1g8h

ATP SULFURYLASE FROM S. CEREVISIAE: THE TERNARY PRODUCT COMPLEX WITH APS AND PPI

Method: X-RAY DIFFRACTION Dmax: 141.4 Å Quality: GOOD

SAXS 散射曲线 SAXS Profile

SAXS profile for 1g8h

P(r) 距离分布 P(r) Distribution

P(r) distribution for 1g8h
下载 Download

1. 结构基本信息 1. Structure Basics

条目编号 entry_id1g8h
沉积日期 deposition_date2000-11-17
结构标题 titleATP SULFURYLASE FROM S. CEREVISIAE: THE TERNARY PRODUCT COMPLEX WITH APS AND PPI
关键词 keywords;alpha-beta protein, beta-barrel, Rossmann-fold, kinase fold, product complex with adenosine-5'-phosphosulfate and pyrophosphate, displacement mechanism, TRANSFERASE ;; TRANSFERASE
实验方法 methodX-RAY DIFFRACTION

2. SAXS 参数 (CRYSOL 理论计算) 2. SAXS Parameters (CRYSOL)

回转半径 Rg (Guinier) rg_guinier47.16
回转半径 Rg (电子) rg_electron47.26
零角强度 I(0) i0209518000.00
分子量 molecular_weight119120.0 kDa
排除体积 excluded_volume148240 ų
包络体积 envelope_volume213370 ų
水化壳体积 shell_volume37116 ų
包络直径 envelope_diameter155.3
壳层 Rg shell_rg53.34
包络 Rg envelope_rg45.24
形状 Rg shape_rg47.23
总 Rg total_rg47.61
总原子数 total_atoms8317
残基数 n_residues1020
球谐函数阶数 n_harmonics20
q 范围 q_range— – 0.5000 −1
数据点数 n_points101
壳层类型 shell_typedirectional
溶剂电子密度 solvent_density0.3340 e/ų
壳层衬度 contrast_shell0.0300 e/ų
CRYSOL 版本 crysol_version4.1.3

3. P(r) 距离分布 (GNOM 反演) 3. P(r) Analysis (GNOM)

最大尺寸 Dmax dmax141.4
Rg (实空间) rg_real47.49
Rg 误差 (实空间) rg_real_error1.44
I(0) (实空间) i0_real2.0950e+08
I(0) 误差 (实空间) i0_real_error4.2330e+06
Rg (倒空间) rg_reciprocal47.16
I(0) (倒空间) i0_reciprocal209400000.0000
解质量估计 total_estimate0.7505
解质量评级 solution_quality GOOD a GOOD solution
P(r) 峰数 n_peaks3
主峰位置 r_peak_primary30.0
偏度 Skewness skewness0.230
峰度 Kurtosis kurtosis-1.001
角度范围 angular_range— – 0.1650 −1
当前正则化参数 α current_alpha0.0000
最高正则化参数 α highest_alpha9216000.0000
实空间数据点数 n_real_points34
GNOM 版本 gnom_version4.1.3
质量判据 quality_criteria AN1: 0.000; Oscil: 0.703; Stabil: 0.999; Sysdev: 1.000; Positv: 1.000; Valcen: 0.635; Smooth: 0.010

4. 晶体学与实验 4. Crystallography & Experiment

5. 实体与聚合体信息 (9)

6. 折叠分类 (SCOP + CATH) 12 domains

SCOP 2.08 (6 domains)

结构域编号 domain_idd1g8ha1
类 Class classb — All beta proteins
折叠类型 Fold foldb.122 — PUA domain-like
超家族 Superfamily superfamilyb.122.1 — PUA domain-like
家族 Family familyb.122.1.3 — ATP sulfurylase N-terminal domain
结构域编号 domain_idd1g8ha2
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.26 — Adenine nucleotide alpha hydrolase-like
超家族 Superfamily superfamilyc.26.1 — Nucleotidylyl transferase
家族 Family familyc.26.1.5 — ATP sulfurylase catalytic domain
结构域编号 domain_idd1g8ha3
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.37 — P-loop containing nucleoside triphosphate hydrolases
超家族 Superfamily superfamilyc.37.1 — P-loop containing nucleoside triphosphate hydrolases
家族 Family familyc.37.1.15 — ATP sulfurylase C-terminal domain
结构域编号 domain_idd1g8hb1
类 Class classb — All beta proteins
折叠类型 Fold foldb.122 — PUA domain-like
超家族 Superfamily superfamilyb.122.1 — PUA domain-like
家族 Family familyb.122.1.3 — ATP sulfurylase N-terminal domain
结构域编号 domain_idd1g8hb2
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.26 — Adenine nucleotide alpha hydrolase-like
超家族 Superfamily superfamilyc.26.1 — Nucleotidylyl transferase
家族 Family familyc.26.1.5 — ATP sulfurylase catalytic domain
结构域编号 domain_idd1g8hb3
类 Class classc — Alpha and beta proteins (a/b)
折叠类型 Fold foldc.37 — P-loop containing nucleoside triphosphate hydrolases
超家族 Superfamily superfamilyc.37.1 — P-loop containing nucleoside triphosphate hydrolases
家族 Family familyc.37.1.15 — ATP sulfurylase C-terminal domain

CATH v4.4 (6 domains)

结构域编号 domain_id1g8hA01
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily620 — HUPs
结构域编号 domain_id1g8hA02
类 Class class3 — Alpha Beta
架构 Architecture architecture10 — Roll
拓扑 Topology topology400 — Sulfate adenylyltransferase
同源超家族 H-superfamily homologous superfamily10 — Sulfate adenylyltransferase
结构域编号 domain_id1g8hA03
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily300 — P-loop containing nucleotide triphosphate hydrolases
结构域编号 domain_id1g8hB01
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily620 — HUPs
结构域编号 domain_id1g8hB02
类 Class class3 — Alpha Beta
架构 Architecture architecture10 — Roll
拓扑 Topology topology400 — Sulfate adenylyltransferase
同源超家族 H-superfamily homologous superfamily10 — Sulfate adenylyltransferase
结构域编号 domain_id1g8hB03
类 Class class3 — Alpha Beta
架构 Architecture architecture40 — 3-Layer(aba) Sandwich
拓扑 Topology topology50 — Rossmann fold
同源超家族 H-superfamily homologous superfamily300 — P-loop containing nucleotide triphosphate hydrolases

7. 引用文献 (1)

8. 文件与曲线 (10)