domain_id1qluB03
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology462 — Vanillyl-alcohol Oxidase; Chain A, domain 3
同源超家族 H-superfamily homologous superfamily10 — FAD-linked oxidases, C-terminal domain
结构域编号 domain_id1qluB04
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology45 — Vanillyl-alcohol Oxidase; Chain A, domain 4
同源超家族 H-superfamily homologous superfamily10 — Vanillyl-alcohol Oxidase; Chain A, domain 4

7. 引用文献 (2)

8. 文件与曲线 (10)