2efr

;Crystal structure of the c-terminal tropomyosin fragment with N- and C-terminal extensions of the leucine zipper at 1.8 angstroms resolution ;

Method: X-RAY DIFFRACTION Dmax: 221.6 Å Quality: SUSPICIOUS

SAXS 散射曲线 SAXS Profile

SAXS profile for 2efr

P(r) 距离分布 P(r) Distribution

P(r) distribution for 2efr
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1. 结构基本信息 1. Structure Basics

条目编号 entry_id2efr
沉积日期 deposition_date2007-02-23
结构标题 title;Crystal structure of the c-terminal tropomyosin fragment with N- and C-terminal extensions of the leucine zipper at 1.8 angstroms resolution ;
关键词 keywordsDESTABILIZING CLUSTER, HYDROPHOBIC CORE, CONTRACTILE PROTEIN; CONTRACTILE PROTEIN
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier87.79
回转半径 Rg (电子) rg_electron92.42
零角强度 I(0) i079177100.00
分子量 molecular_weight72868.0 kDa
排除体积 excluded_volume91271 ų
包络体积 envelope_volume178180 ų
水化壳体积 shell_volume24535 ų
包络直径 envelope_diameter353.7
壳层 Rg shell_rg45.58
包络 Rg envelope_rg95.65
形状 Rg shape_rg92.27
总 Rg total_rg91.39
总原子数 total_atoms5118
残基数 n_residues618
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax221.6
Rg (实空间) rg_real77.97
Rg 误差 (实空间) rg_real_error1.65
I(0) (实空间) i0_real7.5140e+07
I(0) 误差 (实空间) i0_real_error1.6340e+06
Rg (倒空间) rg_reciprocal77.56
I(0) (倒空间) i0_reciprocal76930000.0000
解质量估计 total_estimate0.4593
解质量评级 solution_quality SUSPICIOUS a SUSPICIOUS solution
P(r) 峰数 n_peaks3
主峰位置 r_peak_primary24.6
偏度 Skewness skewness0.340
峰度 Kurtosis kurtosis-0.996
角度范围 angular_range— – 0.0900 −1
当前正则化参数 α current_alpha0.0580
最高正则化参数 α highest_alpha7818000.0000
实空间数据点数 n_real_points19
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.018; Oscil: 0.269; Stabil: 0.906; Sysdev: 0.000; Positv: 1.000; Valcen: 0.243; Smooth: 0.202

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (2)

6. 折叠分类 (SCOP + CATH) 4 domains

CATH v4.4 (4 domains)

结构域编号 domain_id2efrA00
类 Class class1 — Mainly Alpha
架构 Architecture architecture20 — Up-down Bundle
拓扑 Topology topology5 — Single alpha-helices involved in coiled-coils or other helix-helix interfaces
同源超家族 H-superfamily homologous superfamily170
结构域编号 domain_id2efrB00
类 Class class1 — Mainly Alpha
架构 Architecture architecture20 — Up-down Bundle
拓扑 Topology topology5 — Single alpha-helices involved in coiled-coils or other helix-helix interfaces
同源超家族 H-superfamily homologous superfamily170
结构域编号 domain_id2efrC00
类 Class class1 — Mainly Alpha
架构 Architecture architecture20 — Up-down Bundle
拓扑 Topology topology5 — Single alpha-helices involved in coiled-coils or other helix-helix interfaces
同源超家族 H-superfamily homologous superfamily170
结构域编号 domain_id2efrD00
类 Class class1 — Mainly Alpha
架构 Architecture architecture20 — Up-down Bundle
拓扑 Topology topology5 — Single alpha-helices involved in coiled-coils or other helix-helix interfaces
同源超家族 H-superfamily homologous superfamily170

7. 引用文献 (1)

8. 文件与曲线 (10)