1y8n

Crystal structure of the PDK3-L2 complex

Method: X-RAY DIFFRACTION Dmax: 92.9 Å Quality: GOOD

SAXS 散射曲线 SAXS Profile

SAXS profile for 1y8n

P(r) 距离分布 P(r) Distribution

P(r) distribution for 1y8n
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1. 结构基本信息 1. Structure Basics

条目编号 entry_id1y8n
沉积日期 deposition_date2004-12-13
结构标题 titleCrystal structure of the PDK3-L2 complex
关键词 keywordspyruvate dehydrogenase kinase 3, lipoyl-bearing domain, protein-protein complex, TRANSFERASE; TRANSFERASE
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier26.72
回转半径 Rg (电子) rg_electron25.78
零角强度 I(0) i045487000.00
分子量 molecular_weight53960.0 kDa
排除体积 excluded_volume68222 ų
包络体积 envelope_volume87863 ų
水化壳体积 shell_volume28754 ų
包络直径 envelope_diameter96.0
壳层 Rg shell_rg32.49
包络 Rg envelope_rg26.37
形状 Rg shape_rg25.77
总 Rg total_rg26.57
总原子数 total_atoms3802
残基数 n_residues471
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax92.9
Rg (实空间) rg_real26.72
Rg 误差 (实空间) rg_real_error0.69
I(0) (实空间) i0_real4.5490e+07
I(0) 误差 (实空间) i0_real_error6.1790e+05
Rg (倒空间) rg_reciprocal26.72
I(0) (倒空间) i0_reciprocal45490000.0000
解质量估计 total_estimate0.8675
解质量评级 solution_quality GOOD a GOOD solution
P(r) 峰数 n_peaks2
主峰位置 r_peak_primary31.5
偏度 Skewness skewness0.366
峰度 Kurtosis kurtosis-0.173
角度范围 angular_range— – 0.2950 −1
当前正则化参数 α current_alpha0.0000
最高正则化参数 α highest_alpha10160000.0000
实空间数据点数 n_real_points60
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.789; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.940; Smooth: 0.966

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (5)

6. 折叠分类 (SCOP + CATH) 6 domains

SCOP 2.08 (3 domains)

结构域编号 domain_idd1y8na1
类 Class classa — All alpha proteins
折叠类型 Fold folda.29 — Bromodomain-like
超家族 Superfamily superfamilya.29.5 — alpha-ketoacid dehydrogenase kinase, N-terminal domain
家族 Family familya.29.5.1 — alpha-ketoacid dehydrogenase kinase, N-terminal domain
结构域编号 domain_idd1y8na2
类 Class classd — Alpha and beta proteins (a+b)
折叠类型 Fold foldd.122 — ATPase domain of HSP90 chaperone/DNA topoisomerase II/histidine kinase
超家族 Superfamily superfamilyd.122.1 — ATPase domain of HSP90 chaperone/DNA topoisomerase II/histidine kinase
家族 Family familyd.122.1.4 — alpha-ketoacid dehydrogenase kinase, C-terminal domain
结构域编号 domain_idd1y8nb_
类 Class classb — All beta proteins
折叠类型 Fold foldb.84 — Barrel-sandwich hybrid
超家族 Superfamily superfamilyb.84.1 — Single hybrid motif
家族 Family familyb.84.1.1 — Biotinyl/lipoyl-carrier proteins and domains

CATH v4.4 (3 domains)

结构域编号 domain_id1y8nA01
类 Class class1 — Mainly Alpha
架构 Architecture architecture20 — Up-down Bundle
拓扑 Topology topology140 — Butyryl-CoA Dehydrogenase, subunit A; domain 3
同源超家族 H-superfamily homologous superfamily20 — Alpha-ketoacid/pyruvate dehydrogenase kinase, N-terminal domain
结构域编号 domain_id1y8nA02
类 Class class3 — Alpha Beta
架构 Architecture architecture30 — 2-Layer Sandwich
拓扑 Topology topology565 — Heat Shock Protein 90
同源超家族 H-superfamily homologous superfamily10 — Histidine kinase-like ATPase, C-terminal domain
结构域编号 domain_id1y8nB00
类 Class class2 — Mainly Beta
架构 Architecture architecture40 — Beta Barrel
拓扑 Topology topology50 — OB fold (Dihydrolipoamide Acetyltransferase, E2P)
同源超家族 H-superfamily homologous superfamily100 — RNA polymerase II/Efflux pump adaptor protein, barrel-sandwich hybrid domain

7. 引用文献 (1)

8. 文件与曲线 (10)