1bx3
EFFECTS OF COMMONLY USED CRYOPROTECTANTS ON GLYCOGEN PHOSPHORYLASE ACTIVITY AND STRUCTURE
SAXS Profile
P(r) Distribution
1. Structure Basics
| entry_id | 1bx3 |
| deposition_date | 1999-10-13 |
| title | EFFECTS OF COMMONLY USED CRYOPROTECTANTS ON GLYCOGEN PHOSPHORYLASE ACTIVITY AND STRUCTURE |
| keywords | PHOSPHORYLASE, INHIBITOR, CRYOPROTECTANT, MPD, DMSO, CRYOCRYSTALLOGRAPHY, TRANSFERASE; TRANSFERASE |
| method | X-RAY DIFFRACTION |
Download Data
2. SAXS Parameters (CRYSOL)
| rg_guinier | 28.11 Å |
| rg_electron | 27.07 Å |
| i0 | 134955000.00 |
| molecular_weight | 92651.0 kDa |
| excluded_volume | 116300 ų |
| envelope_volume | 134720 ų |
| shell_volume | 39854 ų |
| envelope_diameter | 96.8 Å |
| shell_rg | 35.89 Å |
| envelope_rg | 27.35 Å |
| shape_rg | 27.08 Å |
| total_rg | 27.88 Å |
| total_atoms | 6534 |
| n_residues | 801 |
| n_harmonics | 20 |
| q_range | — – 0.5000 Å−1 |
| n_points | 101 |
| shell_type | directional |
| solvent_density | 0.3340 e/ų |
| contrast_shell | 0.0300 e/ų |
| crysol_version | 4.1.3 |
3. P(r) Analysis (GNOM)
| dmax | 89.3 Å |
| rg_real | 27.94 Å |
| rg_real_error | 0.48 Å |
| i0_real | 1.3500e+08 |
| i0_real_error | 1.9020e+06 |
| rg_reciprocal | 28.00 Å |
| i0_reciprocal | 135000000.0000 |
| total_estimate | 0.8975 |
| solution_quality | GOOD a GOOD solution |
| n_peaks | 2 |
| r_peak_primary | 33.5 Å |
| skewness | 0.193 |
| kurtosis | -0.479 |
| angular_range | — – 0.2800 Å−1 |
| current_alpha | 0.0000 |
| highest_alpha | 39030000.0000 |
| n_real_points | 57 |
| gnom_version | 4.1.3 |
| quality_criteria | AN1: 0.000; Oscil: 0.893; Stabil: 1.000; Sysdev: 1.000; Positv: 1.000; Valcen: 0.995; Smooth: 0.989 |