2cke

Human death-associated DRP-1 kinase in complex with inhibitor

Method: X-RAY DIFFRACTION Dmax: 155.7 Å Quality: GOOD

SAXS 散射曲线 SAXS Profile

SAXS profile for 2cke

P(r) 距离分布 P(r) Distribution

P(r) distribution for 2cke
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1. 结构基本信息 1. Structure Basics

条目编号 entry_id2cke
沉积日期 deposition_date2006-04-18
结构标题 titleHuman death-associated DRP-1 kinase in complex with inhibitor
关键词 keywordsTRANSFERASE-INHIBITOR COMPLEX, CALMODULIN-BINDING, NUCLEOTIDE-BINDING, SERINE/THREONINE-PROTEIN KINASE, APOPTOSIS; TRANSFERASE/INHIBITOR
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier43.66
回转半径 Rg (电子) rg_electron43.96
零角强度 I(0) i0274234000.00
分子量 molecular_weight139310.0 kDa
排除体积 excluded_volume176030 ų
包络体积 envelope_volume239580 ų
水化壳体积 shell_volume49162 ų
包络直径 envelope_diameter165.4
壳层 Rg shell_rg44.27
包络 Rg envelope_rg43.47
形状 Rg shape_rg43.95
总 Rg total_rg44.02
总原子数 total_atoms9844
残基数 n_residues1201
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax155.7
Rg (实空间) rg_real44.16
Rg 误差 (实空间) rg_real_error1.74
I(0) (实空间) i0_real2.7420e+08
I(0) 误差 (实空间) i0_real_error5.4860e+06
Rg (倒空间) rg_reciprocal43.67
I(0) (倒空间) i0_reciprocal274100000.0000
解质量估计 total_estimate0.7839
解质量评级 solution_quality GOOD a GOOD solution
P(r) 峰数 n_peaks2
主峰位置 r_peak_primary38.9
偏度 Skewness skewness0.594
峰度 Kurtosis kurtosis-0.305
角度范围 angular_range— – 0.1800 −1
当前正则化参数 α current_alpha0.0000
最高正则化参数 α highest_alpha32460000.0000
实空间数据点数 n_real_points37
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.607; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.662; Smooth: 0.705

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (3)

6. 折叠分类 (SCOP + CATH) 12 domains

SCOP 2.08 (4 domains)

结构域编号 domain_idd2ckea_
类 Class classd — Alpha and beta proteins (a+b)
折叠类型 Fold foldd.144 — Protein kinase-like (PK-like)
超家族 Superfamily superfamilyd.144.1 — Protein kinase-like (PK-like)
家族 Family familyd.144.1.0 — automated matches
结构域编号 domain_idd2ckeb_
类 Class classd — Alpha and beta proteins (a+b)
折叠类型 Fold foldd.144 — Protein kinase-like (PK-like)
超家族 Superfamily superfamilyd.144.1 — Protein kinase-like (PK-like)
家族 Family familyd.144.1.0 — automated matches
结构域编号 domain_idd2ckec_
类 Class classd — Alpha and beta proteins (a+b)
折叠类型 Fold foldd.144 — Protein kinase-like (PK-like)
超家族 Superfamily superfamilyd.144.1 — Protein kinase-like (PK-like)
家族 Family familyd.144.1.0 — automated matches
结构域编号 domain_idd2cked_
类 Class classd — Alpha and beta proteins (a+b)
折叠类型 Fold foldd.144 — Protein kinase-like (PK-like)
超家族 Superfamily superfamilyd.144.1 — Protein kinase-like (PK-like)
家族 Family familyd.144.1.0 — automated matches

CATH v4.4 (8 domains)

结构域编号 domain_id2ckeA01
类 Class class3 — Alpha Beta
架构 Architecture architecture30 — 2-Layer Sandwich
拓扑 Topology topology200 — Phosphorylase Kinase; domain 1
同源超家族 H-superfamily homologous superfamily20 — Phosphorylase Kinase; domain 1
结构域编号 domain_id2ckeA02
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology510 — Transferase(Phosphotransferase); domain 1
同源超家族 H-superfamily homologous superfamily10 — Transferase(Phosphotransferase) domain 1
结构域编号 domain_id2ckeB01
类 Class class3 — Alpha Beta
架构 Architecture architecture30 — 2-Layer Sandwich
拓扑 Topology topology200 — Phosphorylase Kinase; domain 1
同源超家族 H-superfamily homologous superfamily20 — Phosphorylase Kinase; domain 1
结构域编号 domain_id2ckeB02
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology510 — Transferase(Phosphotransferase); domain 1
同源超家族 H-superfamily homologous superfamily10 — Transferase(Phosphotransferase) domain 1
结构域编号 domain_id2ckeC01
类 Class class3 — Alpha Beta
架构 Architecture architecture30 — 2-Layer Sandwich
拓扑 Topology topology200 — Phosphorylase Kinase; domain 1
同源超家族 H-superfamily homologous superfamily20 — Phosphorylase Kinase; domain 1
结构域编号 domain_id2ckeC02
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology510 — Transferase(Phosphotransferase); domain 1
同源超家族 H-superfamily homologous superfamily10 — Transferase(Phosphotransferase) domain 1
结构域编号 domain_id2ckeD01
类 Class class3 — Alpha Beta
架构 Architecture architecture30 — 2-Layer Sandwich
拓扑 Topology topology200 — Phosphorylase Kinase; domain 1
同源超家族 H-superfamily homologous superfamily20 — Phosphorylase Kinase; domain 1
结构域编号 domain_id2ckeD02
类 Class class1 — Mainly Alpha
架构 Architecture architecture10 — Orthogonal Bundle
拓扑 Topology topology510 — Transferase(Phosphotransferase); domain 1
同源超家族 H-superfamily homologous superfamily10 — Transferase(Phosphotransferase) domain 1

7. 引用文献 (1)

8. 文件与曲线 (10)